Method for producing spherical alumina powder
A production method comprising the steps of: spraying an aluminum hydroxide powder having a specific surface area measured by a nitrogen adsorption method of 0.3 m 2 /g or more and 3 m 2 /g or less; a ratio of an average particle diameter D50, which is a particle diameter at which 50% by weight of particles from the finest particle side are accumulated in a particle diameter distribution measured by a laser diffraction scattering method, to a sphere conversion particle diameter Dbet calculated from a specific surface area, of 10 or less; and the average particle diameter D50 of 2 μm or more and 100 μm or less, into flames, and then collecting it in the form of a powder to give a spherical alumina powder having a small specific surface area and a low uranium content, and capable of providing high thermal conductivity to resin compositions.
1. A spherical alumina powder for adding to a resin, which has an average particle diameter D50, which is a particle diameter at which 50% by weight of particles from the finest particle side are accumulated in a particle diameter distribution measured by a laser diffraction scattering method, of 2 μm or more and 100 μm or less; a specific surface area measured by a nitrogen adsorption method of 1 m 2 /g or less; a ratio of the average particle diameter D50 to a sphere conversion particle diameter Dbet calculated from a specific surface area, D50/Dbet, of 5 or less; and a uranium content of 10 ppb or less.
2. A method for producing a spherical alumina powder according to claim 1 , comprising the steps of:
spraying an aluminum hydroxide powder having a specific surface area measured by a nitrogen adsorption method of 0.3 m 2 /g or more and 3 m 2 /g or less; a ratio of an average particle diameter D50, which is a particle diameter at which 50% by weight of particles from the finest particle side are accumulated in a particle diameter distribution measured by a laser diffraction scattering method, to a sphere conversion particle diameter Dbet calculated from a specific surface area, D50/Dbet, of 10 or less; and the average particle diameter D50 of 2 μm or more and 100 μm or less, into flames, and then,
collecting the spherical alumina powder.
3. The production method according to claim 2 , wherein the aluminum hydroxide powder has a gibbsite crystal form which is measured by powder X-ray diffraction and a peak intensity ratio of the crystal face (110) to the crystal face (002), I(110)/I(002), of 0.20 or more.
4. The production method according to claim 2 , wherein the aluminum hydroxide powder has a particle diameter distribution index of a particle diameter D10, which is a particle diameter at which 10% by weight of particles from the finest particle side are accumulated in a particle diameter distribution measured by a laser diffraction scattering method and a particle diameter D90, which is a particle diameter at which 90% by weight of particles are accumulated, D90/D10, of 12 or less.
5. The production method according to claim 2 , wherein the aluminum hydroxide powder has a uranium content of 10 ppb or less.