IP Library Granted Patent US 9,412,568
Granted Patent B2
US 9,412,568 · App. 13/628,093 · Granted Aug 9, 2016

Large-area sputtering targets

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Quick Facts
Patent No.
US 9,412,568
App. No.
13/628,093
Granted
Aug 9, 2016
Kind
B2
Abstract

In various embodiments, joined sputtering targets are formed at least in part by spray deposition of the sputtering material and/or welding.

Claims (39)

1. A joined sputtering target comprising a sputtering material, the joined sputtering target comprising:

first and second discrete sputtering-target tiles joined at an interface therebetween, the tiles comprising the sputtering material,

wherein:

the interface comprises a recess therealong at least partially filled with unmelted powder,

the first tile comprises a beveled edge forming at least a portion of the recess and disposed in contact with the unmelted powder,

the beveled edge has a reentrant surface comprising (i) one or more concave portions and (ii) one or more convex portions, and (iii) one or more inflection points each separating a concave portion from a convex portion, and

no part of the beveled edge overlaps any portion of the second tile.

2. The joined sputtering target of claim 1 , wherein the first and second tiles are joined at opposing edges, and the interface further comprises portions of the two opposing edges substantially in contact with each other and disposed beneath the at least partially filled recess.

3. The joined sputtering target of claim 1 , wherein at least a portion of the beveled edge is substantially planar and forms an angle of greater than 45° with respect to a normal to a top surface of the joined sputtering target.

4. The joined sputtering target of claim 3 , wherein the angle is selected from the range of 45° to 60°.

5. The joined sputtering target of claim 1 , wherein the unmelted powder comprises the sputtering material.

6. The joined sputtering target of claim 5 , wherein the unmelted powder consists essentially of the sputtering material.

7. The joined sputtering target of claim 1 , wherein each of the first and second tiles consists essentially of the sputtering material.

8. The joined sputtering target of claim 1 , wherein the sputtering material comprises a mixture or alloy of at least two constituent materials.

9. The joined sputtering target of claim 8 , wherein the unmelted powder comprises discrete regions each substantially free of at least one of the constituent materials, and the joined sputtering target comprises at least one region at the interface in which at least two of the constituent materials are interdiffused.

10. The joined sputtering target of claim 8 , wherein the at least two constituent materials comprise Mo and Ti.

11. The joined sputtering target of claim 1 , further comprising a backing plate attached to the first and second tiles.

12. The joined sputtering target of claim 11 , wherein the unmelted powder is in contact with the backing plate.

13. The joined sputtering target of claim 1 , wherein at least a portion of the joined sputtering target is substantially planar.

14. The joined sputtering target of claim 1 , wherein at least a portion of the joined sputtering target is substantially tubular.

15. The joined sputtering target of claim 1 , wherein (i) the reentrant surface comprises a first concave portion having a first radius of curvature, (ii) the reentrant surface comprises a first convex portion having a second radius of curvature, and (iii) the first radius of curvature is approximately equal to the second radius of curvature.

16. The joined sputtering target of claim 1 , wherein (i) the reentrant surface comprises a first concave portion having a first radius of curvature, (ii) the reentrant surface comprises a first convex portion having a second radius of curvature, and (iii) the first radius of curvature is smaller than the second radius of curvature.

17. The joined sputtering target of claim 1 , wherein:

each of the first and second tiles comprises a beveled edge forming at least a portion of the recess and disposed in contact with the unmelted powder,

each beveled edge has a reentrant surface comprising (i) one or more concave portions and (ii) one or more convex portions, and (iii) one or more inflection points each separating a concave portion from a convex portion, and

neither beveled edge overlaps any portion of the other tile.

18. The joined sputtering target of claim 1 , wherein the reentrant surface comprises a plurality of concave portions, each pair of concave portions being separated by a convex portion therebetween.

19. The joined sputtering target of claim 18 , wherein the reentrant surface comprises a plurality of convex portions.

20. The joined sputtering target of claim 1 , wherein the interface comprises a gap between the first and second tiles having a width of at least 2 mm, the gap comprising unmelted powder therewithin.

21. The joined sputtering target of claim 20 , wherein the width of the gap ranges from 2 mm to 8 mm.

22. The joined sputtering target of claim 1 , wherein the sputtering material comprises at least one of titanium, niobium, tantalum, or tungsten.

23. The joined sputtering target of claim 1 , wherein the sputtering material consists essentially of at least one of titanium, niobium, tantalum, or tungsten.

24. The joined sputtering target of claim 8 , wherein the at least two constituent materials comprise W and Ti.

25. The joined sputtering target of claim 8 , wherein the at least two constituent materials comprise Cu and W.

26. The joined sputtering target of claim 11 , wherein the backing plate is attached to the first and second tiles via a joining compound.

27. The joined sputtering target of claim 26 , wherein the joining compound comprises In solder.

28. The joined sputtering target of claim 1 , wherein the joined sputtering target is substantially free of residual stress.

29. The joined sputtering target of claim 1 , wherein an areal dimension of the joined sputtering target is at least 2800 mm×2500 mm.

30. The joined sputtering target of claim 1 , wherein a length of the joined sputtering target is 2.7 meters or longer.

Assignments (7)
CHANGE OF NAME Recorded Nov 1, 2023
From: EUCLID FACILITY HOLDINGS, LLC
To: H.C. STARCK SOLUTIONS EUCLID, LLC
Reel/Frame 065415/0762 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 31, 2023
From: H.C. STARCK INC.
To: EUCLID FACILITY HOLDINGS, LLC
Reel/Frame 065402/0594 →
RELEASE OF SECURITY INTEREST Recorded Nov 2, 2021
From: GLAS TRUST CORPORATION LIMITED
To: H.C. STARCK INC.
Reel/Frame 058769/0242 →
RELEASE OF SECURITY INTEREST Recorded Nov 2, 2021
From: GLAS TRUST CORPORATION LIMITED
To: H.C. STARCK INC.
Reel/Frame 058768/0827 →
SECURITY INTEREST Recorded Mar 31, 2016
From: H.C. STARCK INC.
To: GLAS TRUST CORPORATION LIMITED, AS SECURITY AGENT FOR THE BENEFIT OF THE SENIOR SECURED PARTIES
Reel/Frame 038311/0460 →
SECURITY INTEREST Recorded Mar 31, 2016
From: H.C. STARCK INC.
To: GLAS TRUST CORPORATION LIMITED, AS SECURITY AGENT FOR THE BENEFIT OF THE SECOND LIEN SECURED PARTIES
Reel/Frame 038311/0472 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2012
From: DARY, FRANCOIS-CHARLES; GAYDOS, MARK; LOEWENTHAL, WILLIAM; MILLER, STEVEN ALFRED; ROZAK, GARY; VOLCHKO, SCOTT JEFFREY; ZIMMERMANN, STEFAN; STAWOVY, MICHAEL THOMAS
To: H.C. STARCK INC.
Reel/Frame 029379/0515 →