IP Library Granted Patent US 8,580,788
Granted Patent B2
US 8,580,788 · App. 13/479,622 · Granted Nov 12, 2013

Opioid antagonists

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Quick Facts
Patent No.
US 8,580,788
App. No.
13/479,622
Granted
Nov 12, 2013
Kind
B2
Abstract

Certain quinolizidine and octahydropyridopyrazine compounds, pharmaceutical compositions, and methods of their use, inter alia, as opioid receptor antagonists are disclosed.

Claims (49)

1. A compound of formula I:

wherein:

R 1 is —C(═O)NR 6 R 7 ;

R 2 and R 3 are each independently alkyl or alkenyl;

R 4 is H, alkyl, cycloalkyl, cycloalkylalkyl, aryl, heteroaryl, aralkyl, alkylaralkyl, or heteroarylalkyl;

X is NR 5 ;

R 5 is —C(═O)R 8b ;

R 6 is H, alkyl, cycloalkyl, alkylcycloalkyl, or aralkyl;

R 7 is H, alkyl, aralkyl, or aryl;

R 8b is H, alkyl, cycloalkyl, cycloalkylalkyl, heteroaryl, heteroarylalkyl, aralkyl, or aryl;

m is 1; and

n is 1,

or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 , wherein R 6 is H or alkyl.

3. The compound of claim 2 , wherein R 7 is H or alkyl.

4. The compound of claim 1 , having the structure of formula IIa:

wherein

R 6 and R 7 are each independently alkyl;

R 2 and R 3 are each independently alkyl; and

R 8b is heteroaryl, heteroarylalkyl, aralkyl, or aryl.

5. The compound according to claim 4 , having the structure of formula IIb:

6. The compound of claim 4 , wherein R 6 and R 7 are each independently methyl.

7. The compound of claim 4 , wherein R 8b is aralkyl or aryl.

8. The compound of claim 7 , wherein R 8b is aryl and R 6 and R 7 are each independently methyl.

9. The compound of claim 8 , wherein R 8b is aryl substituted with halo.

10. The compound of claim 9 , wherein R 8b is aryl substituted with fluoro.

11. A method for binding delta opioid receptors, comprising the step of: contacting one or more delta opioid receptors with a compound of formula (I) or a salt thereof in an amount effective to bind to the opioid receptor,

wherein:

R 1 is —C(═O)NR 6 R 7 ;

R 2 and R 3 are each independently alkyl or alkenyl;

R 4 is H, alkyl, cycloalkyl, cycloalkylalkyl, aryl, heteroaryl, aralkyl, alkylaralkyl, or heteroarylalkyl;

X is NR 5 ;

R 5 is —C(═O)R 8b ;

R 6 is H, alkyl, cycloalkyl, alkylcycloalkyl, or aralkyl;

R 7 is H, alkyl, aralkyl, or aryl;

R 8b is H, alkyl, cycloalkyl, cycloalkylalkyl, heteroaryl, heteroarylalkyl, aralkyl, or aryl;

m is 1; and

n is 1.

12. The method of claim 11 , wherein the compound has the structure of formula IIa:

wherein

R 6 and R 7 are each independently alkyl;

R 2 and R 3 are each independently alkyl; and

R 8b is heteroaryl, heteroarylalkyl, aralkyl, or aryl.

13. The method of claim 12 , wherein the compound has the structure of formula IIb:

14. The method of claim 12 , wherein R 6 and R 7 are each independently methyl.

15. The method of claim 12 , wherein R 8b is aralkyl or aryl.

16. The method of claim 15 , wherein R 8b is aryl and R 6 and R 7 are each independently methyl.

17. The method of claim 16 , wherein R 8b is aryl substituted with halo.

18. The method of claim 17 , wherein R 8b is aryl substituted with fluoro.

Assignments (4)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
RELEASE OF SECURITY INTEREST Recorded Jul 24, 2015
From: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
To: CALIXA THERAPEUTICS, INC.; ADOLOR CORPORATION; CUBIST PHARMACEUTICALS, INC.
Reel/Frame 036180/0070 →
NUNC PRO TUNC ASSIGNMENT Recorded Jul 9, 2015
From: ADOLOR CORPORATION
To: MERCK SHARP & DOHME CORP.
Reel/Frame 036046/0153 →
SECURITY AGREEMENT Recorded Nov 20, 2012
From: CUBIST PHARMACEUTICALS, INC.; ADOLOR CORPORATION; CALIXA THERAPEUTICS, INC.; CUBIST PHARMACEUTICALS HOLDINGS, INC.; CUBIST PHARMACEUTICALS U.S.
To: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
Reel/Frame 029339/0669 →