IP Library Granted Patent US 8,801,897
Granted Patent B2
US 8,801,897 · App. 12/938,879 · Granted Aug 12, 2014

Compact wastewater concentrator and contaminant scrubber

Inventors: Bernard F. Duesel, Jr. (Goshen, NY); Michael J. Rutsch (Tulsa, OK); Craig Clerkin (Stoughton, WI)
Assignee: Heartland Technology Partners LLC
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Quick Facts
Patent No.
US 8,801,897
App. No.
12/938,879
Granted
Aug 12, 2014
Kind
B2
Abstract

A compact and portable liquid concentrator and contaminant scrubber includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. A reagent may be mixed with the liquid to react with contaminants in the liquid.

Claims (31)

1. A process for removing contaminants from flowback water from a natural gas well, the process using a wastewater concentrator including a gas inlet, a gas outlet, a concentrating section between the gas inlet and the gas outlet, the concentrating section having a narrowed portion, the process comprising:

mixing a reagent with liquid flowback water from a natural gas well, the reagent reacting with a soluble chemical compound in the liquid flowback water to form an insoluble chemical compound;

combining a gas and the liquid flowback water in the concentrating section to form a mixture of gas and entrained liquid flowback water, the entrained liquid flowback water including the insoluble chemical compound;

directing the combined gas and entrained liquid flowback water into a demister where at least some of the entrained liquid flowback water is removed from the gas and collected in a sump of the demister;

removing a portion of the liquid flowback water in the sump of the demister and sending the portion of the liquid flowback water to a settling tank where suspended solids and insoluble chemical compounds in the liquid flowback water separate from liquid portions of the liquid wastewater;

removing the separated solid portion from the settling tank and returning the separated liquid portion to the demister sump.

2. The process of claim 1 , wherein the reagent is sodium sulfate.

3. The process of claim 2 , wherein the soluble chemical compound is barium chloride.

4. The process of claim 3 , wherein a sulfate ion from the sodium sulfate reacts with a barium ion from the barium chloride to form barium sulfate, which is highly insoluble.

5. The process of claim 1 , wherein the reagent is stored in a reagent tank that is connected to a liquid flowback water inlet for injecting liquid flowback water into the concentrating section.

6. The process of claim 1 , wherein the reagent is stored in a reagent tank that is connected to the concentrating section upstream of the narrowed portion.

7. The process of claim 1 , wherein the separated solid portion removed from the settling tank is sent to a vacuum belt filtration system for further solid/liquid separation.

8. The process of claim 1 , wherein the insoluble chemical compound is purified after removal from the settling tank.

9. The process of claim 8 , wherein the purified insoluble chemical compound is sold for use in well drilling mud.

10. The process of claim 1 , wherein a pump delivers reagent to the concentrating section, the pump delivering between approximately 150% and approximately 600% of the amount of reagent that would be needed to fully react with the soluble chemical compound.

11. The process of claim 10 , wherein the pump delivers between approximately 200% and approximately 500% of the amount of reagent that would be needed to fully react with the soluble chemical compound.

12. The process of claim 11 , wherein the pump delivers approximately 400% of the amount of reagent that would be needed to fully react with the soluble chemical compound.

13. The process of claim 1 , wherein the liquid wastewater contains more than approximately 250,000 parts per million of dissolved solids.

14. A flowback concentrating and containment removal system for flowback water from natural gas wells, the system comprising:

a gas inlet;

a gas outlet;

a concentrating section disposed between the gas inlet and the gas outlet, the concentrating section having a narrowed portion in which gas flow within the concentrating section accelerates;

a liquid inlet through which flowback water is injected into the concentrating section, the liquid inlet being disposed in the concentrating section upstream of the narrowed portion;

a demister disposed downstream of the narrowed portion, the demister removing entrained liquid droplets from the gas flow; and

a reagent tank for holding a supply of reagent, the reagent tank being connected to the concentrating section to inject reagent into the concentrating section.

15. The system of claim 14 , further comprising a reagent pump connected to the reagent tank.

16. The system of claim 15 , wherein the reagent tank is connected to the liquid inlet.

17. The system of claim 15 , wherein the reagent tank is connected to the concentrating section upstream of the narrowed portion.

18. The system of claim 15 , wherein the entrained liquid droplets that are removed by the demister collect in a sump.

19. The system of claim 18 , wherein the sump is connected to a settling tank and liquid and solid portions of the collected entrained liquid droplets separate from one another in the settling tank.

20. The system of claim 18 , wherein the settling tank is connected to the sump with a return line that returns a liquid portion of the collected entrained liquid droplets to the sump.

Assignments (5)
SECURITY INTEREST Recorded Jan 14, 2022
From: THE DONNA M. IRWIN FAMILY TRUST
To: HEARTLAND TECHNOLOGY PARTNERS, LLC
Reel/Frame 058660/0396 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 29, 2021
From: HEARTLAND TECHNOLOGY PARTNERS LLC
To: HEARTLAND WATER TECHNOLOGY, INC.
Reel/Frame 058501/0124 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE PREVIOUSLY RECORDED ON REEL 026469 FRAME 0181. ASSIGNOR(S) HEREBY CONFIRMS THE HEARTLAND TECHNOLOGY PATNERS LLC. Recorded Jul 28, 2011
From: DUESEL JR., BERNARD F.; RUTSCH, MICHAEL J.; CLERKIN, CRAIG
To: HEARTLAND TECHNOLOGY PARTNERS LLC
Reel/Frame 026677/0687 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 21, 2011
From: DUESEL, BERNARD F., JR.; RUTSCH, MICHAEL J.; CLERKIN, CRAIG
To: HEARTLAND TECHNOLOGY PARTNERS
Reel/Frame 026469/0181 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2011
From: DUESEL, BERNARD F., JR.; RUTSCH, MICHAEL J.; CLERKIN, CRAIG
To: HEARTLAND TECHNOLOGY PARTNERS LLC
Reel/Frame 025744/0341 →
Continuity (7)
Continuation In Part 12846337 · Jul 29, 2010
Continuation In Part 12705462 · Feb 12, 2010
Continuation In Part 12530484
Provisional Application 61152248 · Feb 12, 2009
Provisional Application 61229650 · Jul 29, 2009
Provisional Application 60906743 · Mar 13, 2007
Related Publication 20110100924A1 · May 5, 2011