IP Library Granted Patent US 8,735,174
Granted Patent B2
US 8,735,174 · App. 12/670,194 · Granted May 27, 2014

Coated colloidal materials

Inventors: Chad A. Mirkin (Wilmette, IL); Xiaodong Chen (Singapore, SG); Can Xue (Singapore, SG); Sarah J. Hurst (Chicago, IL)
Assignee: Northwestern University
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Quick Facts
Patent No.
US 8,735,174
App. No.
12/670,194
Granted
May 27, 2014
Kind
B2
Abstract

Coated colloidal materials, methods for making coated colloidal materials, and methods of using coated colloidal materials are disclosed. The method yields coated colloidal materials where the optical characteristics of the core is not adversely affected. The coated colloidal materials can be self-assembled into films, layers, or structures and used in the detection of analytes through detection assays.

Claims (12)

1. A coated colloidal material comprising (a) a colloidal material having a passivated surface; (b) a coating comprising at least one of a silicate or a titania on the passivated surface; and (c) a functionalizing agent on the coating, wherein the colloidal material comprises a nanoprism and the functionalizing agent is selected from the group consisting of an oligonucleotide, a polypeptide, a protein, an antibody, a peptide, an anticancer agent, a polynucleotide-binding agent, a carbohydrate, a lipid, a cell-surface receptor-binding agent, and mixtures thereof.

2. The coated colloidal material of claim 1 , wherein the colloidal material comprises gold or silver.

3. The coated colloidal material of claim 1 , wherein the functionalizing agent comprises at least one functional group and a first functional group is selected from the group consisting of a halo, an alkoxy, a carboxylic acid, an ester, a thiol, a selenide, an amine, an amide, a phosphate, a phosphite, a phosphonate, an alkene, an alkyne, a silane, a siloxane, a borane, and mixtures thereof.

4. An organized material comprising a monolayer of the coated colloidal material of claim 1 , wherein the coated colloidal material is deposited on the substrate by the Langmuir-Blodgett technique.

5. A method of detecting an analyte in a sample comprising:

contacting the sample with a coated colloidal material of claim 1 under conditions sufficient to permit an interaction of the analyte and the coated colloidal material, and

detecting the interaction, wherein the interaction of the analyte and the coated colloidal material produces a detection event.

6. The method of claim 5 , wherein the functionalizing agent comprises an oligonucleotide, the analyte comprises a complementary oligonucleotide or a oligonucleotide-binding moiety, and the detection event comprises a change in melting temperature of the oligonucleotide.

7. A coated colloidal material prepared by a method comprising:

admixing a colloidal material, a surface passivating agent, and a coating agent in the presence of an optional catalyst, wherein the colloidal material comprises a nanoprism and the surface passivating agent comprises a thiol,

the colloidal material comprising a functionalizing agent on a coating, said coating prepared from the coating agent,

wherein the functionalizing agent is selected from the group consisting of decyl(trimethoxy)silane, decyl(triethoxy)silane, dodecyl(triethoxy)silane, hexadecyl(trimethoxy)silane, octadecyl(trimethoxy)silane, and mixtures thereof.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 25, 2010
From: NORTHWESTERN UNIVERSITY
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA OFFICE OF NAVAL RESEARCH
Reel/Frame 024884/0380 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2010
From: MIRKIN, CHAD A.; XUE, CAN; CHEN, XIAODONG; HURST, SARAH J.
To: NORTHWESTERN UNIVERSITY
Reel/Frame 023912/0863 →
Continuity (2)
Provisional Application 60951620 · Jul 24, 2007
Related Publication 20100291697A1 · Nov 18, 2010