IP Library Granted Patent US 8,324,258
Granted Patent B2
US 8,324,258 · App. 12/677,598 · Granted Dec 4, 2012

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Assignee: The Regents of the University of Michigan
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Quick Facts
Patent No.
US 8,324,258
App. No.
12/677,598
Granted
Dec 4, 2012
Kind
B2
Abstract

The present invention relates to a family of guanidine-based F1F0-ATPase inhibitors, e.g., mitochondrial F1F0-ATPase inhibitors, methods for their discovery, and their use as therapeutic agents for treating certain disorders.

Claims (38)

1. A compound represented by Formula I:

including salts and esters thereof, wherein,

R 1 is imidazolidonyl or a heteroaryl containing at least 1 ring nitrogen atom;

R 2 and R 3 represent independently for each occurrence hydrogen or (C 1 -C 4 )alkyl;

R 4 is

R 5 represents independently for each occurrence hydrogen, halogen, alkyl, haloalkyl, aryl, heteroaryl, —NO 2 , —CN, —C(O)aryl, —C(O)heteroaryl, —C(O)N(R 2 )aryl, or —C(O)N(R 2 )heteroaryl;

R 6 represents independently for each occurrence hydrogen, halogen, alkyl, haloalkyl, alkoxy, aryl, heteroaryl, —NO 2 , —CN, —SO 2 alkyl, or —SO 2 N(alkyl) 2 ;

n is 0, 1, 2, 3, or 4;

m represents independently for each occurrence 1 or 2; and

the stereochemical configuration at a stereocenter in a compound represented by Formula I is R, S, or a mixture thereof.

2. The compound of claim 1 , wherein R 1 is

3. The compound of claim 1 , wherein R 1 is

4. The compound of claim 1 , wherein n is 2, and R 2 and R 3 are hydrogen.

5. The compound of claim 1 , wherein R 4 is

6. The compound of claim 1 , wherein R 6 is

and R 7 represents independently for each occurrence hydrogen, halogen, alkyl, alkoxy, or —CN.

7. The compound of claim 1 , wherein R 5 represents independently for each occurrence halogen, alkyl, haloalkyl, —NO 2 , or —CN.

8. The compound of claim 1 , wherein m is 1.

9. The compound of claim 1 , wherein R 1 is

n is 2, R 2 and R 3 are

hydrogen, and R 4 is

10. The compound of claim 1 , wherein R 1 is

n is 2, R 2 and R 3 are hydrogen, R 4 is

R 5 is halogen, alkyl, haloalkyl, —NO 2 , or —CN, and m is 1.

11. The compound of claim 1 , wherein the compound is one of the following:

12. A pharmaceutical composition comprising a compound of claim 1 and a pharmaceutically acceptable carrier.

13. The compound of claim 1 , wherein the compound has the following formula:

including salts thereof, wherein,

R 1 is a heteroaryl containing at least 1 ring nitrogen atom;

R 2 and R 3 represent independently for each occurrence hydrogen or (C 1 -C 4 )alkyl;

R 4 is

R 5 represents independently for each occurrence hydrogen, halogen, alkyl, haloalkyl, aryl, heteroaryl, —NO 2 , —CN, —C(O)aryl, —C(O)heteroaryl, —C(O)N(R 2 )aryl, or —C(O)N(R 2 )heteroaryl;

R 6 represents independently for each occurrence hydrogen, halogen, alkyl, haloalkyl, alkoxy, aryl, heteroaryl, —NO 2 , —CN, —SO 2 alkyl, or —SO 2 N(alkyl) 2 ;

n is 0, 1, 2, 3, or 4;

m represents independently for each occurrence 1 or 2; and

the stereochemical configuration at a stereocenter in a compound represented by said formula is R, S, or a mixture thereof.

14. The compound of claim 13 , wherein R 5 represents independently for each occurrence halogen, alkyl, or haloalkyl.

15. The compound of claim 14 , wherein R 6 represents independently for each occurrence halogen, alkyl, or haloalkyl.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2010
From: GLICK, GARY D.; NEY, GINA
To: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
Reel/Frame 024122/0048 →
CONFIRMATORY LICENSE Recorded Mar 17, 2010
From: UNIVERSITY OF MICHIGAN
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 024094/0545 →
Continuity (2)
Provisional Application 60972553 · Sep 14, 2007
Related Publication 20100222400A1 · Sep 2, 2010