IP Library Granted Patent US 9,254,606
Granted Patent B2
US 9,254,606 · App. 12/690,558 · Granted Feb 9, 2016

Nanoscale fiber films, composites, and methods for alignment of nanoscale fibers by mechanical stretching

Inventors: Jianwen Bao (Beijing, CN); Zhiyong Liang (Tallahassee, FL); Ben Wang (Tallahassee, FL); Chun Zhang (Tallahassee, FL); Qunfeng Cheng (Tallahassee, FL)
Assignee: FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION
B29C55/04B29C70/14B29K2105/162B29K2105/167B29K2105/243Y10T156/1002Y10T428/25
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Quick Facts
Patent No.
US 9,254,606
App. No.
12/690,558
Granted
Feb 9, 2016
Kind
B2
Abstract

Methods for aligning nanoscale fibers are provided. One method comprises providing a network of nanoscale fibers and mechanically stretching the network of nanoscale fibers in a first direction. The network of nanoscale fibers is substantially devoid of a liquid. A network of aligned nanoscale fibers and a composite comprising a network of aligned nanoscale fibers are also provided.

Claims (18)

1. A method for aligning nanoscale fibers, the method comprising:

providing a network of nanoscale fibers, wherein the network of nanoscale fibers is a buckypaper that is substantially devoid of a liquid, and comprises carbon nanotubes that are randomly oriented;

providing a supporting medium on or in the network of nanoscale fibers; and

mechanically stretching the network of nanoscale fibers and the supporting medium in a first direction.

2. The method of claim 1 , wherein the nanoscale fibers are carbon nanotubes having an average length of at least 1 millimeter.

3. A method for aligning carbon nanotubes or other nanoscale fibers comprising:

providing a network of nanoscale fibers, wherein the network of nanoscale fibers is a buckypaper comprising carbon nanotubes that are randomly oriented;

providing a supporting medium on or in the network of nanoscale fibers; and

mechanically stretching the network of nanoscale fibers and the supporting medium in a first direction.

4. The method of claim 3 , wherein the supporting medium comprises a flexible thermoplastic material.

5. The method of claim 4 , wherein the flexible thermoplastic material comprises a polyethylene film.

6. The method of claim 3 , further comprising, after the stretching, removing the supporting medium from the network of nanoscale fibers.

7. The method of claim 6 , wherein the removing comprises thermally decomposing the supporting medium.

8. The method of claim 7 , further comprising annealing the supporting medium before the thermally decomposing.

9. The method of claim 1 , wherein the mechanically stretching is a continuous process.

10. The method of claim 3 , wherein the mechanically stretching is a continuous process.

11. The method of claim 1 , wherein the supporting medium comprises a flexible thermoplastic material.

12. The method of claim 11 , wherein the flexible thermoplastic material comprises a polyethylene film.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 3, 2010
From: FLORIDA STATE UNIVERSITY
To: AIR FORCE, UNITED STATES
Reel/Frame 024028/0485 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 2, 2010
From: BAO, JIANWEN; LIANG, ZHIYONG; WANG, BEN; ZHANG, CHUN; CHENG, QUNFENG
To: FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION
Reel/Frame 024010/0345 →
Continuity (2)
Provisional Application 61145849 · Jan 20, 2009
Related Publication 20100227155A1 · Sep 9, 2010