IP Library Granted Patent US 8,519,159
Granted Patent B2
US 8,519,159 · App. 12/836,878 · Granted Aug 27, 2013

Tri-substituted 2-benzhydryl-5-benzylamino-tetrahydro-pyran-4-OL and 6-benzhydryl-4-benzylamino-tetrahydro-pyran-3-OL analogues, and novel 3,6-disubstituted pyran derivatives

Inventor: Aloke K. Dutta (Novi, MI)
Assignee: Wayne State University
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Quick Facts
Patent No.
US 8,519,159
App. No.
12/836,878
Granted
Aug 27, 2013
Kind
B2
Abstract

3,6-disubstituted pyrans, optionally with a further substituent at the 4-position, are monoamine reuptake inhibitors with activity profiles of anti-depressants.

Claims (44)

1. A 3,6-substituted pyran group-containing compound having the structural formula:

wherein

A, A′, and B are individually selected from the group of optionally substituted C 4 -C 14 aryl and heteroaryl wherein heteroatoms of heteroaryl A and/or A′ are selected from the group consisting of O, N, and S;

Z is selected from the group consisting of a chemical bond and —Y—(CH 2 ) o — wherein Y is NH or O and o is 0, 1, 2, 3, or 4;

R is H or C 1-8 alkyl;

W is selected from the group consisting of hydrogen and —OH wherein when W is hydrogen, B is phenyl or a phenyl substituted with C 1-4 alkyl, C 2-6 alkenyl, C 2-6 optionally halogenated alkynyl, C 2-6 hydroxyalkynyl, COOR′, —OH, or —NH 2 ;

R′ is C 1-18 alkyl, C 5-10 cycloalkyl, or C 2-18 alkenyl;

R 2 is C 1-8 alkyl, C 5-6 cycloalkyl, or C 2-8 alkenyl; and

n and m individually are 0, 1, 2, 3, or 4, and wherein any carbon of —(CH 2 ) n may be substituted by OR 4 wherein R 4 is C 1-8 alkyl, C 2-18 alkylene, or —COOR 5 wherein R 5 is C 1-18 alkyl or C 2-18 alkylene, or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

2. The compound of claim 1 , wherein at least one of A and A′ is an optionally substituted phenyl, napthyl, anthryl, furanyl, thienyl, or pyridinyl group.

3. The compound of claim 1 , wherein W is —OH and B is an optionally substituted phenyl, napthyl, anthryl, furanyl, thienyl, pyridinyl group, or

where X is N, O, or S.

4. The compound of claim 1 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

5. The compound of claim 2 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

6. The compound of claim 3 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

7. The compound of claim 1 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

8. The compound of claim 2 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

9. The compound of claim 3 , having the formula

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

10. The compound of claim 1 , having a formula selected from the group consisting of:

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

11. The compound of claim 2 , having a formula selected from the group consisting of:

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

12. The compound of claim 3 , wherein A and A′ are both unsubstituted phenyl.

13. The compound of claim 3 , having a formula selected from the group consisting of:

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

14. The compound of claim 12 , having a formula selected from the group consisting of:

or a pharmaceutically acceptable salt, ester, ether or carbamate thereof.

15. A compound selected from the group consisting of: Cis-(6-benzhydryl-tetrahydropyran-3-yl)-(4-hydroxy-benzyl)-amine (16h); Cis-(6-benzhydryl-tetrahydropyran-3-yl)-(1H-iodo-5-ylmethyl)-amine (16n); Cis-(6-benzhydryl-tetrahydropyran-3-yl)-(4-amino-benzyl)-amine (16o); Cis-(6-benzhydryl-tetrahydropyran-3-yl)-(3,4-dichloro-benzyl)-amine (16i); (2R,4R,5R)-2-benzhydryl-5-(4-methoxy-benzylamino)-tetrahydropyran-4-ol (−)29a; (2S,4R,5R)-2-benzhydryl-5-(4-fluoro-benzylamino)-tetrahydro-pyran-4-ol (−)29b; (2S,4R,5R)-2-benzhydryl-5-benzylamino-tetrahydro-pyran-4-ol (−)29d; (2S,4R,5R)-2-benzhydryl-5-(2,4-dimethoxy-benzylamino)-tetrahydropyran-4-ol (−)-29e; (2S,4R,5R)-2-benzhydryl-5-(3,5-dimethoxy-benzylamino)-tetrahydropyran-4-ol (−)-29f; (2S,4R,5R)-2-benzhydryl-5-(4-hydroxy-benzylamino)-tetrahydropyran-4-ol (−)32a; (2S,4R,5R)-2-benzhydryl-5-[(1H-indol-5-ylmethyl)-amino]-tetrahydropyran-4-ol (−)32b; (2R,4S,5S)-2-benzhydryl-5-(4-hydroxy-benzylamino)-tetrahydro-pyran-4-ol (+)32a; (2R,4S,5S)-2-benzhydryl-5-[(1H-indol-5-ylmethyl)-amino]-tetrahydropyran-4-ol (+)32b; cis-(3S,6S)-(6-benzhydryl-tetrahydropyran-3-yl)-(4-hydroxy-benzyl)-amine (−)37a; cis-(3R,6R)-(6-benzhydryl-tetrahydropyran-3-yl)-(4-hydroxy-benzyl)-amine (+)37a and pharmaceutically acceptable salts, esters, ethers and carbamates thereof.

16. A compound selected from the group consisting of: (2S,4R,5R)-2-benzhydryl-5-(4-methoxy-benzylamino)-tetrahydropyran-4-ol (−)29a; (2S,4R, 5R)-2-benzhydryl-5-(4-fluoro-benzylamino)-tetrahydro-pyran-4-ol (−)29b; (2S,4R,5R)-2-benzhydryl-5-benzylamino-tetrahydro-pyran-4-ol (−)29d; (2S,4R,5R)-2-benzhydryl-5-(2,4-dimethoxy-benzylamino)-tetrahydropyran-4-ol (−)-29e; (2S,4R,5R)-2-benzhydryl-5-(3,5-dimethoxy-benzylamino)-tetrahydropyran-4-ol (−)-29f; (2S,4R,5R)-2-benzhydryl-5-(4-hydroxy-benzylamino)-tetrahydropyran-4-ol (−)32a; (2S,4R,5R)-2-benzhydryl-5-[(1H-indol-5-ylmethyl)-amino]-tetrahydropyran-4-ol (−)32b; (2R,4S,5S)-2-benzhydryl-5-(4-hydroxy-benzylamino)-tetrahydro-pyran-4-ol (+)32a; (2R,4S,5S)-2-benzhydryl-5-[(1H-indol-5-ylmethyl)-amino]-tetrahydropyran-4-ol (+)32b; cis-(3S,6S)-(6-benzhydryl-tetrahydropyran-3-yl)-(4-hydroxy-benzyl)-amine (−)37a; cis-(3R, 6R)-(6-benzhydryl-tetrahydropyran-3-yl)-(4-hydroxy-benzyl)-amine (+)37a and pharmaceutically acceptable salts, esters, ethers and carbamates thereof.

17. A method of reducing monoamine reuptake in a mammalian species, comprising administering a binding amount of a monoamine receptor binder comprising the compound of claim 1 .

18. A method of reducing monoamine reuptake in a mammalian species, comprising administering a binding amount of a monoamine receptor binder comprising the compound of claim 2 .

19. A method of reducing monoamine reuptake in a mammalian species, comprising administering a binding amount of a monoamine receptor binder comprising the compound of claim 10 .

20. A method for treatment of depression, comprising administering to a patient exhibiting signs of depression, the compound of claim 1 in an amount effective to inhibit reuptake of serotonin at the SERT and norepinephrine at the NET.

21. The method of claim 20 wherein the compound exhibits greater inhibition of serotonin and norepinephrine reuptake than of dopamine reuptake.

22. A method for treatment of depression, comprising administering to a patient exhibiting signs of depression, the compound of claim 1 in an amount effective to inhibit norepinephrine reuptake at the NET.

23. The method of claim 22 wherein said compound exhibits higher norepinephrine reuptake inhibition than serotonin reuptake inhibition and dopamine reuptake inhibition.

24. The compound of claim 18 , wherein W is —OH and B is selected from the group consisting of an optionally substituted phenyl, napthyl, anthryl, furanyl, thienyl, pyridinyl group, or

where X is N, O, or S.

Assignments (1)
CONFIRMATORY LICENSE Recorded Jul 30, 2012
From: WAYNE STATE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 028670/0066 →
Continuity (3)
Continuation 10599892
Provisional Application 60563189 · Apr 16, 2004
Related Publication 20100280091A1 · Nov 4, 2010