IP Library Granted Patent US 9,242,241
Granted Patent B2
US 9,242,241 · App. 13/501,811 · Granted Jan 26, 2016

Copper containing levyne molecular sieve for selective reduction of NOx

Inventors: Ivor Bull (Hopewell Junction, NY); Ulrich Müller (Neustadt, DE); Bilge Yilmaz (New York, NY)
Assignee: BASE SE
B01J35/002B01D53/9409B01J29/064B01J29/072B01J29/70B01J29/72B01J29/76B01J29/83B01J29/84B01J37/0009B01D2255/20761B01D2255/50B01D2257/402B01D2257/404B01D2257/406B01D2258/012B01J29/85B01J37/10B01J2229/186B01J2229/36Y02C20/10
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Quick Facts
Patent No.
US 9,242,241
App. No.
13/501,811
Granted
Jan 26, 2016
Kind
B2
Abstract

Aspects of the present invention relates to a copper containing Levyne molecular sieve having a silica to alumina mole ratio less than 30 and a Cu:Al atomic ratio less than 0.45, wherein the Levyne molecular sieve retains at least 60% of its surface area after exposure to a temperature of from about 750° C. to about 950° C. in the present of up to 10 volume percent water vapor for a time ranging from about 1 to about 48 hours.

Claims (9)

1. A copper-containing Levyne molecular sieve having a silica to alumina mole ratio of from about 15 to about 26 and a Cu:Al atomic ratio of from about 0.20 to about 0.45.

2. The copper-containing Levyne molecular sieve of claim 1 , wherein the silica to alumina mole ratio is less than 23.

3. The copper-containing Levyne molecular sieve of claim 1 , wherein the atomic ratio of copper to proton is less than 7.

4. The copper-containing Levyne molecular sieve of claim 1 , wherein moles Cu per 100 g zeolite (calculated as moles) are more than 0.01.

5. The copper-containing Levyne molecular sieve of claim 1 , wherein Cu content of the copper containing Levyne molecular sieve, calculated as CuO, is from about 2 to about 4 wt.-% based on the total weight of the calcined Levyne molecular sieve.

6. The copper-containing Levyne molecular sieve of claim 1 , wherein the Cu:Al atomic ratio is from about 0.2 to about 0.4.

7. The copper-containing Levyne molecular sieve of claim 1 , wherein the Levyne molecular sieve is a ZSM-45.

8. The copper-containing Levyne molecular sieve of claim 1 , wherein the Levyne molecular sieve is a Nu-3.

9. A catalyst containing the copper-containing Levyne molecular sieve of claim 1 disposed on a substrate.

Assignments (2)
MERGER AND CHANGE OF NAME Recorded Jan 14, 2016
From: BASF CATALYSTS LLC; BASF CORPORATION
To: BASF CORPORATION
Reel/Frame 037489/0678 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 30, 2012
From: BULL, IVOR; MULLER, ULRICH; YILMAZ, BILGE
To: BASF SE; BASF CATALYSTS LLC
Reel/Frame 028286/0766 →
Continuity (2)
Provisional Application 61251350 · Oct 14, 2009
Related Publication 20120208691A1 · Aug 16, 2012