Device and method for producing crystalline bodies by directional solidification
The invention relates to a device and a method for producing crystalline bodies by directional solidification. The device comprises a melting furnace ( 11 ) having a heating chamber ( 12 ) in which at least one supporting surface ( 13 ) for a crucible ( 8 ) and at least one gas purging device arranged above the supporting surface ( 13 ) and having a gas outlet facing the supporting surface ( 13 ) are defined. An embodiment of the device is characterized in that the gas outlet is defined by one or more openings in a lower plunger surface of a plunger-shaped element ( 2 ) which has a geometry adapted to the inner shape of the crucible ( 8 ), said shape allowing an at least partial insertion of the plunger-shaped body ( 2 ) into the crucible ( 8 ). The gas purging device and/or the supporting surface ( 13 ) comprise an adjusting mechanism or are designed to be adjustable in such a manner that they allow an adjustment of a perpendicular distance between the supporting surface ( 13 ) and the plunger-shaped body ( 2 ). The device and the corresponding method allow carbon- and oxygen-containing materials to be discharged from the melt more efficiently and in a controlled manner. The device and the method thus allow—within certain limits—a specific adjustment of the carbon and oxygen content of the crystalline bodies.
1. A device for producing crystalline bodies by directional solidification, which encompasses a melting furnace with a heating chamber, in which are defined at least one supporting surface for a crucible having a lateral wall and floor, and at least one gas purging device arranged over the supporting surface with a gas outlet facing the supporting surface, characterized in that the gas outlet is formed by one or more openings in a lower plunger surface of a plunger-shaped body, which has a geometry adapted to the inner shape of the crucible, permitting at least a partial insertion of the plunger-shaped body into the crucible at a lateral distance to the lateral wall of the crucible, that the gas purging device and/or supporting surface are situated or mounted so that they can be adjusted in an axial direction, thereby enabling a change in the perpendicular distance between the supporting surface and plunger-shaped body, and that the plunger-shaped body has a continuous lateral projection at a distance from the lower plunger surface that makes it possible to completely cover an upper edge of the crucible.
2. A device for producing crystalline bodies by directional solidification, which encompasses a melting furnace with a heating chamber, in which are defined at least one supporting surface for a crucible having a lateral wall and floor, and at least one gas purging device arranged over the supporting surface with a gas outlet facing the supporting surface, characterized in that the gas outlet is formed by one or more openings in lower plunger surfaces of a group of several side-by-side plunger-shaped bodies, which has a geometry adapted to the inner shape of the crucible, permitting at least a partial insertion of the group of plunger-shaped bodies into the crucible at a lateral distance to the lateral wall of the crucible, and that the gas purging device and/or supporting surface are situated or mounted so that they can be adjusted in an axial direction, thereby enabling a change in the perpendicular distance between the supporting surface and plunger-shaped body.
3. The device according to claim 1 , characterized in that the plunger-shaped body has a geometry that enables at least a partial insertion of the plunger-shaped body into the crucible at a unilaterally identical distance to the lateral wall.
4. The device according to claim 2 , characterized in that the group of plunger-shaped bodies has a geometry that enables at least a partial insertion of the group of plunger-shaped bodies into the crucible at a unilaterally identical distance to the lateral wall.
5. The device according to claim 2 or 4 , characterized in that the plunger-shaped bodies have a continuous lateral projection at a distance from the lower plunger surface that makes it possible to cover an upper edge of the crucible.
6. The device according to claim 1 or 2 , characterized in that the lower plunger surface is flat and arranged parallel to the supporting surface.
7. The device according to claim 1 or 2 , characterized in that the geometry of the plunger-shaped body or group of plunger-shaped bodies is selected in such a way that the lateral distance to the lateral wall of the crucible measures ≦1 cm.
8. The device according to claim 1 or 2 , characterized in that the gas purging device consists of a carbon-free material.