IP Library Granted Patent US 9,140,657
Granted Patent B2
US 9,140,657 · App. 13/264,376 · Granted Sep 22, 2015

Detection of J-coupling using atomic magnetometer

Inventors: Micah P. Ledbetter (Oakland, CA); Charles W. Crawford (Albuquerque, NM); David E. Wemmer (Berkeley, CA); Alexander Pines (Berkeley, CA); Svenja Knappe (Boulder, CO); John Kitching (Boulder, CO); Dmitry Budker (El Cerrito, CA)
Assignees: The Regents of the University of California; The United States of America, as represented by the Secretary of Commerce, the National Institute of Standards and Technology
G01N24/08G01N24/087G01R33/26G01R33/46G01R33/445G01R33/4608G01R33/5605
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Quick Facts
Patent No.
US 9,140,657
App. No.
13/264,376
Granted
Sep 22, 2015
Kind
B2
Abstract

An embodiment of a method of detecting a J-coupling includes providing a polarized analyte adjacent to a vapor cell of an atomic magnetometer; and measuring one or more J-coupling parameters using the atomic magnetometer. According to an embodiment, measuring the one or more J-coupling parameters includes detecting a magnetic field created by the polarized analyte as the magnetic field evolves under a J-coupling interaction.

Claims (17)

1. A method of detecting a J-coupling comprising:

(a) providing an analyte in a detector cell adjacent to a vapor cell of an atomic magnetometer, the analyte being polarized, the detector cell and the vapor cell being housed in a magnetic shield that isolates the detector cell and the vapor cell in a static magnetic field;

(b) applying a magnetic field pulse to the analyte in the detector cell; and

(c) detecting a magnetic field generated by the analyte using the atomic magnetometer as a magnetization of the analyte evolves under one or more J-coupling interactions.

2. The method of claim 1 further comprising:

polarizing the analyte before operation (a).

3. The method of claim 2 wherein polarizing the analyte employs a polarization technique selected from a group consisting of thermalization in a magnetic field, spin-exchange optical pumping, para-hydrogen induced polarization, and dynamic nuclear polarization.

4. The method of claim 1 further comprising:

transporting the analyte to the detector cell.

5. The method of claim 1 wherein the one or more J-coupling interactions are selected from a group consisting of a heteronuclear scalar coupling, a homonuclear scalar coupling, and a combination thereof.

6. The method of claim 1 further comprising:

generating a graph of the one or more J-coupling interactions.

7. The method of claim 1 wherein a magnitude of the static magnetic field is less than about 2.5 nanotesla.

8. The method of claim 1 wherein a larmor precession frequency of the analyte is less than about 100 mHz in the static magnetic field.

9. The method of claim 1 wherein a magnitude of the static magnetic field is less than about 100 microtesla.

10. The method of claim 1 wherein the magnetic field pulse is applied by applying a pulse of DC current to coils positioned in the magnetic shield.

11. The method of claim 1 wherein a magnitude of the static magnetic field is less than about 1 millitesla.

Assignments (3)
CONFIRMATORY LICENSE Recorded Apr 28, 2022
From: UNIVERSITY OF CALIF-LAWRENC BERKELEY LAB
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 059765/0504 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 15, 2015
From: KITCHING, JOHN
To: GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF COMMERCE, THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY
Reel/Frame 035425/0488 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2012
From: LEDBETTER, MICAH P.; BUDKER, DMITRY; CRAWFORD, CHARLES W.; WEMMER, DAVID E.; PINES, ALEXANDER
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 027964/0312 →
Continuity (2)
Provisional Application 61168795 · Apr 13, 2009
Related Publication 20120176130A1 · Jul 12, 2012