Method for manufacturing a nitride semiconductor substrate
The invention provides a method for manufacturing a nitride semiconductor substrate capable of reducing a cleavage during slicing of the nitride semiconductor single crystal and capable of improving a yield rate of the nitride semiconductor substrate. The method includes growing a nitride semiconductor single crystal on a seed crystal substrate by vapor phase epitaxy; grinding an outer peripheral surface the grown nitride semiconductor single crystal; and slicing the nitride semiconductor single crystal with its outer peripheral surface ground. A grinding amount of the outer peripheral surface of the nitride semiconductor single crystal in the step of grinding is 1.5 mm or more.
1. A method for manufacturing a nitride semiconductor substrate, comprising:
growing a nitride semiconductor single crystal on a seed crystal substrate made of a nitride semiconductor single crystal by vapor phase epitaxy;
grinding a single crystal outer peripheral surface of the grown nitride semiconductor single crystal; and
slicing the grown nitride semiconductor single crystal with its outer peripheral surface ground,
wherein, after the grinding step, the single crystal outer peripheral surface has a surface roughness RMS of 3 μm or less and wherein a grinding amount of the single crystal outer peripheral surface of the grown nitride semiconductor single crystal is 1.5 mm or more to increase slice yield in the step of slicing.
2. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein the nitride semiconductor single crystal, grown in the step of growing, is formed into a cylindrical shape.
3. The method for manufacturing a nitride semiconductor substrate according to claim 2 , wherein a diameter of the cylindrical nitride semiconductor single crystal is 36 mm or more.
4. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein a thickness of the nitride semiconductor single crystal is 3 mm or more.
5. A method for manufacturing a nitride semiconductor substrate, comprising:
growing a nitride semiconductor single crystal on a seed crystal substrate by vapor phase epitaxy;
grinding a single crystal outer peripheral surface of the grown nitride semiconductor single crystal; and
slicing the nitride semiconductor single crystal with its outer peripheral surface ground, wherein a grinding amount of the single crystal outer peripheral surface of the grown nitride semiconductor single crystal is 1.5 mm or more, and
wherein, after the grinding step, the single crystal outer peripheral surface has a surface roughness RMS of 3 μm or less.
6. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein the nitride semiconductor single crystal is formed into a cylindrical shape.
7. The method for manufacturing a nitride semiconductor substrate according to claim 6 , wherein a diameter of the cylindrical nitride semiconductor single crystal is 36 mm or more.
8. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein a thickness of the nitride semiconductor single crystal is 3 mm or more.
9. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein the nitride semiconductor single crystal, after grinding, is formed into a shape selected from the group consisting of a cylindrical shape, a truncated cone shape, a prism shape, and a truncated pyramid shape.
10. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein the nitride semiconductor single crystal, after grinding, is formed into a shape selected from the group consisting of a cylindrical shape, a truncated cone shape, a prism shape, and a truncated pyramid shape.
11. A method for manufacturing a nitride semiconductor substrate, comprising:
growing a nitride semiconductor single crystal on a seed crystal substrate by vapor phase epitaxy; the nitride semiconductor single crystal grown formed into a cylindrical shape and having a diameter of 36 mm or more;
grinding a single crystal outer peripheral surface of the grown nitride semiconductor single crystal, wherein an entirety of the outer peripheral surface is ground; and
slicing the nitride semiconductor single crystal with its outer peripheral surface ground, wherein a grinding amount of the single crystal outer peripheral surface of the grown nitride semiconductor single crystal is 1.5 mm or more, and
wherein, after the grinding step, the single crystal outer peripheral surface has a surface roughness RMS of 3 μm or less.
12. The method for manufacturing a nitride semiconductor substrate according to claim 11 , wherein a thickness of the nitride semiconductor single crystal is 3 mm or more.
13. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein an entirety of the outer peripheral surface of the grown nitride semiconductor single crystal is ground.
14. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein an entirety of the outer peripheral surface of the grown nitride semiconductor single crystal is ground.
15. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein the grinding in the step of grinding is to a depth of 1.5 mm or more into the grown nitride semiconductor single crystal.
16. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein the grinding in the step of grinding is to a depth of 1.5 mm or more into the grown nitride semiconductor single crystal.
17. The method for manufacturing a nitride semiconductor substrate according to claim 11 , wherein the grinding in the step of grinding is to a depth of 1.5 mm or more into the grown nitride semiconductor single crystal.
18. The method for manufacturing a nitride semiconductor substrate according to claim 1 , wherein the nitride semiconductor single crystal, grown in the step of growing, is grown on an N-polar face of the seed crystal substrate and is formed into a reversed, circular truncated cone shape wherein a diameter of the nitride semiconductor single crystal is increased in a growth direction.
19. The method for manufacturing a nitride semiconductor substrate according to claim 5 , wherein the nitride semiconductor single crystal, grown in the step of growing, is grown on an N-polar face of the seed crystal substrate and is formed into a reversed, circular truncated cone shape wherein a diameter of the nitride semiconductor single crystal is increased in a growth direction.