IP Library Granted Patent US 8,758,646
Granted Patent B2
US 8,758,646 · App. 12/866,533 · Granted Jun 24, 2014

Phosphorescent compositions, methods of making the compositions, and methods of using the compositions

Inventors: Weiyi Jia (Chelmsford, MA); Xiaojun Wang (Statesboro, GA); William Yen (Athens, GA); George D. Jia (Oak Ridge, TN); Linda Lewis (Oak Ridge, TN)
Assignees: Georgia Southern University Research and Service Foundation, Inc.; Lock Haven University of Pennsylvania
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Quick Facts
Patent No.
US 8,758,646
App. No.
12/866,533
Granted
Jun 24, 2014
Kind
B2
Abstract

Compositions, methods of making compositions, materials including compositions, crayons including compositions, paint including compositions, ink including compositions, waxes including compositions, polymers including compositions, vesicles including the compositions, methods of making each, and the like are disclosed.

Claims (13)

1. A composition comprising:

a phosphor that emits radiation when irradiated with a wavelength of about 250 nm to 450 nm, wherein the phosphor has the following chemical formula:

La 3 Ga 5 GeO 14 :Cr 3+ , T, wherein T is Dy 3+ , and wherein the emission persists from about 1 second to 8 hours after excitation.

2. The composition of claim 1 , wherein the radiation has a radiation wavelength with an emission band peak at about 700 to 1100 nm.

3. A method of making the composition of claim 1 , comprising causing the oxides of the individual metals in that composition to react with each other in a mixture.

4. The method of claim 3 , further comprising pre-sintering the mixture of oxides.

5. The method of claim 4 , wherein a flux material is added to the mixture prior to pre-sintering.

6. The method of claim 5 , wherein the flux material is selected from the group consisting of B 2 O 3 , H 3 BO 3 , Li 2 CO 3 , Na 2 CO 3 , Bi 2 O 3 , PbO, and a combination thereof.

7. The method of claim 5 , further comprising grinding the mixture after it has been pre-sintered.

8. The method of claim 7 , further comprising sintering the mixture.

9. A material comprising:

the composition of claim 1 , wherein the composition is in a form selected from the group consisting of: powders, nanopowders, ceramics, single crystals, and a combination thereof.

10. An article comprising the composition of claim 1 , wherein the article is selected from the group consisting of a crayon, a paint, an ink, a wax, a polymer composition, a polymer-based vesicle, and a combination thereof.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 28, 2013
From: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC.
To: LOCK HAVEN UNIVERSITY OF PENNSYLVANIA
Reel/Frame 029702/0942 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2013
From: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC.
To: GEORGIA SOUTHERN UNIVERSITY RESEARCH AND SERVICE FOUNDATION, INC.
Reel/Frame 029675/0854 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 29, 2012
From: JIA, WEIYI; WANG, XIAOJUN; YEN, WILLIAM, MRS.; JIA, GEORGE D.
To: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION
Reel/Frame 028869/0705 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2012
From: LEWIS, LINDA A.
To: UT-BATTELLE, LLC
Reel/Frame 028681/0483 →
CONFIRMATORY LICENSE Recorded Mar 16, 2012
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 027875/0334 →
Continuity (2)
Provisional Application 61027121 · Feb 8, 2008
Related Publication 20120119143A1 · May 17, 2012