IP Library Granted Patent US 9,103,000
Granted Patent B2
US 9,103,000 · App. 12/953,129 · Granted Aug 11, 2015

Low melting point sputter targets for chalcogenide photovoltaic applications and methods of manufacturing the same

Inventors: Mariana Munteanu (Santa Clara, CA); Brian Josef Bartholomeusz (Palo Alto, CA); Michael Bartholomeusz (Phoenix, AZ); Erol Girt (Burnaby, CA)
Assignee: ZETTA RESEARCH AND DEVELOPMENT LLC—AQT SERIES
C22C1/0491C04B35/547C04B35/6455C04B35/653C23C14/0623C23C14/3414B22F2998/10C04B2235/3201C04B2235/3206C04B2235/3217C04B2235/3232C04B2235/3239C04B2235/3244C04B2235/3251C04B2235/3256C04B2235/3258C04B2235/3262C04B2235/3281C04B2235/3284C04B2235/3286C04B2235/3289C04B2235/3293C04B2235/3296C04B2235/3298C04B2235/3418C04B2235/42C04B2235/6565C04B2235/72C04B2235/721C04B2235/722C04B2235/723C04B2235/77
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Quick Facts
Patent No.
US 9,103,000
App. No.
12/953,129
Granted
Aug 11, 2015
Kind
B2
Abstract

In one example embodiment, a sputter target structure for depositing semiconducting chalcogenide films is described. The sputter target includes a target body having a target body composition that comprises Cu 1-x (Se 1-y-z S y Te z ) x , wherein the value of x is greater than or equal to approximately 0.5, the value of y is between approximately 0 and approximately 1, the value of z is between approximately 0 and approximately 1, and the total amount of Se, S, and Te phases in the target body composition comprise less than 50 volume percent of the target body composition.

Claims (19)

1. A sputter target structure for depositing semiconducting chalcogenide films, comprising:

a target body having a target body composition that comprises Cu 1-x (Se 1-y-z S y Te z ) x , wherein:

the value of x is greater than or equal to approximately 0.5;

the value of y is greater than 0 and less than or equal to 1;

the value of z is greater than 0 and less than or equal to 1; and

the total amount of Se, S, and Te phases in the target body composition comprise less than 50 volume percent of the target body composition, and

wherein at least approximately 50 volume percent (50 vol. %) of the target body composition consists of CuSe and CuSe 2 phases.

2. The sputter target structure of claim 1 wherein at least approximately 80 volume percent (80 vol. %) of the target body composition consists of CuSe and CuSe 2 phases.

3. The sputter target structure of claim 1 wherein at least approximately 90 volume percent (90 vol. %) of the target body composition consists of CuSe and CuSe 2 phases.

4. The sputter target structure of claim 1 ,

wherein the sputter target composition has a purity of at least approximately 2N7, gaseous impurities less than approximately 500 parts-per-million (ppm) for oxygen (O), nitrogen (N), and hydrogen (H) individually, a carbon (C) impurity less than approximately 500 ppm, and a density of at least 95% of a theoretical density for the sputter target composition.

5. The sputter target structure of claim 4 wherein the sputter target composition includes one or more dopants selected from the group consisting of phosphorus (P), nitrogen (N), boron (B), arsenic (As), and antimony (Sb).

6. The sputter target structure of claim 4 wherein the sputter target composition contains up to approximately 5 atomic % of at least one element of Na, potassium (K), rubidium (RB), or magnesium (Mg).

7. The sputter target structure of claim 4 wherein the sputter target composition contains up to approximately 10 atomic % of at least one element of Al, Si, Ti, V, Zn, Ga, Zr, Nb, Mo, Ru, Pd, In, Sn, Ta, W, Re, Ir, Pt, Au, Pb, and Bi.

8. The sputter target structure of claim 4 wherein the sputter target composition contains one or more of insulating oxides, nitrides, carbides, and/or borides.

9. The sputter target structure of claim 1 wherein the sputter target composition includes one or more dopants selected from the group consisting of phosphorus (P), nitrogen (N), boron (B), arsenic (As), and antimony (Sb).

10. The sputter target structure of claim 1 wherein the sputter target composition contains up to approximately 5 atomic % of at least one element of Na, potassium (K), rubidium (RB), or magnesium (Mg).

11. The sputter target structure of claim 1 wherein the sputter target composition contains up to approximately 10 atomic % of at least one element of Al, Si, Ti, V, Zn, Ga, Zr, Nb, Mo, Ru, Pd, In, Sn, Ta, W, Re, Ir, Pt, Au, Pb, and Bi.

12. The sputter target structure of claim 1 wherein the sputter target composition contains one or more of insulating oxides, nitrides, carbides, and/or borides.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 17, 2013
From: AQT SOLAR, INC.
To: SWANSON, JOHN A.
Reel/Frame 029650/0366 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 17, 2013
From: SWANSON, JOHN A.
To: ZETTA RESEARCH AND DEVELOPMENT LLC - AQT SERIES
Reel/Frame 029650/0500 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2011
From: MUNTEANU, MARIANA RODICA; BARTHOLOMEUSZ, BRIAN JOSEF; BARTHOLOMEUSZ, MICHAEL; GIRT, EROL
To: AQT SOLAR, INC.
Reel/Frame 025662/0965 →
Continuity (2)
Provisional Application 61264568 · Nov 25, 2009
Related Publication 20110290643A1 · Dec 1, 2011