IP Library Granted Patent US 9,034,108
Granted Patent B2
US 9,034,108 · App. 12/736,446 · Granted May 19, 2015

Cleaning compositions for use in closed loop cleaning machines

Inventors: Konrad Geissler (Zurich, CH); Marius Kuemin (Huenenberg, CH)
Assignee: Dow Global Technologies LLC
B08B3/08B08B3/14C11D7/263C11D7/5022D06F43/007D06L1/02D06L1/10
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Quick Facts
Patent No.
US 9,034,108
App. No.
12/736,446
Granted
May 19, 2015
Kind
B2
Abstract

Embodiments of the present disclosure include cleaning processes, closed loop cleaning machines, and methods of cleaning an article. The cleaning process includes contacting a surface of an article with a cleaning composition in a cleaning chamber, where the cleaning composition includes at least about 85 percent by weight organic solvents, based on total weight of the cleaning composition, and where at least about 5 percent by weight of the organic solvents is propylene glycol, based on total weight of the organic solvents, to clean the surface of the article, collecting the cleaning composition including contaminants, and recovering the cleaning composition via distillation, where a distillation apparatus removes the contaminants from the cleaning composition and is connected to the cleaning chamber by a process stream.

Claims (22)

1. A closed loop cleaning process, comprising:

loading an article to be cleaned into a cleaning chamber;

closing the cleaning chamber;

vaporizing a non-aqueous cleaning composition into a non-aqueous cleaning composition vapor, where the non-aqueous cleaning composition includes at least about 85 percent by weight organic solvents, based on total weight of the non-aqueous cleaning composition, and where at least about 5 percent by weight of the organic solvents is propylene glycol, based on total weight of the organic solvents;

directing the non-aqueous cleaning composition vapor into the cleaning chamber;

condensing the non-aqueous cleaning composition vapor into a liquid on a surface of the article, to clean the surface of the article;

collecting the non-aqueous cleaning composition including contaminants from the article;

recovering the non-aqueous cleaning composition via distillation from contaminants in the non-aqueous cleaning composition, where a distillation apparatus removes the contaminants from the non-aqueous cleaning composition; and

recycling, by a process stream in the closed loop cleaning process, the non-aqueous cleaning composition recovered via distillation back to the closed cleaning chamber.

2. The closed loop cleaning process of claim 1 , including flowing the recycled non-aqueous cleaning composition to a storage tank connected to the cleaning chamber.

3. The closed loop cleaning process of claim 1 , where the organic solvents in the non-aqueous cleaning composition include propylene glycol in a range of about 5 percent by weight to about 99 percent by weight, based on total weight of the organic solvents.

4. The closed loop cleaning process of claim 1 , where the organic solvents in the non-aqueous cleaning composition include propylene glycol in a range of about 15 percent by weight to about 35 percent by weight, based on total weight of the organic solvents.

5. A method of cleaning an article in a closed loop cleaning machine, comprising:

loading the article including soils on an article surface, where the soils are to be removed, into a cleaning chamber;

closing the cleaning chamber;

vaporizing a non-aqueous cleaning composition into a non-aqueous cleaning composition vapor, where the non-aqueous cleaning composition includes at least about 85 percent by weight organic solvents, based on total weight of the non-aqueous cleaning composition, and where at least about 5 percent by weight of the organic solvents is propylene glycol, based on total weight of the organic solvents;

directing the non-aqueous cleaning composition vapor into the cleaning chamber;

condensing the non-aqueous cleaning composition vapor into a liquid on the article surface to remove the soils;

collecting the non-aqueous cleaning composition including the soils from the article;

distilling the non-aqueous cleaning composition, including the soils, to separate the non-aqueous cleaning composition from the soils; and

recycling, by a process stream in the closed loop cleaning process, the non-aqueous cleaning composition recovered via distillation back to the closed cleaning chamber.

6. The method of claim 5 , where the soils on the article surface have a polarity and the non-aqueous cleaning composition has a polarity, and where the method includes dissolving the soils on the article surface by adjusting the amount of propylene glycol included in the organic solvents of the non-aqueous cleaning composition up to 99 percent by weight based on the total weight of the organic solvents.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 27, 2017
From: THE DOW CHEMICAL COMPANY
To: SAFECHEM EUROPE GMBH
Reel/Frame 041105/0104 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2011
From: GEISSLER, KONRAD; KUEMIN, MARIUS
To: DOW EUROPE GMBH
Reel/Frame 026187/0933 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2011
From: DOW EUROPE GMBH
To: THE DOW CHEMICAL COMPANY
Reel/Frame 026188/0117 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2011
From: THE DOW CHEMICAL COMPANY
To: DOW GLOBAL TECHNOLOGIES INC.
Reel/Frame 026188/0196 →
CHANGE OF NAME Recorded Apr 27, 2011
From: DOW GLOBAL TECHNOLOGIES INC.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 026188/0667 →
Continuity (2)
Provisional Application 61123538 · Apr 9, 2008
Related Publication 20110088722A1 · Apr 21, 2011