IP Library Patent Application 13356574
Patent Application
App. No. 13/356,574

RARE EARTH REMOVAL OF PHOSPHORUS-CONTAINING MATERIALS

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Patent No.
US None
App. No.
13/356,574
Abstract

This disclosure relates generally to methods and rare earth-containing additives for removing inorganic and organic phosphorus-containing target materials.

Claims (33)

1 . A method, comprising:

contacting an aqueous medium comprising a phosphorus-containing target material with a rare earth-containing additive to remove at least a portion of the phosphorus-containing target material from the aqueous medium to form a treated aqueous medium, wherein the phosphorus-containing target material comprises one or more of phosphoric acid, phosphinate, non-fluoridated phosphonates, phosphonic acid, phosphinic acid, phosphonite, thiophosphate, thiophosphyoryl amide, and phosphatidylcholine.

2 . The method of claim 1 , wherein the rare earth-containing additive is primarily in the form of cerium (IV), cerium (III) or a mixture of cerium (IV) and cerium (III).

3 . The method of claim 1 , wherein the contacting step comprises the sub-steps:

contacting the aqueous medium with an oxidizing agent to oxidize the phosphorus-containing target material to form an oxidized phosphorus-containing target material, the oxidized phosphorus-containing target mater having one or both of a different structure and composition than the phosphorus-containing target material; and

thereafter contacting, in the aqueous medium, the rare earth-containing additive with the oxidized phosphorus-containing target material to remove the oxidized phosphorus-containing target material.

4 . The method of claim 1 , wherein the contacting step comprises the sub-steps:

contacting the aqueous medium with a reducing agent to reduce the phosphorus-containing target material to form a reduced phosphorus-containing target material, the reduced phosphorus-containing target material having one or both of a different structure and composition than the phosphorus-containing target material; and

thereafter contacting, in the aqueous medium, the rare earth-containing additive with the reduced target phosphorus-containing target material to remove the reduced phosphorus-containing target material.

5 . The method of claim 1 , wherein the contacting step comprises the sub-steps:

contacting the aqueous medium with a base and/or base equivalent to convert the phosphorus-containing target material to a primary species different from the phosphorus-containing target material; and

thereafter contacting, in the aqueous medium, the rare earth-containing additive with the primary species to remove the primary species.

6 . The method of claim 1 , wherein the contacting step comprises the sub-steps:

contacting the aqueous medium with an acid and/or acid equivalent to convert the phosphorus-containing target material to a primary species different from the phosphorus-containing target material; and

thereafter contacting, in the aqueous medium, the rare earth-containing additive with the primary species to remove the primary species.

7 . The method of claim 1 , wherein the rare earth-containing additive is water-soluble.

8 . The method of claim 1 , wherein the rare earth-containing additive is water-insoluble.

9 . The method of claim 1 , wherein the phosphorus-containing target material is selected from the group consisting essentially of phosphoric acid, phosphinate, phosphinite, non-fluoridated phosphonates, phosphonic acid, phosphinic acid, phosphonite, thiophosphate, and thiophosphyoryl ester.

10 . The method of claim 1 , wherein the phosphorus-containing target material comprises phosphatidylcholine.

11 . The method of claim 1 , wherein the phosphorus-containing target material comprises a thiophosphyoryl amide.

12 . A composition, comprising:

an aqueous medium,

a rare earth-containing additive,

a phosphorus-containing target material comprising one or more of one or more of phosphoric acid, phosphinate, phosphinite, non-fluoridated phosphonates, phosphonic acid, phosphinic acid, phosphonite, thiophosphate, thiophosphyoryl ester, thiophosphyoryl amide, and phosphatidylcholine, and

a target-laden rare earth composition formed by the rare earth-containing additive and the phosphorus-containing target material.

13 . The composition of claim 12 , wherein the rare earth-containing additive comprises primarily cerium and wherein the target-laden rare earth composition is a complex formed by the rare earth-containing additive and phosphorus-containing target material.

14 . The composition of claim 12 , wherein the rare earth-containing additive comprises primarily cerium and wherein the target-laden rare earth composition is formed by sorption of the phosphorus-containing target material by the rare earth-containing additive.

15 . The composition of claim 12 , wherein the rare earth-containing additive comprises primarily cerium and wherein the target-laden rare earth composition is formed by a chemical reaction between the phosphorus-containing target material and the rare earth-containing additive.

16 . The composition of claim 12 , wherein the rare earth-containing additive is water-soluble.

17 . The composition of claim 12 , wherein the rare earth-containing additive is water-insoluble.

18 . The composition of claim 12 , wherein the phosphorus-containing target material is selected from the group consisting essentially of phosphoric acid, phosphinate, phosphinite, non-fluoridated phosphonates, phosphonic acid, phosphinic acid, phosphonite, thiophosphate, and thiophosphyoryl ester.

19 . The composition of claim 12 , wherein the phosphorus-containing target material comprises phosphatidylcholine.

20 . The composition of claim 12 , wherein the phosphorus-containing target material comprises a thiophosphyoryl amide.

Assignments (2)
SECURITY AGREEMENT Recorded Jun 11, 2012
From: MOLYCORP MINERALS, LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 028355/0440 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2012
From: HASSLER, CARL; BURBA, JOHN; CABLE, ROBERT
To: MOLYCORP MINERALS, LLC
Reel/Frame 027871/0705 →