IP Library Granted Patent US 9,180,413
Granted Patent B2
US 9,180,413 · App. 13/288,595 · Granted Nov 10, 2015

One-step synthesis of mesoporous pentasil zeolite with single-unit-cell lamellar structural features

Inventors: Michael Tsapatsis (Minneapolis, MN); Xueyi Zhang (Minneapolis, MN)
Assignee: Regents of the University of Minnesota
B01D67/0051B01D71/028B01J29/0308B01J29/041B01J29/40B01J35/10C01B37/005C01B37/02C01B39/36C01B39/40B01D2323/24B01J29/035B01J35/002B01J35/065
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Quick Facts
Patent No.
US 9,180,413
App. No.
13/288,595
Granted
Nov 10, 2015
Kind
B2
Abstract

A method for making a pentasil zeolite material includes forming an aqueous solution that includes a structure directing agent and a silica precursor; and heating the solution at a sufficient temperature and for sufficient time to form a pentasil zeolite material from the silica precursor, wherein the structure directing agent includes a quaternary phosphonium ion.

Claims (8)

1. A material, comprising:

a plurality of zeolite particles each having a unit-cell structure that is lamellar and has a single unit-cell thickness in at least one dimension,

wherein the zeolite particles are intergrown to define pores that extend between the intergrown zeolite particles and so that the lamellar unit cells intersect perpendicular to one another, and

wherein the plurality of zeolite particles are either MFI zeolite particles or pentasil zeolite particles.

2. The material of claim 1 , wherein the pores have at least one dimension of 10 nm or less.

3. The material of claim 1 , wherein the lamellar single-unit-cell structure has a dimension of 2 nm or less.

4. The material of claim 1 , wherein the material has an X-ray diffraction pattern corresponding to the traces shown in FIG. 1( c ).

5. A composite material, comprising the material of claim 1 , wherein the composite material is a film or a coating.

Assignments (2)
CONFIRMATORY LICENSE Recorded Oct 22, 2020
From: UNIVERSITY OF MINNESOTA
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 054176/0205 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2012
From: TSAPATSIS, MICHAEL; ZHANG, XUEYI
To: REGENTS OF THE UNIVERSITY OF MINNESOTA
Reel/Frame 027561/0959 →
Continuity (2)
Provisional Application 61531349 · Sep 6, 2011
Related Publication 20130059722A1 · Mar 7, 2013