IP Library Granted Patent US 8,835,445
Granted Patent B2
US 8,835,445 · App. 13/151,683 · Granted Sep 16, 2014

Dihydrofolate reductase inhibitors

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,835,445
App. No.
13/151,683
Granted
Sep 16, 2014
Kind
B2
Abstract

The present disclosure provides compounds of Formula I: or a pharmaceutically acceptable salt thereof, wherein R 5 , R 6 and Z are as described herein. The disclosure also provides pharmaceutical compositions thereof; and methods for inhibiting DHFR activity; and methods for treating cell proliferative diseases, autoimmune disease, inflammatory disease or bacterial, fungal or parasitic infection by administering a compound of Formula I.

Claims (26)

1. A compound having the structure

wherein

Z is a seven to 10-membered heteroaryl ring comprising 0-4 heteroatoms independently selected from the group consisting of N, O, and S;

when two rings comprise the seven to 10-membered heteroaryl ring, the two rings are heteroaromatic;

R represents one or more moieties independently selected from the group consisting of H, halo, lower alkyl, lower alkoxy, CF 3 , amino, CN, CO 2 CH 3 , optionally-substituted aryl, and optionally-substituted heterocyclyl;

R 5 is selected from the group consisting of H, halo, lower alkyl, and lower alkoxy;

R 6 is selected from the group consisting of H, halo, lower alkyl, lower alkoxy, CF 3 , 5-membered heteroarylmethylene, and amino; and pharmaceutically acceptable salts and solvates thereof.

2. The compound of claim 1 , wherein Z is selected from the group consisting of optionally-substituted isoquinoline, benzofuran, benzothiophene, indole, pyrrolopyridine, imidazopyridine, indazole benzimidazole, benzothiazole, quinoline, and benzotriazole.

3. The compound of claim 2 , wherein Z is optionally-substituted benzimidazole.

4. The compound of claim 1 , wherein R is selected from the group consisting of halo, optionally-substituted lower alkyl, lower alkoxy, and heterocyclyl.

5. The compound of claim 1 , wherein R is selected from the group consisting of Me, Et, i-Pr, Cl, F, MeO, cyano, and CF 3.

6. The compound of claim 1 , wherein R is an optionally-substituted heteroaryl group.

7. The compound of claim 1 , wherein R 5 and R 6 are independently selected from the group consisting of F, Cl, lower alkyl, OMe, CF 3 , NMe 2 , and imidazolylmethyl.

8. The compound of claim 1 , where the compound is

7-(5,6-dimethyl-2-(pyridin-2-yl)-1H-benzo[d]-imidazol-1-yl)quinazoline-2,4-diamine.

9. The compound of claim 1 , where the compound is

7-[5,6-dimethyl-2-(thiazol-2-yl)-1H-benzo[d]-imidazol-1-yl]quinazoline-2,4-diamine.

10. The compound of claim 1 , where the compound is

7-(5,6-dimethoxy-2-(thiazol-2-yl)-1H-benzo[d]imidazo-1-yl)quinazoline-2,4-diamine.

11. The compound of claim 1 , where the compound is

7-(2-(furan-2-yl)-5,6-dimethoxy-1H-benzo[d]-imidazol-1-yl)quinazoline-2,4-diamine.

12. The compound of claim 1 , where the compound is

7-(5,6-dimethyl-2-(thiophen-2-yl)-1H-benzo[d]-imidazol-1-yl)quinazoline-2,4-diamine.

13. The compound of claim 1 , where the seven to 10-membered heteroaryl ring is an eight to 10-membered heteroaryl ring.

14. A pharmaceutical composition comprising a compound of claim 1 and a pharmaceutically acceptable diluent or carrier.

15. A method of impeding growth of a bacterium by exposing the bacterium to a compound of claim 1 .

Assignments (6)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
NUNC PRO TUNC ASSIGNMENT Recorded Sep 3, 2015
From: TRIUS THERAPEUTICS LLC
To: MERCK SHARP & DOHME CORP.
Reel/Frame 036484/0796 →
CHANGE OF NAME Recorded Sep 2, 2015
From: TRIUS THERAPEUTICS, INC.
To: TRIUS THERAPEUTICS LLC
Reel/Frame 036528/0029 →
RELEASE OF SECURITY INTEREST Recorded Jul 24, 2015
From: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
To: TRIUS THERAPEUTICS, INC.; OPTIMER PHARMACEUTICALS, INC.
Reel/Frame 036178/0175 →
SECURITY AGREEMENT Recorded Nov 13, 2013
From: OPTIMER PHARMACEUTICALS, INC.; TRIUS THERAPEUTICS INC.
To: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
Reel/Frame 031628/0850 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 22, 2011
From: CHEN, ZHIYONG; CREIGHTON, CHRISTOPHER J.; CUNNINGHAM, MARK; FINN, JOHN; HILGERS, MARK; JUNG, MICHAEL; KOHNEN, LUCY AGUIRRE; LAM, THANH; LI, XIAOMING; STIDHAM, MARK; TARI, LES; TRZOSS, MICHAEL; ZHANG, JUNHU
To: TRIUS THERAPEUTICS, INC.
Reel/Frame 026634/0456 →