IP Library Granted Patent US 8,591,677
Granted Patent B2
US 8,591,677 · App. 12/612,675 · Granted Nov 26, 2013

Utility materials incorporating a microparticle matrix formed with a setting agent

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Quick Facts
Patent No.
US 8,591,677
App. No.
12/612,675
Granted
Nov 26, 2013
Kind
B2
Abstract

A composition, utility material, and method of making a utility material is disclosed. A composition having an improved setting time may include a plurality of microparticles mixed with a sodium silicate binder and an isocyanate setting agent, where the microparticle composition has a setting time of less than or equal to one hour. A utility material may be a wallboard that includes the composition.

Claims (26)

1. A method of making a utility material comprising:

providing a wallboard having a first facing membrane and a second facing membrane;

forming a core matrix including a mixture of:

a plurality of microparticles,

wherein the microparticles are cenospheres having an outer shell and a hollow interior filled with a gas, and

wherein the microparticles have a crush strength between 3000 psi and 5000 psi,

a sodium silicate binder, and

an isocyanate setting agent;

disposing the core matrix between the first facing membrane and the second facing membrane of the wallboard,

wherein the outer shell of the microparticles excludes the sodium silicate binder and the isocyanate setting agent from the hollow interior of the plurality of microparticles;

setting the core matrix to form a set core matrix; and

making the utility material.

2. The method of claim 1 , wherein forming the core matrix further comprises:

forming a first mixture including a first portion of the plurality of microparticles and the sodium silicate binder;

forming a second mixture including a second portion of the plurality of microparticles and the isocyanate setting agent; and

mixing the first mixture with the second mixture to form the core matrix mixture.

3. The method of claim 1 , further comprising coating a contact surface of one of the first facing membrane and the second facing membrane with a sodium silicate coating prior to disposing the core matrix mixture therebetween.

4. The method of claim 1 , wherein the plurality of microparticles is from about 25 wt % to about 75 wt % of wet core matrix mixture, wherein the sodium silicate is from about 20 wt % to about 60 wt % of wet core matrix mixture, and wherein the isocyanate setting agent is from about 2 wt % to about 10 wt % of wet core matrix mixture.

5. The method of claim 1 , wherein the core matrix mixture includes the sodium silicate binder and the isocyanate setting agent at a ratio of from about 1:1 to about 15:1.

6. The method of claim 1 , wherein the core matrix mixture includes the sodium silicate binder and the isocyanate setting agent at a ratio of from about 8:1 to about 12:1.

7. The method of claim 1 , wherein setting time of the core matrix mixture is less than or equal to 30 minutes.

8. The method of claim 1 , wherein setting the core matrix mixture occurs at ambient temperature.

9. The method of claim 1 , further comprising curing the set core matrix mixture.

10. The method of claim 1 , wherein the utility material has a density between 0.4 g/ml and 0.6 g/ml.

11. The method of claim 1 , wherein the isocyanate setting agent is configured to cause the core matrix to set in one hour or less.

12. The method of claim 9 , wherein the curing includes subjecting the core matrix to a temperature ranging from ambient temperature to about 400 degrees F.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2024
From: MICROSPHERE LABS LLC
To: SPHERIC INVESTORS LLC
Reel/Frame 068152/0941 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2024
From: SPHERIC INVESTORS LLC
To: AKAMAI MATERIALS, INC.
Reel/Frame 068324/0534 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 18, 2022
From: ASHTECH INDUSTRIES, LLC
To: MICROSPHERE LABS LLC
Reel/Frame 061455/0531 →
SECURITY INTEREST Recorded May 9, 2018
From: ASHTECH INNOVATION AND RESEARCH INC.; ASHTECH INDUSTRIES LLC
To: KDL INVESTMENTS, LLC
Reel/Frame 045753/0654 →
SECURITY INTEREST Recorded Sep 18, 2017
From: ASHTECH INNOVATION AND RESEARCH INC.; ASHTECH INDUSTRIES LLC
To: KDL INVESTMENTS, LLC
Reel/Frame 043894/0282 →
SECURITY INTEREST Recorded Aug 6, 2014
From: ASHTECH INNOVATION AND RESEARCH INC.; ASHTECH INDUSTRIES LLC
To: KDL INVESTMENTS, LLC
Reel/Frame 033481/0710 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 20, 2010
From: KIPP, MICHAEL D.; PUGH, DILWORTH L.; RIDGES, MICHAEL D.; MCCARVILL, WILLIAM T.
To: ASHTECH INDUSTRIES, LLC
Reel/Frame 023819/0506 →