IP Library Granted Patent US 9,090,833
Granted Patent B2
US 9,090,833 · App. 13/202,239 · Granted Jul 28, 2015

Converting biomass to gaseous fuel hydrocarbons

Inventors: Maria Flytzani-Stephanopoulos (Winchester, MA); Branko Zugic (Somerville, MA); Brian Ricks (Cambridge, MA); Gregory Stephanopoulos (Winchester, MA)
Assignee: Tufts University
C10G3/45C07C1/2078C10G3/47C10G3/49C10G3/50C07C2521/00C07C2521/16C07C2521/18C07C2523/02C07C2523/14C07C2523/36C07C2523/42C07C2523/44C07C2523/46C07C2523/50C07C2523/52C07C2523/70C07C2523/72C07C2527/04C07C2529/00C07C2529/04C10G3/42C10G2300/1014
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Quick Facts
Patent No.
US 9,090,833
App. No.
13/202,239
Granted
Jul 28, 2015
Kind
B2
Abstract

A method for producing a C 1-5 hydrocarbon from a solution containing a C 2-6 carboxylic acid or a C 2-6 carboxylate which is derived from biomass by contacting the solution with a solid catalyst to decarboxylate the C 2-6 carboxylic acid or the C 2-6 carboxylate, thereby forming a C 1-5 hydrocarbon.

Claims (27)

1. A method of decarboxylating a C 2-6 carboxylic acid or a C 2-6 carboxylate, the method comprising:

providing a solution containing a C 2-6 carboxylic acid or a C 2-6 carboxylate that is derived from biomass; and

contacting the solution with a solid catalyst to form a C 1-5 hydrocarbon.

2. The method of claim 1 , wherein the contacting step is performed at 200° C.-500° C. and at 1-30 atm.

3. The method of claim 1 , wherein the contacting step is performed at 200-400° C. and at 1 atm.

4. The method of claim 2 , wherein the solution is carried by a gas to effect contact with the solid catalyst.

5. The method of claim 4 , wherein the gas is hydrogen, an inert gas, or a mixture thereof.

6. The method of claim 2 , wherein the solid catalyst includes a metal and a substrate.

7. The method of claim 6 , wherein the metal is Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, Au, or a combination thereof.

8. The method of claim 7 , wherein the metal is Co, Cu, Pt, Pd, Sn, Re, Au, or a combination thereof.

9. The method of claim 8 , wherein the metal is Au.

10. The method of claim 6 , wherein the solution is carried by a gas to effect contact with the solid catalyst.

11. The method of claim 10 , wherein the gas is hydrogen, an inert gas, or a mixture thereof.

12. The method of claim 6 , wherein the substrate is a metal oxide, a metal sulfide, a metal nitride, a metal carbide, a zeolite, a molecular sieve, a perovskite, a clay, or a combination thereof.

13. The method of claim 12 , wherein the metal is Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, Au, or a combination thereof.

14. The method of claim 6 , wherein the substrate is a carbonaceous material.

15. The method of claim 14 , wherein the metal is Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, Au, or a combination thereof.

16. The method of claim 14 , wherein the carbonaceous material is activated carbon, carbon black, graphite, charcoal, carbon nanotubes, carbon fibers, or a combination thereof.

17. The method of claim 14 , wherein the carbonaceous material includes carbon nanotubes.

18. The method of claim 17 , wherein the metal is Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, Au, or a combination thereof.

19. The method of claim 1 , wherein the biomass is a plant or a photosynthetic organism or a part thereof.

20. The method of claim 1 , wherein the biomass is a carbohydrate.

21. The method of claim 19 , wherein the solution is carried by a gas to effect contact with the solid catalyst and the contacting step is performed at 200° C.-500° C. and at 1-30 atm.

22. The method of claim 21 , wherein the solid catalyst includes a metal selected from the group consisting of Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, and Au.

23. The method of claim 1 , wherein the solution is an aqueous solution.

24. The method of claim 23 , wherein the solution is carried by a gas to effect contact with the solid catalyst and the contacting step is performed at 200° C.-500° C. and at 1-30 atm.

25. The method of claim 24 , wherein the solid catalyst includes a metal selected from the group consisting of Fe, Co, Ni, Mn, Ru, Rh, Pd, Re, Os, Ir, Pt, Sn, Cu, Ag, and Au.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jun 18, 2015
From: TUFTS UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 035948/0792 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 31, 2011
From: FLYTZANI-STEPHANOPOULOS, MARIA; ZUGIC, BRANKO; RICKS, BRIAN; STEPHANOPOULOS, GREGORY
To: TUFTS UNIVERSITY
Reel/Frame 027147/0785 →
Continuity (3)
Provisional Application 61154598 · Feb 23, 2009
Provisional Application 61176605 · May 8, 2009
Related Publication 20120035403A1 · Feb 9, 2012