IP Library Granted Patent US 8,314,089
Granted Patent B2
US 8,314,089 · App. 12/884,113 · Granted Nov 20, 2012

Substituted pyrazolamides and their use

Assignee: AiCuris GmbH & Co. KG
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Quick Facts
Patent No.
US 8,314,089
App. No.
12/884,113
Granted
Nov 20, 2012
Kind
B2
Abstract

The present invention relates to novel substituted pyrazolamides, methods for their preparation, their use for the treatment and/or prophylaxis of diseases, as well as their use for the manufacture of medicaments for the treatment and/or prophylaxis of diseases, especially of retroviral diseases, in humans and/or animals.

Claims (97)

1. A method for treating retroviral diseases in humans and animals by administering a compound of formula

in which

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, C 1 -C 4 alkyl and C 1 -C 4 alkoxy,

R 3 represents a 5- to 8-membered heterocycle bonded via nitrogen,

whereby the heterocycle may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, hydroxy, hydroxymethyl, formyl, amino, oxo, trifluoromethyl, trifluoromethoxy, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl,

or one of its salts, to a human or animal in need thereof.

2. The method of claim 1 , wherein in the compound of formula (I)

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 3 represents pyrrolidin-1-yl, morpholin-4-yl, thiomorpholin-4-yl, 1,3-thiazolidin-3-yl, piperidin-1-yl, piperazin-1-yl or 1,4-oxazepan-4-yl,

whereby pyrrolidin-1-yl, morpholin-4-yl, thiomorpholin-4-yl, 1,3-thiazolidin-3-yl, piperidin-1-yl, piperazin-1-yl or 1,4-oxazepan-4-yl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of hydroxy, hydroxymethyl, formyl, amino, oxo, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl.

3. The method of claim 1 , wherein in the compound of formula (I)

(a) R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

and

R 3 represents a 5- to 8-membered heterocycle bonded via nitrogen,

whereby the heterocycle is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, hydroxy, hydroxymethyl, formyl, amino, oxo, trifluoromethyl, trifluoromethoxy, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl,

or

(b) R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of trifluoromethoxy and trifluoromethylthio,

and

R 3 represents an unsubstituted 5- to 8-membered heterocycle bonded via nitrogen.

4. A compound of formula

in which

(a) R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

and

R 3 represents a 5- to 8-membered heterocycle bonded via nitrogen,

whereby the heterocycle is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, hydroxy, hydroxymethyl, formyl, amino, oxo, trifluoromethyl, trifluoromethoxy, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl,

or one of its salts;

or a compound of formula (I) in which

(b) R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of trifluoromethoxy and trifluoromethylthio,

and

R 3 represents an unsubstituted 5- to 8-membered heterocycle bonded via nitrogen, or one of its salts.

5. A method for preparing (a) a compound of formula

in which

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

and

R 3 represents a 5- to 8-membered heterocycle bonded via nitrogen,

whereby the heterocycle is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, hydroxy, hydroxymethyl, formyl, amino, oxo, trifluoromethyl, trifluoromethoxy, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl,

or one of its salts; or

(b) a compound of formula (I) in which

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of trifluoromethoxy and trifluoromethylthio,

and

R 3 represents an unsubstituted 5- to 8-membered heterocycle bonded via nitrogen,

or one of its salts;

comprising reacting a compound of formula

in which

R 1 and R 2 have the meaning indicated in (a) or (b),

with a compound of formula

in which

A is a heterocycle as defined for R 3 in (a) or (b).

6. A method for the manufacture of a medicament for the treatment of diseases, comprising mixing a compound of claim 4 with at least one inert non-toxic pharmaceutically acceptable excipient.

7. A method for the manufacture of a medicament for the treatment of retroviral diseases, comprising mixing a compound of claim 4 with at least one inert non-toxic pharmaceutically acceptable excipient.

8. A medicament containing a compound as defined in claim 4 in combination with another active substance.

9. A medicament containing at least one compound of claim 4 in combination with at least one inert, nontoxic, pharmaceutically suitable excipient.

10. A method for controlling retroviral diseases in humans and animals by administering an antivirally effective amount of (a) at least one compound of formula

in which

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

and

R 3 represents a 5- to 8-membered heterocycle bonded via nitrogen,

whereby the heterocycle is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, hydroxy, hydroxymethyl, formyl, amino, oxo, trifluoromethyl, trifluoromethoxy, (C 1 -C 4 )-alkyl, (C 1 -C 4 )-alkoxy and (C 1 -C 4 )-alkoxycarbonyl,

(b) at least one compound of formula (I) in which

R 1 represents phenyl,

whereby phenyl is substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of halogen, cyano, nitro, trifluoromethyl, trifluoromethoxy, trifluoromethylthio, (C 1 -C 4 )-alkyl and (C 1 -C 4 )-alkoxy,

R 2 represents phenyl,

whereby phenyl may be substituted with 1 to 3 substituents, whereby the substituents are selected independently of one another from the group consisting of trifluoromethoxy and trifluoromethylthio,

and

R 3 represents an unsubstituted 5- to 8-membered heterocycle bonded via nitrogen,

or one of its salts;

(c) a medicament comprising a compound of Formula (I), or one of its salts, as defined in (a) or (b), in combination with another active substance; or

(d) a medicament comprising at least one compound of Formula (I), or one of its salts, as defined in (a) or (b), in combination with at least one inert, nontoxic, pharmaceutically suitable excipient;

to a human or animal in need thereof.

11. The method of claim 10 , wherein the retroviral disease is an infection with the HI-virus.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2012
From: BAYER SCHERING PHARMA AKTIENGESELLSCHAFT
To: AICURIS GMBH & CO. KG
Reel/Frame 029115/0399 →
MERGER Recorded Oct 11, 2012
From: BAYER HEALTHCARE AG
To: BAYER SCHERING PHARMA AKTIENGESELLSCHAFT
Reel/Frame 029125/0267 →
Priority Claims (1)
DE 10 2008 015 032 · Mar 17, 2008 · national
Continuity (2)
Continuation PCTEP2009001877 · Mar 14, 2009
Related Publication 20110172207A1 · Jul 14, 2011