IP Library Granted Patent US 8,114,368
Granted Patent B2
US 8,114,368 · App. 13/169,187 · Granted Feb 14, 2012

Sorbents for coal combustion

Assignee: NOx II, Ltd.
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,114,368
App. No.
13/169,187
Granted
Feb 14, 2012
Kind
B2
Abstract

Sorbent compositions containing halogen and calcium are added to coal to mitigate the release of sulfur and/or other harmful elements, including mercury, into the environment during combustion of coal containing natural levels of mercury.

Claims (95)

1. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel, wherein the sorbent composition comprises a halogen compound and a source of calcium;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of calcium addition according to the measured level of sulfur.

2. A method according to claim 1 , wherein the sorbent composition comprises an inorganic source of bromine.

3. A method according to claim 1 , wherein the sorbent composition comprises an organic bromine compound.

4. A method according to claim 1 , wherein the sorbent composition comprises calcium oxide, calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium sulfate, calcium bisulfate, calcium nitrate, calcium nitrite, calcium acetate, calcium citrate, calcium phosphate, or calcium hydrogen phosphate.

5. A method according to claim 1 , wherein the sorbent composition comprises a calcium mineral.

6. A method according to claim 1 , wherein the sorbent composition comprises an organic calcium compound.

7. A method according to claim 1 , wherein the sorbent composition comprises a basic powder containing calcium.

8. A method according to claim 7 , wherein the basic powder is selected from portland cement, cement kiln dust, and lime kiln dust.

9. A method according to claim 1 , wherein the sorbent composition comprises an aluminosilicate clay.

10. A method according to claim 1 , wherein the sorbent composition comprises an iodine compound.

11. A method according to claim 10 , wherein the sorbent composition comprises an iodine containing salt of an alkali metal or an alkaline earth metal.

12. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises an organic halogen compound and a source of calcium.

13. A method according to claim 12 , comprising measuring sulfur in the combustion gases and adjusting the rate of calcium added according to the measured level of sulfur.

14. A method according to claim 12 , wherein the sorbent composition comprises calcium oxide, calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium sulfate, calcium bisulfate, calcium nitrate, calcium nitrite, calcium acetate, calcium citrate, calcium phosphate, or calcium hydrogen phosphate.

15. A method according to claim 12 , wherein the sorbent composition comprises a calcium mineral.

16. A method according to claim 12 , wherein the sorbent composition comprises an organic calcium compound.

17. A method according to claim 12 , wherein the sorbent composition comprises a basic powder containing calcium.

18. A method according to claim 17 , wherein the basic powder is selected from portland cement, cement kiln dust, and lime kiln dust.

19. A method according to claim 12 , wherein the sorbent composition comprises an aluminosilicate clay.

20. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises a halogen compound and a source of calcium selected from calcium oxide, calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium sulfate, calcium bisulfate, calcium nitrate, calcium nitrite, calcium acetate, calcium citrate, calcium phosphate, and calcium hydrogen phosphate.

21. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises a halogen compound and an organic calcium compound.

22. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises a halogen compound and a basic powder selected from the group consisting of Portland cement, cement kiln dust, and lime kiln dust.

23. A method according to claim 22 , comprising measuring sulfur in the combustion gases and adjusting the rate of calcium added according to the measured level of sulfur.

24. A method according to claim 22 , wherein the sorbent composition comprises an inorganic source of bromine.

25. A method according to claim 22 , wherein the sorbent composition comprises an organic bromine compound.

26. A method according to claim 22 , wherein the sorbent composition comprises an aluminosilicate clay.

27. A method according to claim 22 , wherein the sorbent composition comprises an iodine compound.

28. A method according to claim 27 , wherein the sorbent composition comprises an iodine containing salt of an alkali metal or an alkaline earth metal.

29. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises a halogen compound and an aluminosilicate clay.

30. A method according to claim 29 , wherein the sorbent composition comprises an inorganic source of bromine.

31. A method according to claim 29 , wherein the sorbent composition comprises an organic bromine compound.

32. A method according to claim 29 , wherein the sorbent composition further comprises calcium oxide, calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium sulfate, calcium bisulfate, calcium nitrate, calcium nitrite, calcium acetate, calcium citrate, calcium phosphate, or calcium hydrogen phosphate.

33. A method according to claim 29 , wherein the sorbent composition further comprises a calcium mineral.

34. A method according to claim 29 , wherein the sorbent composition further comprises an organic calcium compound.

35. A method according to claim 29 , wherein the sorbent composition further comprises a basic powder containing calcium.

36. A method according to claim 35 , wherein the basic powder is selected from portland cement, cement kiln dust, and lime kiln dust.

37. A method according to claim 29 , wherein the sorbent composition comprises an iodine compound.

38. A method according to claim 37 , wherein the sorbent composition comprises an iodine containing salt of an alkali metal or an alkaline earth metal.

39. A method for reducing emissions of mercury arising from combustion of mercury containing fuels in a fuel burning facility, the method comprising:

applying a sorbent composition onto the fuel;

delivering the fuel with the sorbent composition applied into a furnace of the facility;

combusting the fuel with the sorbent composition in the furnace to produce combustion gases and ash;

removing the ash from the combustion gases by capturing it in a particulate removal system disposed in a convective pathway of the facility downstream of the furnace;

measuring the level of mercury and/or sulfur remaining in the combustion gases after capture of the ash; and

adjusting the rate of sorbent addition according to the measured level of mercury and/or sulfur,

wherein the sorbent composition comprises an iodine compound and a source of calcium.

40. A method according to claim 39 , comprising measuring sulfur in the combustion gases and adjusting the rate of calcium added according to the measured level of sulfur.

41. A method according to claim 39 , wherein the sorbent composition comprises calcium oxide, calcium hydroxide, calcium carbonate, calcium bicarbonate, calcium sulfate, calcium bisulfate, calcium nitrate, calcium nitrite, calcium acetate, calcium citrate, calcium phosphate, or calcium hydrogen phosphate.

42. A method according to claim 39 , wherein the sorbent composition comprises a calcium mineral.

43. A method according to claim 39 , wherein the sorbent composition comprises an organic calcium compound.

44. A method according to claim 39 , wherein the sorbent composition comprises a basic powder containing calcium.

45. A method according to claim 44 , wherein the basic powder is selected from portland cement, cement kiln dust, and lime kiln dust.

46. A method according to claim 39 , wherein the sorbent composition further comprises an aluminosilicate clay.

47. A method according to claim 39 , wherein the sorbent composition comprises an iodine containing salt of an alkali metal or an alkaline earth metal.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 10, 2019
From: COMRIE, DOUGLAS C.
To: NOX II, LTD.
Reel/Frame 051233/0249 →
Continuity (6)
Continuation 12839154 · Jul 19, 2010
Continuation 12705196 · Feb 12, 2010
Continuation 12351191 · Jan 9, 2009
Continuation 11377528 · Mar 16, 2006
Provisional Application 60662911 · Mar 17, 2005
Related Publication 20110281222A1 · Nov 17, 2011