IP Library Granted Patent US 9,260,575
Granted Patent B2
US 9,260,575 · App. 13/581,719 · Granted Feb 16, 2016

Film and method of preparing the same

Inventors: Jin Ryul Son (Incheon, KR); Sung Hwan Bang (Incheon, KR); Jyung Hee Jeon (Incheon, KR); Sang Youb Lee (Incheon, KR); Ju Hee Shin (Incheon, KR)
Assignee: SAMSUNG FINE CHEMICALS CO., LTD.
C08J5/18B05D1/18B05D3/007B29C41/24B29D7/01C08J3/28C08K3/16C08L1/26C08L1/284B29K2001/08C08J2301/28
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Quick Facts
Patent No.
US 9,260,575
App. No.
13/581,719
Granted
Feb 16, 2016
Kind
B2
Abstract

A film and a method of preparing the same. The film includes cellulose ether and sodium chloride, wherein an amount of the sodium chloride is from about 0.25 wt % to about 0.6 wt % based on a total weight of the film, and the film has a light-transmission reduction ratio of about 15% or less.

Claims (16)

1. A film comprising cellulose ether and sodium chloride, wherein an amount of the sodium chloride is from about 0.25 wt % to about 0.6 wt % based on a total weight of the film, and the film has a light-transmission reduction ratio of about 15% or less.

2. The film of claim 1 , wherein the film has a light-transmission reduction ratio of about 2% or less.

3. The film of claim 1 , wherein the film is a transparent film.

4. The film of claim 3 , wherein the film has a light-transmission of about 80% or greater.

5. The film of claim 1 , wherein the film is a colored film.

6. The film of claim 1 , wherein the film has a water vapor transmission rate (WVTR) of about 160 g/m 2 /day or less.

7. The film of claim 1 , wherein the film is used for hard capsules, food films, medical films, or industrial films.

8. A method of preparing the film of claim 1 , the method comprising: dissolving cellulose ether in a solvent to obtain an untreated cellulose ether solution; ultrasonicating the untreated cellulose ether solution to obtain a treated cellulose ether solution; coating the treated cellulose ether solution on a substrate; and drying the coated cellulose ether solution.

9. The method of claim 8 , wherein the cellulose ether comprises sodium chloride, wherein an amount of the sodium chloride is greater than about 0.3 wt % and equal to or less than 0.6 wt % based on the total weight of the cellulose ether.

10. The method of claim 8 , wherein the cellulose ether is water-soluble, and the solvent is an aqueous solvent.

11. The method of claim 8 , wherein the cellulose ether comprises at least one selected from the group consisting of methyl cellulose, hydroxypropylmethyl cellulose, and hydroxyethylmethyl cellulose.

12. The method of claim 8 , wherein the untreated cellulose ether solution has a cellulose ether concentration of from about 5 wt % to about 25 wt %.

13. The method of claim 8 , wherein the ultrasonication comprises irradiating ultrasonic waves having a frequency of from about 10 kHz to about 30 kHz onto the untreated cellulose ether solution at an energy of from about 80 kJ/L (per volume of the untreated cellulose ether solution) to about 300 kJ/L (per volume of the untreated cellulose ether solution) .

14. The method of claim 8 , further comprising adding a plasticizer into the untreated cellulose ether solution.

15. The method of claim 14 , wherein the plasticizer comprises at least one selected from the group consisting of glycerol, sorbitol, propylene glycol, and polyethylene glycol.

16. The method of claim 14 , wherein an amount of the plasticizer is from 1 part by weight to 10 parts by weight based on 100 parts by weight of the cellulose ether.

Assignments (2)
CHANGE OF NAME Recorded May 17, 2016
From: SAMSUNG FINE CHEMICALS CO., LTD.
To: LOTTE FINE CHEMICAL CO., LTD.
Reel/Frame 038726/0289 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 29, 2012
From: SON, JIN RYUL; BANG, SUNG HWAN; JEON, JYUNG HEE; LEE, SANG YOUB; SHIN, JU HEE
To: SAMSUNG FINE CHEMICALS CO., LTD.
Reel/Frame 028870/0476 →
Priority Claims (1)
KR 10-2012-0040422 · Apr 18, 2012 · national
Continuity (1)
Related Publication 20150027343A1 · Jan 29, 2015