IP Library Granted Patent US 8,859,590
Granted Patent B2
US 8,859,590 · App. 13/132,665 · Granted Oct 14, 2014

Inhibitors of BACE1 and methods for treating Alzheimer's disease

Inventor: Arun K. Ghosh (West Lafayette, IN)
Assignee: Purdue Research Foundation
C07D277/28C07C2102/08C07C311/08
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Quick Facts
Patent No.
US 8,859,590
App. No.
13/132,665
Granted
Oct 14, 2014
Kind
B2
Abstract

Inhibitors of BACE1 and compositions containing them are described. Use of the inhibitors and compositions containing them to treat Alzheimer's disease are described.

Claims (24)

1. A compound of formula

or a pharmaceutically acceptable salt, isomer, mixture of isomers, crystalline form, non crystalline form, hydrate, or solvate thereof, wherein

R is optionally substituted aryl, X 1 is optionally substituted alkylene, and A is NR 1 , where R 1 is hydrogen or alkyl; or

R is optionally substituted heteroaryl, X 1 is CH 2 , A is NR 1 , and R 1 is hydrogen or alkyl; or

A is NR 1 , R is heteroaryl, and R 1 , X 1 and the attached nitrogen form a heterocycle;

X 2 is C(O);

Q 1 is 1,3-phenylene, which is optionally substituted at the 5-position with N-methylmethylsulfonylamido, alkyl, or heteroalkyl;

X 3 is C(O);

R 2 , R 3 , and R 4 are each hydrogen;

R 5 is arylalkyl, which is optionally substituted;

R 6a is C(O)NHR 10a , where R 10a is alkyl; and R 6b is alkyl.

2. The compound of claim 1 which is the most potent isomer of diastereoisomers formed by R 6a and R 6b in the inhibition of BACE1.

3. The compound of claim 1 wherein R is optionally substituted aryl, X 1 is optionally substituted alkylene, and A is NR 1 , where R 1 is hydrogen or alkyl.

4. The compound of claim 3 wherein R 1 is hydrogen.

5. The compound of claim 3 wherein R is aryl, X 1 is alkylene, and R 1 is hydrogen.

6. The compound of claim 1 wherein R is optionally substituted heteroaryl, X 1 is CH 2 , A is NR 1 , and R 1 is hydrogen or alkyl.

7. The compound of claim 6 wherein the heteroaryl is optionally substituted oxazolyl or thiazolyl.

8. The compound of claim 1 wherein A is NR 1 , R is heteroaryl, and R 1 , X 1 and the attached nitrogen form a heterocycle.

9. The compound of claim 8 wherein the heterocycle is pyrrolidinyl.

10. The compound of claim 1 which is a compound of formula

wherein X is O, S, or NMe; R is hydrogen, alkyl, or heteroalkyl; and y is hydrogen, alkyl, or heteroalkyl.

11. The compound of claim 1 wherein A is NR 1 , where R 1 is hydrogen; and R—X 1 — form (R)-1-phenyl-1-ethyl.

12. The compound of claim 1 which is a compound of formula

13. A pharmaceutical composition comprising the compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier or excipient.

Assignments (1)
CONFIRMATORY LICENSE Recorded Apr 18, 2013
From: PURDUE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 030242/0227 →
Continuity (3)
Provisional Application 61120174 · Dec 5, 2008
Provisional Application 61181350 · May 27, 2009
Related Publication 20110275619A1 · Nov 10, 2011