Process for producing biopolymer nanoparticles
A process for producing a biopolymer nanoparticles product is disclosed. In this process, biopolymer feedstock and a plasticizer are fed to a feed zone of an extruder having a screw configuration in which the feedstock is process using shear forces in the extruder, and a crosslinking agent is added to the extruder downstream of the feed zone. The biopolymer feedstock and plasticizer are preferably added separately to the feed zone. The screw configuration may include two or more steam seal sections. Shear forces in a first section of the extruder may be greater than shear forces in an adjacent second section of the extruder downstream of the first section. In a post reaction section located after a point in which the crosslinking reaction has been completed, water may be added to improve die performance.
1. A process for producing a biopolymer product, the process comprising:
feeding biopolymer feedstock and a plasticizer to a feed zone of an
extruder having a screw configuration such that the biopolymer feedstock is processed using shear forces in the extruder;
wherein the screw configuration includes two or more steam seal sections to prevent water from flashing to steam and back venting to the feed zone, and wherein each of the two or more steam seal sections has an upstream pressure generating section and an adjacent downstream reverse kneading block, the upstream pressure generating section providing enough forward pumping action to overcome a seal formed by the adjacent downstream reverse kneading block; and
increasing the pressure in the extruder faster than the vapor pressure of water
increases due to increasing temperature in the reverse kneading blocks.
2. The process of claim 1 wherein:
each upstream pressure generating section has a forward kneading block.
3. The process of claim 1 wherein the plasticizer comprises water.