IP Library Granted Patent US 8,858,657
Granted Patent B1
US 8,858,657 · App. 13/333,479 · Granted Oct 14, 2014

Direct conversion of algal biomass to biofuel

Inventors: Shuguang Deng (Las Cruces, NM); Prafulla D. Patil (Las Cruces, NM); Veera Gnaneswar Gude (Klamath Falls, OR)
Assignee: Arrowhead Center, Inc.
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Quick Facts
Patent No.
US 8,858,657
App. No.
13/333,479
Granted
Oct 14, 2014
Kind
B1
Abstract

A method and system for providing direct conversion of algal biomass. Optionally, the method and system can be used to directly convert dry algal biomass to biodiesels under microwave irradiation by combining the reaction and combining steps. Alternatively, wet algae can be directly processed and converted to fatty acid methyl esters, which have the major components of biodiesels, by reacting with methanol at predetermined pressure and temperature ranges.

Claims (11)

1. A single-step method of converting wet algae biomass to biodiesel comprising:

reacting the wet algae biomass with a non-catalytic supercritical methanol; and

the reaction resulting in the biodiesel.

2. The method of claim 1 wherein a drying step is not performed.

3. The method of claim 1 wherein the reacting step is performed at a constant predetermined pressure of about 1000 psi to about 1500 psi.

4. The method of claim 1 wherein the reacting step is performed at a constant predetermined temperature of about 200° C. to about 300° C.

5. The method of claim 1 wherein the wet algae biomass to methanol ratio is about 1:2 to about 1:20 (wt/vol.).

6. The method of claim 1 wherein a separate extraction step is not performed.

7. The method of claim 1 comprising reacting the wet algae biomass with the non-catalytic supercritical methanol in the presence of nitrogen.

8. The method of claim 1 wherein the reaction takes approximately 5 to 45 minutes.

9. The method of claim 1 wherein the reacting step comprises simultaneously extracting and transesterification of the wet algae biomass.

Assignments (3)
CONFIRMATORY LICENSE Recorded Mar 7, 2018
From: NEW MEXICO STATE UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 045518/0950 →
CONFIRMATORY LICENSE Recorded Feb 24, 2014
From: NEW MEXICO STATE UNIVERSITY-ARROWHEAD CENTER
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 032399/0920 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2012
From: DENG, SHUGUANG; PATIL, PRAFULLA D.; GUDE, VEERA GNANESWAR
To: ARROWHEAD CENTER, INC.
Reel/Frame 027814/0357 →
Continuity (2)
Provisional Application 61426333 · Dec 22, 2010
Provisional Application 61426305 · Dec 22, 2010