IP Library Granted Patent US 9,213,106
Granted Patent B2
US 9,213,106 · App. 13/449,607 · Granted Dec 15, 2015

Method of measuring luminescence of a material

Inventor: Steven D. Miller (Richland, WA)
Assignee: BATTELLE MEMORIAL INSTITUTE
G01T1/11G01T1/10G01T1/105G01J1/58G01N21/64G21K5/00
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Quick Facts
Patent No.
US 9,213,106
App. No.
13/449,607
Granted
Dec 15, 2015
Kind
B2
Abstract

A method of measuring luminescence of a material is disclosed. The method includes applying a light source to excite an exposed material. The method also includes amplifying an emission signal of the material. The method further includes measuring a luminescent emission at a fixed time window of about 10 picoseconds to about 10 nanoseconds. The luminescence may be radio photoluminescence (RPL) or optically stimulated luminescence (OSL).

Claims (24)

1. A method of measuring luminescence of a material, comprising:

a. applying a light source to excite an exposed, irradiated material;

b. amplifying an emission signal of the material; and

c. measuring a luminescent emission at a fixed time window of about 10 picoseconds to about 10 nanoseconds, wherein an excitation pulse of the light source is an approximately 10 picosecond to 300 picosecond wide pulse, and wherein the material is an alkali halide, alkali earth halide, glass, or combinations thereof.

2. The method of claim 1 wherein the luminescence is one of the following: radio photoluminescence (RPL) and optically stimulated luminescence (OSL).

3. The method of claim 1 wherein the light source is one of the following: a laser, a light-emitting diode (LED), and a flash lamp.

4. The method of claim 1 further comprising filtering to isolate a desired range of emission wavelengths.

5. The method of claim 1 wherein an excitation pulse of the light source is shorter than a decay time constant of the material.

6. The method of claim 5 wherein the decay time constant is a sub-nano-second decay constant.

7. The method of claim 6 wherein the decay time constant is in the range of 100 to 300 picoseconds.

8. The method of claim 1 wherein a train of light pulses is applied repeatedly to quantify a radiation dose imparted to the material.

9. The method of claim 1 wherein the alkali halide material is lithium fluoride.

10. The method of claim 9 wherein the alkali halide material is combined with a polymer.

11. The method of claim 1 wherein the alkali halide material is at least one of the following: sodium fluoride, a bromide, a chloride, and an iodide.

12. The method of claim 11 wherein the alkali halide material is combined with a polymer.

13. The method of claim 1 wherein the material is in the size range of approximately 10 nanometers to approximately 500 micrometers.

14. A method of altering properties of a luminescent material, comprising:

a. preparing the luminescent material to a size range of approximately 1 to 2,000 nanometers, wherein the luminescent material is an alkali halide, alkali earth halide, glass, or combinations thereof;

b. irradiating the material; and

c. exciting the irradiated material with a pico-second pulse from a light source to measure at least one of the following altered properties of the material: excitation curves, emission curves, and a time constant of a luminescent emission of the material.

15. The method of claim 14 wherein the alkali halide material is lithium fluoride.

16. The method of claim 14 wherein the alkali halide material is at least one of the following: sodium fluoride, a bromide, a chloride, and an iodide.

17. The method of claim 14 wherein the light source is one of the following: a laser, a LED, and a flash lamp.

18. The method of claim 14 wherein the time constant includes more than one time constant.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 22, 2012
From: BATTELLE MEMORIAL INSTITUTE, PACIFIC NORTHWEST DIVISION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 028246/0540 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 18, 2012
From: MILLER, STEVEN D.
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 028064/0895 →
Continuity (2)
Provisional Application 61494796 · Jun 8, 2011
Related Publication 20120313011A1 · Dec 13, 2012