IP Library Granted Patent US 8,859,090
Granted Patent B2
US 8,859,090 · App. 13/062,721 · Granted Oct 14, 2014

Micro-structured surface having tailored wetting properties

Inventors: Dan Angelescu (Noisy le Grand Cedex, FR); Tullio Moscato (Paris, FR); Frederic Pauchet (Montigny sur Loing, FR); Robert Van Kuijk (Le Plessis Robinson, FR)
Assignee: Schlumberger Technology Corporation
B01D69/02B01D2325/028B01D2325/06
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Quick Facts
Patent No.
US 8,859,090
App. No.
13/062,721
Granted
Oct 14, 2014
Kind
B2
Abstract

A micro-structured surface for immersing in a multiphase fluid mixture comprises a substrate having pores and a wetting liquid phase trapped in the pores. The wetting liquid phase is immiscible with all the phases of the multiphase fluid mixture. Alternatively, the wetting liquid phase is miscible with one of the phase of the multiphase fluid mixture.

Claims (30)

1. A micro-structured surface immersed in a multiphase fluid mixture comprising a substrate having pores and a wetting liquid phase trapped in the pores, said wetting liquid phase being immiscible with all phases of the multiphase fluid mixture.

2. A micro-structured surface according to claim 1 , wherein the substrate receives a chemical treatment improving the wetting of the substrate by the wetting liquid phase.

3. A micro-structured surface according to claim 1 , wherein the surface comprises a closed-cell network of micro-wells forming the pores made in the substrate.

4. A micro-structured surface according to claim 1 , wherein the surface comprises an open-cell network of micro-pillars forming the pores made on the substrate.

5. A micro-structured surface according to claim 1 , wherein the surface comprises a combination of an open-cell network of micro-pillars and a closed-cell network of micro-wells forming the pores in the substrate.

6. A micro-structured surface according to claim 1 , wherein the substrate is made of a material chosen in the group of material comprising silicon, silicon oxide, glass, metal, ceramic, sapphire, alumina, titanium oxide, fluorinated polymer, plastics, naturally porous material, mesh, and solid foam.

7. A micro-structured surface according to claim 1 , wherein the substrate is covered with a coating film.

8. A micro-structured surface according to claim 7 , wherein the film is chosen among the group of film comprising fluoropolymer film, fluorocarbon film, photocatalytic film, titanium dioxide film, silicon dioxide film, and metal film.

9. A micro-structured surface according to claim 1 , wherein the wetting liquid phase is a fluorinated solvent.

10. A measuring device comprising: a micro-structured surface immersed in a multiphase fluid mixture comprising:

a substrate having pores and a wetting liquid phase trapped in the pores, said wetting liquid phase being immiscible with all phases of the multiphase fluid mixture.

11. A measuring device according to claim 10 , wherein the measuring device further comprises a radiation source for permanently or periodically activating the micro-structured surface by exposure to radiation.

12. A method of manufacturing a micro-structured surface having a controlled wetting property that is immersed in a multiphase fluid mixture comprising:

providing a micro-structured surface, and

trapping a wetting liquid phase within the micro-structured surface through a surface priming process

wherein the wetting liquid phase is immiscible with all phases of the multiphase fluid mixture.

13. A method of manufacturing a micro-structured surface according to claim 12 , wherein providing a micro-structured surface further comprises micro-structuring a substrate.

14. A method of manufacturing a micro-structured surface according to claim 13 , wherein providing a micro-structured surface consists in providing a naturally porous material.

15. A method of manufacturing a micro-structured surface according to claim 12 , wherein providing a micro-structured surface is further followed by conformal coating or film deposition.

16. A method of manufacturing a micro-structured surface according to claim 15 , wherein the coating or film having photocatalytic properties is activated upon exposure to a source of radiation.

17. A method of manufacturing a micro-structured surface according to claim 12 , wherein the surface priming process comprises:

submerging the micro-structured surface inside the wetting liquid phase,

pulling a vacuum by reducing an initial pressure enough so that the gas phases initially trapped in the micro-structured surface leaves the pores of the micro-structured surface; and

increasing the pressure to the initial pressure.

18. A method of manufacturing a micro-structured surface according to claim 17 , wherein the pressure reduction and increasing cycle is repeated several times.

19. A method of manufacturing a micro-structured surface according to claim 12 , wherein the surface priming process comprises:

putting the wetting liquid phase into contact with the micro-structured surface;

pressurizing the micro-structured surface and the wetting liquid phase such as to allow the gas phases initially trapped in the microstructure to diffuse into the liquid;

waiting a determined duration; and

decreasing the pressure to the initial pressure.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2011
From: ANGELESCU, DAN; MOSCATO, TULLIO; PAUCHET, FREDERIC; VAN KUIJK, ROBERT
To: SCHLUMBERGER TECHNOLOGY CORPORATION
Reel/Frame 026749/0314 →
Continuity (1)
Related Publication 20110283778A1 · Nov 24, 2011