IP Library Granted Patent US 8,439,252
Granted Patent B2
US 8,439,252 · App. 12/513,784 · Granted May 14, 2013

Method for bonding metal surfaces, method for producing an object having cavities, object having cavities, structure of a light emitting diode

Inventors: Ulrich Traupe (Wiesbaden, DE); Stefan Weise (Hohenstein, DE); Pellegrino Ballacchino (Wiesbaden, DE); Edgar Spandl (Hunfelden, DE)
Assignee: Excelitas Technologies GmbH & Co KG
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Quick Facts
Patent No.
US 8,439,252
App. No.
12/513,784
Granted
May 14, 2013
Kind
B2
Abstract

A method for bonding two partially form-fitting surfaces of two metal bodies which contain the same metal is carried out by generating a first layer on the surface of a first one of the two bodies, the first layer containing a mixture of the metal and the oxide of the metal; generating a second layer on the first layer, the second layer containing the metal but less oxide of the metal than does the first layer; placing the partially form-fitting surfaces of the two metal bodies adjacent to each other; heating the bodies placed adjacent to each other to a temperature which lies in a target range below the melting point of the metal and above the eutectic temperature of the eutectic of the metal and the metal oxide; and holding the temperature within the target range over a predetermined or a controllable duration of time.

Claims (34)

1. Method for bonding two partially form-fitting surfaces of two metal bodies which comprise the same metal, comprising the steps of:

(a) generating a first layer on the partially form-fitting surface of a first one of the two bodies, the first layer comprising a mixture of the metal and the oxide of the metal;

(b) generating a second layer on the first layer, the second layer comprising the metal but less oxide of the metal than does the first layer;

(c) placing the partially form-fitting surfaces of the two metal bodies adjacent to each other;

(d) heating the bodies placed adjacent to each other to a temperature which lies in a target range below the melting point of the metal and above a eutectic temperature of a eutectic of the metal and the metal oxide; and

(e) holding the temperature within the target range over a predetermined or a controllable duration of time two bond the two partially form-fitting surfaces of the two metal bodies together.

2. The method according to claim 1 , characterized in that (f) before step (c) a first layer is also generated on the second body.

3. Method according to claim 2 , characterized in that (g) after step (f) and before step (c) a second layer is also generated on the first layer of the second body.

4. Method according to claim 1 characterized in that the first layer is generated by oxidizing the material of the metal body.

5. Method according to claim 1 , characterized in that the first layer is generated by applying the metal of the metal body in the form of fine particles on the surface thereof in an oxygen-containing atmosphere.

6. Method according to claim 5 , characterized in that the application of the metal is a vacuum deposition process or a sputtering process.

7. Method according to claim 5 , characterized in that the application is performed at room temperature.

8. Method according to claim 1 , characterized in that the first layer is generated in such a way that before step (d) it comprises a hypereutectic proportion of oxygen.

9. Method according to claim 1 , characterized in that the metal comprises at least 90% by weight of copper.

10. Method according to claim 1 , characterized in that the second layer is generated by applying the metal of the metal body in the form of fine particles on the surface thereof in an inert atmosphere.

11. Method according to claim 1 , characterized in that in step (d) and/or in step (e) the bodies are pressed together at least temporarily.

12. Method according to claim 1 , wherein in step (d) the heating is performed in accordance with a predetermined temperature variation over time.

13. Method according to claim 1 , characterized in that plate-shaped or foil-shaped bodies are used which can have recesses.

14. Method according to claim 13 , wherein the plates have a thickness of below 2 mm.

15. Method according to claim 1 , wherein the second layer is generated in such a way that its proportion of oxide is less than 10% of that of the first layer.

16. Method according to claim 1 , wherein at least one of the two metal bodies comprises a Cu—Al alloy wherein Al is provided in a proportion of more than 0.02% by weight or more than 0.1% by weight and/or less than 1% by weight or less than 0.2% by weight, the remainder being essentially copper.

17. Method according to claim 16 , wherein the Al is dispersed in the Cu in the shape of aluminum oxide particles.

18. Method according to claim 16 , wherein during steps (d) and/or (e) pressure is exerted at least temporarily on the bodies superimposed on each other.

19. Method according to claim 18 , wherein the pressure is exerted for at least 2 or at least 5 minutes and/or for at most 50 minutes or at most 30 minutes.

20. Method according to claim 18 , wherein the heating to a target temperature is performed wherein the target temperature is below a melting point of the eutectic of copper and copper oxide without pressure load.

21. Method for bonding partially form-fitting surfaces of a plurality of metal bodies which comprise the same metal, comprising the steps of:

(a) generating a first layer on the partially form-fitting surface of a first metal body, the first layer comprising a mixture of the metal and the oxide of the metal;

(b) generating a second layer on the first layer, the second layer comprising the metal but less oxide of the metal than does the first layer;

(c) placing the partially form-fitting surfaces of the first metal body and a second metal body adjacent to each other;

(d) heating the metal bodies placed adjacent to each other to a temperature which lies in a target range below the melting point of the metal and above a eutectic temperature of a eutectic of the metal and the metal oxide; and

(e) holding the temperature within the target range over a predetermined or a controllable duration of time to bond the plurality of partially form-fitting surfaces of the plurality of metal bodies together.

22. Method according to claim 21 , characterized in that three or more bodies are bonded to each other at the same time by preparing for each interface at least one of the surfaces according to steps (a) and (b) and, subsequently, performing steps (c) to (e) for all bodies together.

23. Method for producing an object with cavities therein, wherein the object is produced by bonding plate-shaped bodies forming individual layers of the object and being designed according to the desired cavities, characterized in that at least two bodies are bonded to each other by a method according to claim 21 .

24. Method according to claim 23 , wherein three or more bodies are simultaneously pressurized as a stack during heating and one or more compensation openings are provided in one or more bodies.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 20, 2012
From: PERKINELMER TECHNOLOGIES GMBH & CO KG
To: EXCELITAS TECHNOLOGIES GMBH & CO KG
Reel/Frame 028080/0453 →
CHANGE OF NAME Recorded Oct 13, 2010
From: PERKINELMER OPTOELECTRONICS GMBH & CO. KG
To: PERKINELMER TECHNOLOGIES GMBH & CO. KG
Reel/Frame 025135/0085 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2010
From: TRAUPE, ULRICH; WEISE, STEFAN; BALLACCHINO, PELLEGRINO; SPANDL, EDGAR
To: PERKIN ELMER OPTOELECTRONICS GMBH & CO. KG
Reel/Frame 024046/0629 →
Continuity (2)
Provisional Application 60857140 · Nov 7, 2006
Related Publication 20100187560A1 · Jul 29, 2010