IP Library Granted Patent US 9,083,045
Granted Patent B2
US 9,083,045 · App. 13/116,360 · Granted Jul 14, 2015

Composite materials, production thereof and use thereof in electrical cells

Inventor: Nicole Janssen (Bermersheim, DE)
Assignee: BASF SE
H01M4/58H01M4/136H01M4/5815H01M4/622H01M4/624H01M4/1397H01M4/16H01M4/362H01M4/625H01M4/668H01M10/052H01M10/058H01M10/0569H01M10/3909Y02E60/122
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Quick Facts
Patent No.
US 9,083,045
App. No.
13/116,360
Granted
Jul 14, 2015
Kind
B2
Abstract

A composite material comprising a reaction product of (A) at least one organic polymer, (B) sulfur and (C) carbon in a polymorph which comprises at least 60% sp 2 -hybridized carbon atoms, and additionally particles or domains which comprise carbon (C) filled with sulfur (B).

Claims (25)

1. A process for producing composite materials, which comprises reacting

a. at least one organic polymer,

b. sulfur and

c. carbon in a polymorph which comprises at least 60% sp 2 -hybridized carbon atoms,

with one another at temperatures in the range from 200 to 400° C.

2. The process according to claim 1 , wherein said organic polymer is selected from polyethylene, polypropylene, polyacrylonitrile, polybutadiene, polystyrene and copolymers of at least two comonomers selected from ethylene, propylene, styrene, acrylonitrile and 1,3-butadiene.

3. The process according to claim 1 , wherein said organic polymer (A) is a polyacrylonitrile.

4. The process according to claim 1 , wherein said polyacrylonitrile is present after the reaction at least partially in the form of a cyclization product of the formula I

5. The process according to claim 1 , wherein said carbon is carbon black.

6. The process according to claim 1 , wherein said polyacrylonitrile before the reaction has a mean molecular weight M w , in the range from 50 000 to 250 000 g/mol.

7. The process according to claim 1 , further comprising a binder (D).

8. The process according to claim 1 , which further comprises carbon black which has not been reacted with said polyacrylonitrile and said sulfur.

9. A process for producing composite materials, which comprises reacting

a. at least one organic polymer,

b. sulfur and

c. carbon in a polymorph which comprises at least 60% sp 2 -hybridized carbon atoms,

with one another at temperatures in the range from 200 to 400° C.,

wherein in said reacting particles or domains which comprise said carbon filled with said sulfur are formed.

10. The process according to claim 9 , wherein said organic polymer is selected from polyethylene, polypropylene, polyacrylonitrile, polybutadiene, polystyrene and copolymers of at least two comonomers selected from ethylene, propylene, styrene, acrylonitrile and 1,3-butadiene.

11. The composite material process according to claim 9 , wherein said organic polymer is a polyacrylonitrile.

12. The process according to claim 11 , wherein said polyacrylonitrile is present after the reaction at least partially in the form of a cyclization product of the formula I

13. The process according to claim 9 , wherein said carbon is carbon black.

14. The process according to claim 9 , wherein said polyacrylonitrile before the reaction has a mean molecular weight M w in the range from 50 000 to 250 000 g/mol.

15. The process according to claim 9 , further comprising a binder (D).

16. The process according to claim 9 , which further comprises carbon black which has not been reacted with said polyacrylonitrile and said sulfur.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2011
From: JANSSEN, NICOLE
To: BASF SE
Reel/Frame 026901/0760 →
Continuity (2)
Provisional Application 61349218 · May 28, 2010
Related Publication 20110318654A1 · Dec 29, 2011