IP Library Granted Patent US 8,901,914
Granted Patent B2
US 8,901,914 · App. 13/362,220 · Granted Dec 2, 2014

High throughput label free nanoparticle detection and size assay

Inventors: Jean-Luc Fraikin (Boulder, CO); Andrew N. Cleland (Santa Barbara, CA)
Assignee: The Regents of the University of California
G01N27/06G01N2015/1087G01N15/1209G01N2015/0092G01N2015/0038G01N2015/1236G01N2015/1062
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Quick Facts
Patent No.
US 8,901,914
App. No.
13/362,220
Granted
Dec 2, 2014
Kind
B2
Abstract

The present invention reports a novel microfluidic analyzer for the high-throughput, label-free measurement of particles suspended in a fluid. The present invention employs the resistive pulse technique (RPT) which affords very high electrical bandwidth for the device, which surpasses that of currently available systems and devices. Further, devices in accordance with the present invention are fabricated with very simple microfabrication technologies, making the present invention more cost efficient and easier to manufacture than currently available devices.

Claims (25)

1. An apparatus for detecting particles in a fluid, comprising:

a first electrode;

a sensing electrode;

a fluid resistor between the first electrode and the sensing electrode;

a second electrode; and

a constriction between the sensing electrode and the second electrode, wherein a bias voltage is applied between the first electrode and the second electrode to create a current through the fluid, such that a size and a number of a particle is sensed by a change in voltage sensed at the sensing electrode.

2. The apparatus of claim 1 , further comprising a filter element such that the particles are sensed by the apparatus and undesired particles are blocked by the filter element from being sensed by the apparatus.

3. The apparatus of claim 1 , wherein a bandwidth of the apparatus is greater than 100 kHz.

4. The apparatus of claim 1 , wherein the fluid resistor and the constriction comprise a voltage divider in the apparatus.

5. The apparatus of claim 1 , wherein the sensing electrode is fabricated using lithographic techniques.

6. The apparatus of claim 1 , wherein the bias voltage is a constant voltage.

7. The apparatus of claim 1 , wherein the apparatus senses different sizes of particles in the fluid.

8. The apparatus of claim 1 , further comprising a plurality of constrictions.

9. The apparatus of claim 1 , further including an integrated filter element.

10. A method of detecting particles in a fluid, comprising:

applying a bias voltage between a first electrode and a second electrode;

filtering the fluid prior to entering any smaller constrictions;

restricting the fluid in a constriction between the first electrode and the second electrode; and

sensing a change in voltage at a point between the constriction and the second electrode, wherein the change in voltage is proportional to a volume filling fraction of a particle in the constriction.

11. The method of claim 10 , wherein a bandwidth of the apparatus is greater than 100 kHz.

12. The method of claim 10 , further comprising creating a voltage divider in the apparatus using the constriction.

13. The method of claim 10 , wherein the sensing electrode is fabricated using lithographic techniques.

14. The method of claim 10 , wherein the bias voltage is a constant voltage.

15. The method of claim 10 , further comprising sensing different sizes of particles in the fluid.

16. The method of claim 10 , further comprising constricting the fluid in a plurality of constrictions.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jan 12, 2015
From: UNIVERSITY OF CALIFORNIA SANTA BARBARA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 034750/0887 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 16, 2012
From: FRAIKIN, JEAN-LUC; CLELAND, ANDREW N.
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 027877/0677 →
CONFIRMATORY LICENSE Recorded Feb 15, 2012
From: UNIVERSITY OF CALIFORNIA SANTA BARBARA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 027705/0573 →
Continuity (2)
Provisional Application 61437942 · Jan 31, 2011
Related Publication 20120194167A1 · Aug 2, 2012