IP Library Granted Patent US 8,418,547
Granted Patent B2
US 8,418,547 · App. 13/057,701 · Granted Apr 16, 2013

Force, pressure, or stiffness measurement or calibration using graphene or other sheet membrane

Inventors: Jeffrey William Kysar (New York, NY); James C. Hone (New York, NY); Changgu Lee (New York, NY); Xiaoding Wei (New York, NY)
Assignee: The Trustees of Columbia University in the City of New York
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Quick Facts
Patent No.
US 8,418,547
App. No.
13/057,701
Granted
Apr 16, 2013
Kind
B2
Abstract

Force, pressure, or stiffness measurement or calibration can be provided, such as by using a graphene or other sheet membrane, which can provide a specified number of monolayers suspended over a substantially circular well. In an example, the apparatus can include a substrate, including a substantially circular well. A deformable sheet membrane can be suspended over the well. The membrane can be configured to include a specified integer number of one or more monolayers. A storage medium can comprise accompanying information about the suspended membrane or the substrate that, with a deflection displacement response of the suspended membrane to an applied force or pressure, provides a measurement of the applied force or pressure.

Claims (43)

1. An apparatus comprising:

a substrate, including a substantially circular well;

a deformable sheet membrane, suspended over the well, the membrane configured to include a specified integer number of one or more monolayers; and

a processor-readable storage medium comprising:

accompanying information about the suspended membrane or the substrate that, with a deflection displacement response of the suspended membrane to an applied force or pressure, provides a measurement of the applied force or pressure; and

instructions that, when performed by a processor, cause the processor to calibrate a transducer using the accompanying information about the deflection displacement response of the suspended membrane to the applied force or pressure.

2. The apparatus of claim 1 , wherein the storage medium comprises accompanying information about at least one of a dimension of the well or a tension of the membrane.

3. The apparatus of claim 1 , further comprising the transducer configured to transduce a deflection of the membrane, for use with the accompanying information, to provide the measurement of the applied force or pressure.

4. The apparatus of claim 3 , wherein the transducer comprises at least one of an atomic force microscope (AFM) or a nanoindenter.

5. The apparatus of claim 1 , comprising a plurality of wells, included on the substrate, and corresponding suspended membranes.

6. The apparatus of claim 1 , wherein the membrane comprises graphene.

7. The apparatus of claim 6 , wherein the membrane consists of graphene.

8. A method comprising:

using a substrate including a substantially circular well;

using a deformable sheet membrane that is suspended over the well, the membrane configured to include a specified integer number of monolayers; and

calibrating a device using a deflection displacement response of the suspended membrane to an applied force or pressure.

9. The method of claim 8 , comprising calibrating the device using (1) information about the suspended membrane or the substrate and (2) the deflection displacement response of the suspended membrane to an applied force or pressure.

10. The method of claim 8 , comprising using measured information about a diameter of the well in performing the calibrating.

11. The method of claim 8 , comprising using measured information about a tension of the membrane in performing the calibrating.

12. The method of claim 11 , comprising using measured information about the tension of the membrane in performing the calibrating, wherein the measured information is obtained using x-ray diffraction.

13. The method of claim 11 , comprising using measured information about the tension of the membrane in performing the calibrating, wherein the measured information is obtained using Raman spectroscopy.

14. The method of claim 8 , wherein using a deformable sheet membrane comprises using a material comprising graphene.

15. The method of claim 14 , wherein using a deformable sheet membrane comprises using a material consisting of graphene.

16. The method of claim 8 , wherein the calibrating comprises:

measuring a deflection of the membrane; and

providing information about the deflection to a user or automated process.

17. The method of claim 16 , wherein the measuring the deflection of the membrane comprises using the device being calibrated for measuring the deflection of the membrane.

18. The method of claim 8 , wherein the calibrating the device comprises calibrating an atomic force microscope (AFM).

19. The method of claim 8 , wherein the calibrating the device comprises calibrating a nanoindenter.

20. A method of claim 8 , comprising:

measuring at least one of a diameter of the well or a tension of the membrane; and

providing a user or automated process with information about at least one of the diameter of the well or a tension of the membrane.

21. A method comprising:

providing an apparatus comprising:

a substrate, including a substantially circular well;

a deformable sheet graphene membrane, suspended over the well, the membrane configured to include a specified integer number of one or more graphene monolayers; and

a storage medium comprising accompanying information about the suspended membrane or the substrate that, with a deflection displacement response of the suspended membrane to an applied force or pressure, provides a measurement of the applied force or pressure, wherein the storage medium comprises accompanying information about a dimension of the well and a tension of the membrane;

a transducer configured to transduce a deflection of the membrane, for use with the accompanying information, to provide the measurement of the applied force or pressure, wherein the transducer comprises at least one of an atomic force microscope (AFM) or a nanoindenter; and

calibrating at least one of an atomic force microscope (AFM) device or a nanoindenter device, using (1) information about the suspended membrane or the substrate, including using measured information about a diameter of the well and measured information about a tension of the membrane obtained using at least one of x-ray diffraction or Raman spectroscopy, and (2) the deflection displacement response of the suspended membrane to an applied force or pressure, wherein the calibrating comprises

measuring a deflection of the membrane; and

providing information about the deflection to a user or automated process.

22. The apparatus of claim 4 , wherein the processor-readable medium includes instruction to calibrate the transducer using measured information about a diameter of the well and measured information about a tension of the membrane.

23. The apparatus of claim 22 , wherein the measured information about the tension of the membrane is obtained using at least one of x-ray diffraction or Raman spectroscopy.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 19, 2011
From: COLUMBIA UNIVERSITY NEW YORK MORNINGSIDE
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 026776/0593 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2011
From: KYSAR, JEFFREY WILLIAM; HONE, JAMES C.; LEE, CHANGGU; WEI, XIAODING
To: TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK, THE
Reel/Frame 025940/0096 →
Continuity (2)
Provisional Application 61188212 · Aug 7, 2008
Related Publication 20110185458A1 · Jul 28, 2011