IP Library Granted Patent US 8,938,993
Granted Patent B2
US 8,938,993 · App. 12/957,202 · Granted Jan 27, 2015

Glass strengthening and patterning methods

Inventors: David C. Harper (Kingston, TN); Andrew A. Wereszczak (Oak Ridge, TN); Chad E. Duty (Knoxville, TN)
Assignee: UT-Battelle, LLC
C03B27/012C03C23/006
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Quick Facts
Patent No.
US 8,938,993
App. No.
12/957,202
Granted
Jan 27, 2015
Kind
B2
Abstract

High intensity plasma-arc heat sources, such as a plasma-arc lamp, are used to irradiate glass, glass ceramics and/or ceramic materials to strengthen the glass. The same high intensity plasma-arc heat source may also be used to form a permanent pattern on the glass surface—the pattern being raised above the glass surface and integral with the glass (formed of the same material) by use of, for example, a screen-printed ink composition having been irradiated by the heat source.

Claims (29)

1. A method comprising:

strengthening an untreated glass sample by;

providing a soda-lime silicate glass have a first surface comprising a tin side, a second surface comprising an air side and edges;

providing a plasma-arc heat source capable of delivering a power density of at least 900 W/cm 2 in less than one second;

unidirectionally translating the glass under the plasma-arc heat source at a speed of 8 mm/s;

irradiating the first surface of the glass with the plasma-arc heat source at a power density of 900 W/cm 2 ; and

quenching the glass following irradiation;

thereby increasing an equibiaxial failure stress of the untreated glass by 25% or more and a uniaxial 4-point-bend failure stress of the untreated glass by 65% or more.

2. The method of claim 1 further comprising annealing the strengthened glass using the plasma-arc heat source for a second stage of heating.

3. A method comprising:

patterning a glass sample by;

providing a soda-lime silicate glass have a first surface, a second surface and edges;

forming a first pattern of graphitic ink on the first surface of the glass using a screen printing method;

providing a plasma-arc heat source capable of delivering a power density of at least 900 W/cm 2 in less than one second;

unidirectionally translating the glass under the plasma-arc heat source at a speed of 8 mm/s; and

irradiating the first surface of the glass with the plasma-arc heat source at a power density of 900 W/cm 2 and substantially simultaneously evolving the ink thereby forming a second pattern on the first surface of the glass wherein the second pattern comprises a glass material raised from the first surface of the glass, the second pattern corresponding to the first pattern.

4. The method of claim 3 wherein the graphitic ink comprises permanent black pen ink.

5. A method comprising:

patterning a glass or glass ceramic sample by forming a first pattern of ink on a first surface of the glass; and

irradiating the first surface of the glass with a plasma-arc heat source at a power density of 900 W/cm 2 thereby forming a second pattern on the first surface of the glass wherein the second pattern comprises a glass material raised from the first surface of the glass, the second pattern corresponding to the first pattern.

6. The method of claim 5 wherein the ink is controllably patterned onto the glass or glass ceramic sample.

7. The method of claim 5 further comprising unidirectionally translating the glass under the plasma-arc heat source at a speed of 8 mm/s.

8. The method of claim 5 wherein the glass comprises a silicate glass.

9. The method of claim 5 wherein the ink comprises black pen ink.

10. The method of claim 5 wherein the second pattern comprises a glass material having a different density value than that of the non-raised, unpatterned glass.

11. The method of claim 5 wherein the second pattern comprises a glass material raised from the first surface of the glass such that the pattern is visible to the naked eye.

12. The method of claim 5 wherein the second pattern comprises a glass material raised from the first surface of the glass at a height such that the pattern is capable of detection by touching the glass surface.

13. The method of claim 5 wherein the second pattern comprises a UPC code, a part number and/or a word.

14. The method of claim 5 wherein the second pattern comprises a raised glass material integral with glass material at the first surface.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 11, 2011
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 025935/0427 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2011
From: HARPER, DAVID C.; WERESZCZAK, ANDREW A.
To: UT-BATTELLE, LLC
Reel/Frame 025908/0948 →
Continuity (1)
Related Publication 20120131960A1 · May 31, 2012