IP Library Granted Patent US 8,268,854
Granted Patent B2
US 8,268,854 · App. 12/471,019 · Granted Sep 18, 2012

Aza-beta-carbolines and methods of using same

Assignee: The UWM Research Foundation, Inc.
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Quick Facts
Patent No.
US 8,268,854
App. No.
12/471,019
Granted
Sep 18, 2012
Kind
B2
Abstract

Provided are compounds having the general structure according to Formula (I): Further provided are pharmaceutical compositions comprising these compounds. The invention still further provides methods of treating alcoholism, methods of reducing alcohol intake, methods of treating anhedonia, and methods of treating anxiety using theses compounds or the compositions containing them.

Claims (28)

1. A compound according to Formula (I):

or isomers, or salts thereof;

wherein X 4 , X 5 , and X 8 are CH, X 6 may be N, + NR 6 or CR 6 , and X 7 may be N, + NR 6 or CR 7 , and wherein either X 6 or X 7 is N;

wherein X 9 is NH;

wherein R 3 is CO 2 R, or OR 1 or COR;

wherein R 6 and R 7 are independently H, X, —C≡CR 2 , lower alkyl, lower alkenyl, or lower alkynyl;

wherein R is —C(CH 3 ) 3-n (CF 3 ) n , —C(CH 3 ) 3-r (CH 3-p X p ) r , —CH(CH 3 ) 2-m (CF 3 ) m , or —CH(CH 3 ) 2-t (CH 3-p X p ) t ;

wherein R 1 is —CH 2 CH 2 CH 3 , —CH(CH 3 ) 2 , —CH 2 CH 2 CH 2 CH 3 , —CH 2 CH(CH 3 ) 2 , —CH(CH 3 )CH 2 CH 3 , —CH 2 CH 2 CH 2 CH 2 CH 3 , —CH 2 CH 2 CH(CH 3 ) 2 , —CH 2 CH(CH 3 )CH 2 CH 3 , or —CH(CH 3 )CH 2 CH 2 CH 3 , wherein any of the hydrogens of R 1 may be replaced by X;

wherein R 2 is H, lower alkyl, Me 3 Si, Et 3 Si, n-Pr 3 Si, or i-Pr 3 Si;

wherein n is an integer from 0 to 3, m is an integer from 0 to 2, r is an integer from 1 to 3, p is an integer from 1 to 2, and t is an integer from 0 to 2; and

wherein X is independently selected from F, Cl, Br and I.

2. A compound according to claim 1 , wherein X 6 is N.

3. A compound according to claim 2 , wherein X 7 is CH.

4. A compound according to claim 1 , wherein X 7 is N.

5. A compound according to claim 4 , wherein X 6 is CH.

6. A compound according to claim 1 , wherein R 3 is CO 2 R.

7. A compound according to claim 6 , wherein R is —C(CH 3 ) 3 .

8. A compound according to claim 1 , wherein R 3 is OR 1 .

9. A compound according to claim 8 , wherein R 1 is —CH 2 CH 2 CH 3 .

10. A compound according to claim 1 , wherein X 4 is CH, X 5 is CH, X 6 is N, X 7 is CH, X 9 is CH, X 9 is NH, and R 1 is —CO 2 C(CH 3 ) 3 .

11. A compound according to claim 1 , wherein X 4 is CH, X 5 is CH, X 6 is N, X 7 is CH, X 9 is CH, X 9 is NH, and R 1 is —OCH 2 CH 2 CH 3 .

12. A compound according to claim 1 , wherein X 4 is CH, X 5 is CH, X 6 is CH, X 7 is N, X 9 is CH, X 9 is NH, and R 1 is —CO 2 C(CH 3 ) 3 .

13. A compound according to claim 1 , wherein X 4 is CH, X 5 is CH, X 6 is CH, X 7 is N, X 9 is CH, X 9 is NH, and R 1 is —OCH 2 CH 2 CH 3 .

14. A pharmaceutical composition comprising a compound according to claim 1 and a carrier.

15. The composition according to claim 14 , further comprising an additional active agent.

16. The composition according to claim 15 , wherein the additional active agent is an anxiolytic.

17. The composition according to claim 15 , wherein the additional active agent treats a chemical addiction.

18. The composition according to claim 15 , wherein the additional active agent is selected from the group consisting of diazepam, clonazepam, clorazepate, alprazolam, buspirone, meprobamate, naltrexone, naltrexone hydrochloride, disulfuram, nalmefene, metadoxine, acamposate calcium, and chlordiazepoxide hydrochloride.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jan 6, 2015
From: UNIVERSITY OF WISCONSIN MILWAUKEE
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 034726/0523 →
CONFIRMATORY LICENSE Recorded Feb 12, 2010
From: UNIVERSITY OF WISCONSIN MILWAUKEE
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 023927/0917 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2009
From: COOK, JAMES M.; VAN LINN, MICHAEL L.; YIN, WENYUAN
To: THE UWM RESEARCH FOUNDATION, INC.
Reel/Frame 022829/0102 →
Continuity (2)
Provisional Application 61055334 · May 22, 2008
Related Publication 20090306121A1 · Dec 10, 2009