IP Library Granted Patent US 8,920,764
Granted Patent B2
US 8,920,764 · App. 13/370,076 · Granted Dec 30, 2014

Graphene composition, method of forming a graphene composition and sensor system comprising a graphene composition

Inventors: Alexander Star (Pittsburgh, PA); Narasimha Harindra Vedala (Pittsburgh, PA); Gregg Peter Kotchey (Pittsburgh, PA)
Assignee: University of Pittsburgh—Of the Commonwealth System of Higher Education
G01N27/127B82Y30/00B82Y40/00C01B31/0476C01B31/0484C12P3/00
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Quick Facts
Patent No.
US 8,920,764
App. No.
13/370,076
Granted
Dec 30, 2014
Kind
B2
Abstract

A method of forming a composition includes oxidation of graphene oxide to form holey graphene oxide having defects therein and reduction of the holey graphene oxide.

Claims (13)

1. A method of forming a composition, comprising:

oxidation of graphene oxide sheets to form holey graphene oxide sheets having holes in the basal plane thereof; and

reduction of the holey graphene oxide sheets to provide a network of interconnected graphene nanoribbons.

2. The method of claim 1 wherein the oxidation of graphene oxide sheets comprises enzymatic oxidation of graphene oxide sheets.

3. The method of claim 2 wherein enzymatic oxidation occurs in the presence of a peroxidase and a substrate for the peroxidase.

4. The method of claim 3 wherein the peroxidase is at least one of horseradish peroxidase, myeloperoxidase, cytochrome c peroxidase, cytochrome P450, eosinophil peroxidase, glutathione peroxidase, lactoperoxidase, thyroid peroxidase, deiodinase, lignin peroxidase, dehaloperoxidase or manganese peroxidase.

5. The method of claim 4 wherein the substrate includes hydrogen peroxide and organic hydroperoxide substrates.

6. The method of claim 3 wherein reduction occurs via reaction with a reducing agent or via heating.

7. The method of claim 6 wherein the reducing agent comprises hydrazine hydrate.

8. The method of claim 2 wherein properties of the network of interconnected graphene nanoribbons are controlled via reactions conditions.

9. The method of claim 1 wherein the oxidation of graphene oxide sheets is carried out in a temperature range of approximately 20° C. to 90° C.

10. The method of claim 1 wherein the oxidation of graphene oxide sheets is carried out in a temperature range of approximately 20° C. to 40° C.

11. The method of claim 1 wherein the oxidation of graphene oxide sheets is carried out at a pH in the range of approximately 3.0 to 10.0.

Assignments (2)
CONFIRMATORY LICENSE Recorded Apr 13, 2012
From: UNIVERSITY OF PITTSBURGH - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 028040/0202 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2012
From: STAR, ALEXANDER; VEDALA, NARASIMHA HARINDRA; KOTCHEY, GREGG PETER
To: PITTSBURGH, UNIVERSITY OF - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
Reel/Frame 027905/0885 →
Continuity (2)
Provisional Application 61441925 · Feb 11, 2011
Related Publication 20130040283A1 · Feb 14, 2013