IP Library Granted Patent US 8,431,569
Granted Patent B2
US 8,431,569 · App. 12/747,030 · Granted Apr 30, 2013

Inhibitors of janus kinases

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,431,569
App. No.
12/747,030
Granted
Apr 30, 2013
Kind
B2
Abstract

The instant invention provides for compounds that inhibit the four known mammalian JAK kinases (JAK1, JAK2, JAK3 and TYK2) and PDK1. The invention also provides for compositions comprising such inhibitory compounds and methods of inhibiting the activity of JAK1, JAK2, JAK3 TYK2 and PDK1 by administering the compound to a patient in need of treatment for myeloproliferative disorders or cancer.

Claims (57)

1. A compound of formula I:

wherein R 1 is hydrogen, C 1-6 alkyl, C 2-6 alkenyl, C 3-8 cycloalkyl, C 1-6 haloalkyl, heteroaryl or a carbonyl, wherein said alkyl and cycloalkyl groups are optionally substituted with one to four substituents selected from the group consisting of halo, C 1-3 alkyl and hydroxy;

R 2 is cyclopropyl;

R 3 is hydrogen, C 1-3 alkyl, halo, heteroaryl or heterocyclyl, wherein said alkyl group is optionally substituted with heteroaryl, and said heteroaryl and heterocyclyl groups are optionally substituted on either the carbon or the heteroatom with C 1-3 alkyl, halo, NR 4 R 5 or heterocyclyl;

R 3′ is hydrogen, C 1-3 alkyl, halo, hydroxyl, heteroaryl or heterocyclyl, wherein said alkyl group is optionally substituted with heteroaryl, and said heteroaryl and heterocyclyl groups are optionally substituted on either the carbon or the heteroatom with C 1-3 alkyl, halo, NR 4 R 5 or heterocyclyl;

R 4 is hydrogen or C 1-6 alkyl;

R 5 is hydrogen or C 1-6 alkyl;

or a pharmaceutically acceptable salt or stereoisomer thereof.

2. The compound of claim 1 wherein R 3′ is hydrogen.

3. The compound of claim 2 wherein R 3 is heteroaryl, wherein said heteroaryl is optionally substituted on either the carbon or the heteroatom with C 1-3 alkyl, NR 4 R 5 or heterocyclyl; or a pharmaceutically acceptable salt or stereoisomer thereof.

4. The compound of claim 3 wherein the heteroaryl group is selected from the group consisting of pyrimidine, pyrazole, pyridazine, pyridine and triazole; wherein said groups are optionally substituted on either the carbon or the heteroatom with CH 3 , NH 2 or heterocyclyl;

or a pharmaceutically acceptable salt or stereoisomer thereof.

5. The compound of claim 4 wherein R 1 is C 3-4 cycloalkyl or C 1-6 haloalkyl, or a pharmaceutically acceptable salt or stereoisomer thereof.

6. The compound of claim 5 wherein R 1 is trifluoromethyl or cyclopropyl, or a pharmaceutically acceptable salt or stereoisomer thereof.

7. The compound of claim 1 selected from:

7-(2-Aminopyrimidin-5-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

7-Chloro-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-aminopyrimidin-5-yl)-1-[(1-cyclopropyl-2,2-difluoroethyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-2,2,2-trifluoroethyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-2,2,2-trifluoroethyl)amino]-7-(1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-aminopyrimidin-5-yl)-1-[(1-cyclopropyl-2,2,2-trifluoroethyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-7-(1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-Aminopyrimidin-5-yl)-1-[(dicyclopropylmethyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

7-chloro-1-{[(1S)-1-cyclopropylethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-aminopyrimidin-5-yl)-1-[(1-cyclopropylethyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-aminopyrimidin-5-yl)-1-{[(1S)-1-cyclopropylethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylethyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1R)-1-cyclopropylethyl]amino}-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1S)-1-cyclopropylethyl]amino}-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylethyl)amino]-7-(1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1S)-1-cyclopropylethyl]amino}-7-(1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylethyl)amino]-7-pyridin-3-yl-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylprop-2-en-1-yl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylpropyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-2-methylprop-2-en-1-yl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-2-methylpropyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(dicyclopropylmethyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(dicyclopropylmethyl)amino]-7-(1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(5-aminopyrazin-2-yl)-1-[(dicyclopropylmethyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-aminopyrimidin-5-yl)-1-[(1-cyclopropyl-3-hydroxy-3-methylbutyl)amino]-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-3-hydroxy-3-methylbutyl)amino]-7-(1-methyl-1H-pyrazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(Dicyclopropylmethyl)amino]-7-pyridazin-3-yl-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropylethyl)amino]-7-pyridazin-3-yl-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(6-aminopyridin-3-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-7-[6-(1,1-dioxidothiomorpholin-4-yl)pyridazin-3-yl]-5H-pyrido[4,3-b]indole-4-carboxamide;

1-{[(1R)-1-Cyclopropyl-2,2,2-trifluoroethyl]amino}-7-(1H-1,2,3-triazol-4-yl)-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-Cyclopropylethyl)amino]-8-fluoro-5H-pyrido[4,3-b]indole-4-carboxamide;

1-[(1-cyclopropyl-3-hydroxypropyl)amino]-8-fluoro-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-Aminopyrimidin-5-yl)-8-bromo-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-Aminopyrimidin-5-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-8-iodo-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-Aminopyrimidin-5-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-8-methyl-5H-pyrido[4,3-b]indole-4-carboxamide;

7-(2-Aminopyrimidin-5-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-8-hydroxy-5H-pyrido[4,3-b]indole-4-carboxamide;

or a pharmaceutically acceptable salt or stereoisomer thereof.

8. A pharmaceutical composition comprising a pharmaceutically effective amount of the compound according to claim 1 , and a pharmaceutically acceptable carrier.

9. A method of treating myeloproliferative disorders in a mammal in need thereof with a pharmaceutically acceptable amount of a compound according to claim 1 , wherein the myeloproliferative disorder is selected from polycythemia vera (PV), essential thrombocythemia (ET), myeloid metaplasia with myelofibrosis (MMM), chronic myelogenous leukemia (CML), myelomonocytic leukemia (CMML), hypereosinophilic syndrome (HES), juvenile myelomonocytic leukemia (JMML) or systemic mast cell disease (SMCD).

10. A compound which is 7-(2-Aminopyrimidin-5-yl)-1-{[(1R)-1-cyclopropyl-2,2,2-trifluoroethyl]amino}-5H-pyrido[4,3-b]indole-4-carboxamide and pharmaceutically acceptable salts thereof.

Assignments (5)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
CHANGE OF NAME Recorded Aug 29, 2012
From: SCHERING CORPORATION
To: MERCK SHARP & DOHME CORP.
Reel/Frame 028866/0511 →
MERGER Recorded Aug 27, 2012
From: MERCK SHARP & DOHME CORP.
To: SCHERING CORPORATION
Reel/Frame 028850/0515 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2010
From: YOUNG, JONATHAN R.; LIM, JONGWON; MACHACEK, MICHELLE R.; TAOKA, BRANDON MITSUO; OTTE, RYAN D.
To: MERCK & CO., INC.
Reel/Frame 024510/0242 →
CHANGE OF NAME Recorded Jun 9, 2010
From: MERCK & CO., INC.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 024510/0464 →