IP Library Granted Patent US 9,206,193
Granted Patent B2
US 9,206,193 · App. 13/575,505 · Granted Dec 8, 2015

Substituted norindenoisoquinolines, syntheses thereof, and methods of use

Inventors: Mark S. Cushman (West Lafayette, IN); Yunlong Song (Shanghai, CN)
Assignee: PURDUE RESEARCH FOUNDATION
C07D493/04C07D221/18C07D491/04
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Quick Facts
Patent No.
US 9,206,193
App. No.
13/575,505
Granted
Dec 8, 2015
Kind
B2
Abstract

Described herein are substituted norindenoisoquinoline compounds, and pharmaceutical compositions and formulations comprising the norindenoisoquinoline compounds. Also described herein are methods for using the compounds for the treatment and/or prevention of topoisomerase mediated diseases, such as cancer.

Claims (16)

1. A process for preparing a compound of the formula

or a pharmaceutically acceptable salt thereof,

wherein

R is dimethylamino, pyrrolidin-1-yl, 1H-imidazolyl, 4-methylpiperazin-1-yl, 4-morpholino, or N,N,N′-trimethylethylenediamino;

the process comprising the step of treating a compound of formula

with a compound of formula

and an acid; wherein

R 10 is alkyl; and

P is an aldehyde or protected acetal.

2. The process of claim 1 , wherein said acid is HCl.

3. A compound of the formula

or a pharmaceutically acceptable salt thereof, wherein

R is dimethylamino, pyrrolidin-1-yl, 1H-imidazolyl, 4-methylpiperazin-1-yl, 4-morpholino, or N,N,N′-trimethylethylenediamino.

4. The compound of claim 3 , wherein R is 1H-imidazolyl.

5. A composition comprising one or more compounds of claim 3 , and optionally one or more carriers, diluents, or excipients, or a combination thereof.

6. A method for inhibiting topoisomerase 1, the method comprising the step of contacting topoisomerase 1 with an effective amount of one or more compounds of claim 3 .

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 9, 2012
From: CUSHMAN, MARK S.; SONG, YUNLONG
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 029270/0151 →
CONFIRMATORY LICENSE Recorded Aug 24, 2012
From: PURDUE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 028840/0831 →
Continuity (2)
Provisional Application 61298789 · Jan 27, 2010
Related Publication 20120302563A1 · Nov 29, 2012