Method for constant concentration evaporation and a device using the same
Disclosed herein is a device comprising an evaporator; and a heat exchanger; the heat exchanger being in fluid communication with evaporator; evaporator comprising an outer casing; and an inner casing that is disposed within the outer casing; the inner casing contacting a plate; wherein the inner casing encloses a first conduit that is operative to introduce a carrier fluid into evaporator; and a second conduit that is operative to remove carrier fluid entrained with a precursor; wherein the outer casing is detachably attached to the plate; the plate contacting a first precursor conduit that is operative to introduce the precursor into evaporator from the heat exchanger; where the heat exchanger is disposed proximate to evaporator at a distance effective to maintain the precursor in evaporator at a substantially constant temperature when the ambient temperature around the heat exchanger and evaporator fluctuates by an amount of up to about ±35° C.
1. A device comprising:
an evaporator; and
a heat exchanger; the heat exchanger being in fluid communication with the evaporator;
the evaporator comprising:
an outer casing; and
an inner casing that is disposed within the outer casing; the inner casing contacting a plate; wherein the inner casing encloses:
a first conduit that is operative to introduce a carrier fluid into the evaporator;
wherein the first conduit is an inverted U-shaped conduit that has one end in fluid communication with a first port for introducing the carrier fluid into the evaporator and an opposing end in fluid communication with a sparger; and
a second conduit that is operative to remove the carrier fluid entrained with a precursor; wherein the outer casing is detachably attached to the plate; the plate contacting a first precursor conduit that is operative to introduce the precursor into the evaporator from the heat exchanger; where the heat exchanger is disposed proximate to the evaporator at a distance effective to maintain the precursor in the evaporator at a substantially constant temperature when the ambient temperature around the heat exchanger and the evaporator fluctuates by an amount of up to about ±35° C.
2. The device of claim 1 , wherein the second conduit is an inverted J-shaped conduit that has one end in fluid communication with a second port for removing the carrier fluid entrained with a precursor from the evaporator and an opposing end in fluid communication with a splash shield.
3. The device of claim 1 , wherein the proximity of the heat exchanger to the evaporator is effective to maintain a ratio of the carrier fluid to the precursor that does not change by an amount of greater than or equal to about 0.5% when the ambient temperature around the heat exchanger and the evaporator fluctuates by an amount of up to about ±35° C.
4. The device of claim 1 , wherein the proximity of the heat exchanger to the evaporator is effective to maintain a variation in temperature of the precursor in a fluid path from the heat exchanger to the evaporator to be less than or equal to about ±0.1° C.
5. The device of claim 1 , wherein the inverted U-shaped conduit is disposed in the evaporator via a hole in the plate.
6. The device of claim 2 , wherein the inverted J-shaped conduit is disposed in the evaporator via a hole in the plate.
7. A method comprising:
heating or cooling a precursor in a heat exchanger;
discharging the precursor from the heat exchanger to an evaporator; the evaporator comprising:
an outer casing; and
an inner casing that is disposed within the outer casing; the inner casing contacting a plate; wherein the inner casing encloses:
a first conduit; wherein the first conduit is an inverted U-shaped conduit that has one end in fluid communication with a first port for introducing a carrier fluid into the evaporator and an opposing end in fluid communication with a sparger; and
a second conduit; wherein the second conduit is an inverted J-shaped conduit that has one end in fluid communication with a second port for removing the carrier fluid entrained with a precursor from the evaporator and an opposing end in fluid communication with a splash shield;
introducing a carrier fluid into the evaporator via the first conduit;
sparging the precursor with the carrier fluid; and
removing the carrier fluid entrained with the precursor from the evaporator via the second conduit; where the proximity of the heat exchanger to the evaporator is effective to maintain the precursor in the evaporator at a substantially constant temperature when the ambient temperature around the heat exchanger and the evaporator fluctuates by an amount of up to about ±35° C.
8. The method of claim 7 , further comprising circulating a fluid in a space between the outer casing and the inner casing.
9. A method for manufacturing a device comprising:
disposing an inverted U-shaped conduit in a first hole, an inverted J-shaped conduit in a second hole and a first precursor conduit in a third hole on a plate; the plate being affixed with a heat exchanger; and
disposing an inner casing and an outer casing on a side of the plate that is opposed to a side where the heat exchanger contacts the plate; the inner casing being contained in the outer casing; the inner casing enclosing the inverted U-shaped conduit, the inverted J-shaped conduit and the first precursor conduit.
10. A device comprising:
an evaporator; and
a heat exchanger; the heat exchanger being in fluid communication with the evaporator;
the evaporator comprising:
an outer casing; and
an inner casing that is disposed within the outer casing; the inner casing contacting a plate; wherein the inner casing encloses:
a first conduit that is operative to introduce a carrier fluid into the evaporator; and
a second conduit that is operative to remove the carrier fluid entrained with a precursor; wherein the outer casing is detachably attached to the plate; the plate contacting a first precursor conduit that is operative to introduce the precursor into the evaporator from the heat exchanger; where the heat exchanger is disposed proximate to the evaporator at a distance effective to maintain the precursor in the evaporator at a substantially constant temperature when the ambient temperature around the heat exchanger and the evaporator fluctuates by an amount of up to about ±35° C.; wherein the second conduit is an inverted J-shaped conduit that has one end in fluid communication with a second port for removing the carrier fluid entrained with a precursor from the evaporator and an opposing end in fluid communication with a splash shield.
11. The device of claim 10 , wherein the first conduit is an inverted U-shaped conduit that has one end in fluid communication with a first port for introducing the carrier fluid into the evaporator and an opposing end in fluid communication with a sparger.
12. The device of claim 10 , wherein the proximity of the heat exchanger to the evaporator is effective to maintain a ratio of the carrier fluid to the precursor that does not change by an amount of greater than or equal to about 0.5% when the ambient temperature around the heat exchanger and the evaporator fluctuates by an amount of up to about ±35° C.
13. The device of claim 10 , wherein the proximity of the heat exchanger to the evaporator is effective to maintain a variation in temperature of the precursor in a fluid path from the heat exchanger to the evaporator to be less than or equal to about ±0.1° C.
14. The device of claim 10 , wherein the first conduit is an inverted U-shaped conduit is disposed in the evaporator via a hole in the plate.
15. The device of claim 10 , wherein the inverted J-shaped conduit is disposed in the evaporator via a hole in the plate.