IP Library Granted Patent US 8,444,045
Granted Patent B2
US 8,444,045 · App. 13/465,710 · Granted May 21, 2013

Joining of parts via magnetic heating of metal aluminum powders

Inventor: Ian Baker (Etna, NH)
Assignee: The Trustees of Dartmouth College
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Quick Facts
Patent No.
US 8,444,045
App. No.
13/465,710
Granted
May 21, 2013
Kind
B2
Abstract

A method of joining at least two parts includes steps of dispersing a joining material comprising a multi-phase magnetic metal-aluminum powder at an interface between the at least two parts to be joined and applying an alternating magnetic field (AMF). The AMF has a magnetic field strength and frequency suitable for inducing magnetic hysteresis losses in the metal-aluminum powder and is applied for a period that raises temperature of the metal-aluminum powder to an exothermic transformation temperature. At the exothermic transformation temperature, the metal-aluminum powder melts and resolidifies as a metal aluminide solid having a non-magnetic configuration.

Claims (39)

1. A product comprising at least two parts, said at least two parts being joined together using a joining method, said joining method comprising

(a) dispersing a joining material at an interface between said at least two parts, wherein said joining material comprises a metal-aluminum powder; and

(b) applying an alternating magnetic field (AMF) having a magnetic field strength and frequency that induce magnetic hysteresis losses in said metal-aluminum powder for a period that raises the temperature of said metal-aluminum powder to an exothermic transformation temperature,

(c) allowing said metal-aluminum powder to melt and resolidify as a metal aluminide solid, thereby joining said at least two part, wherein said metal aluminide solid has a non-magnetic configuration.

2. The product of claim 1 , wherein the joining material is a microcrystalline material.

3. The product of claim 1 , wherein the joining material is a nanocrystalline material.

4. The product of claim 1 , wherein particles of the metal-aluminum powder have diameters of between 1 μm and 25 μm.

5. The product of claim 1 , wherein the metal aluminide is according to a formula:

( x )M-( y )Al,

wherein M is a metal or combination of metals selected from Fe, Ni and Co;

x ranges from 55 to 80 atomic percent; and

y ranges from 20 to 45 atomic percent.

6. A method for joining at least two parts to make the product of claim 1 , said method comprising:

dispersing a joining material comprising a metal-aluminum powder at an interface between said at least two parts to be joined; and

applying an alternating magnetic field (AMF) having a magnetic field strength and frequency that induce magnetic hysteresis losses in the metal-aluminum powder for a period that raises the temperature of the metal-aluminum powder to an exothermic transformation temperature where the metal-aluminum powder melts and resolidifies as a metal aluminide solid having a non-magnetic configuration.

7. The method of claim 6 , wherein the joining material further comprises a solder.

8. The method of claim 6 , wherein the joining material is disposed within a polymer.

9. The method of claim 6 , wherein the joining material is disposed within a slurry.

10. The method of claim 6 , wherein the AMF has a magnetic field strength ranging from 50 Oe to 2000 Oe.

11. The method of claim 6 , wherein the AMF has a frequency ranging from 25 KHz to 100 MHz.

12. The method of claim 6 , wherein the period is in a range between 5 seconds and 100 seconds.

13. The method of claim 6 , wherein the at least two parts are joined at a non-planar interface.

14. The method of claim 6 , wherein the non-magnetic configuration of the metal aluminide is a B2 structure.

15. The method of claim 6 , wherein the metal aluminide is according to a formula:

( x )M-( y )Al,

wherein M is a metal or combination of metals selected from Fe, Ni and Co;

x ranges from 55 to 80 atomic percent; and

y ranges from 20 to 45 atomic percent.

16. The method of claim 15 , wherein x is 60 atomic percent and y is 40 atomic percent.

17. The method of claim 6 , wherein the metal aluminide is selected from the group consisting of iron aluminide, nickel aluminide, cobalt aluminide, ternary intermetallic compounds comprising Al and two metals selected from Fe, Ni and Co, quaternary intermetallic compounds comprising Fe, Ni, Co and Al, and physical mixtures thereof.

18. The method of claim 6 , wherein the metal aluminide is iron aluminide.

19. The method of claim 18 , wherein the iron aluminide comprises 60 atomic percent iron and 40 atomic percent aluminum.

20. The method of claim 6 , wherein the at least two parts form a combination selected from polymer-polymer, semiconductor-semiconductor, ceramic-ceramic, polymer-metal, polymer-semiconductor, polymer-ceramic, metal-semiconductor, metal-ceramic and semiconductor-ceramic.

21. The method of claim 6 , wherein the at least two parts form a combination selected from semiconductor-semiconductor, ceramic-ceramic, metal-semiconductor, metal-ceramic and semiconductor-ceramic.

22. The method of claim 6 , wherein the at least two parts form a combination selected from ceramic-ceramic and metal-ceramic.

23. The method of claim 6 , wherein particles of the metal-aluminum powder have diameters of between 6 μm and 25 μm.

24. The method of claim 6 , wherein particles of the metal-aluminum powder have diameters between 5 μm and 10 μm.

25. The method of claim 6 , wherein the step of dispersing comprises painting, silk screening or dipping.

26. The method of claim 6 , wherein the joining material is a microcrystalline material.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 16, 2015
From: DARTMOUTH COLLEGE
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 035168/0978 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2012
From: BAKER, IAN
To: THE TRUSTREES OF DARTMOUTH COLLEGE
Reel/Frame 028862/0434 →
Continuity (3)
Continuation In Part 12993779
Substitution 61054380 · May 19, 2008
Related Publication 20120315493A1 · Dec 13, 2012