IP Library Granted Patent US 9,000,188
Granted Patent B2
US 9,000,188 · App. 13/645,187 · Granted Apr 7, 2015

Monocyclic cyanoenones and methods of use thereof

Inventors: Tadashi Honda (Port Jefferson Station, NY); Emilie David (Kingston, CA); Dale Mierke (Hanover, NH)
Assignee: Trustees of Dartmouth College
C07F7/10C07C255/46C07D215/48C07D217/02C07D217/24C07D235/12C07D235/14C07F7/0818C07F7/1856C07C255/47C07D233/64C07C2101/16
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Quick Facts
Patent No.
US 9,000,188
App. No.
13/645,187
Granted
Apr 7, 2015
Kind
B2
Abstract

The present invention features monocyclic cyanoenone compositions and methods for using the same in the treatment of diseases such as cancer, inflammatory diseases and neurodegenerative diseases.

Claims (31)

1. A pharmaceutical composition comprising a compound of the formula or a pharmaceutically acceptable salt or tautomer thereof:

wherein:

R 1 is:

hydroxy, amino, cyano, or

alkyl (C≦8) , alkenyl (C≦18) , alkynyl (C≦18) , aryl (C≦18) , aralkyl (C≦18) , heteroaryl (C≦18) , heteroaralkyl (C≦18) , acyl (C≦18) , alkoxy (C≦18) , alkenyloxy (C≦18) , alkynyloxy (C≦18) , aryloxy (C≦18) , aralkoxy (C≦18) , heteroaryloxy (C≦18) , heteroaralkoxy (C≦18) , acyloxy (C≦18) , alkyl-amino (C≦18) , dialkylamino (C≦18) , alkoxyamino (C≦18) , alkenyl-amino (C≦18) , alkynylamino (C≦18) , arylamino (C≦18) , aralkylamino (C≦18) , heteroarylamino (C≦18) , heteroaralkylamino (C≦18) , alkylsulphonyl-amino (C≦18) , amido (C≦18) , alkylideneamino (C≦18) , aralkylidene-amino (C≦18) , or a substituted version of any of these groups; and

R 2 is cyano, alkynyl (C≦8) , substituted alkynyl (C≦8) , or —C≡C—R 9 ,

wherein R 9 is:

hydrogen or cyano; or

alkyl (C≦6) , aryl (C≦6) , acyl (C≦6) , alkylsilyl (C≦6) or a substituted version of any of these groups;

and a pharmaceutically acceptable carrier.

2. The pharmaceutical composition of claim 1 , wherein the bond between atoms 4 and 5 is a double bond.

3. The pharmaceutical composition of claim 2 , wherein R 2 is alkynyl (C≦8) or substituted alkynyl (C≦8) .

4. The pharmaceutical composition of claim 2 , wherein R 2 is —C≡C—R 9 ,

wherein R 9 is:

hydrogen or cyano; or

alkyl (C≦6) , aryl (C≦6) , acyl (C≦6) , alkylsilyl (C≦6) or a substituted version of any of these groups.

5. The pharmaceutical composition of claim 4 , wherein R 9 is hydrogen.

6. The pharmaceutical composition of claim 4 , wherein R 9 is —Si(CH 3 ) 2 C(CH 3 ) 3 .

7. The pharmaceutical composition of claim 1 , wherein R 2 is cyano.

8. The pharmaceutical composition of claim 2 , wherein R 1 is alkyl (C≦8) or substituted alkyl (C≦8) .

9. The pharmaceutical composition of claim 8 , wherein R 1 is methyl or ethyl.

10. The pharmaceutical composition of claim 2 , wherein R 1 is aralkyl (C≦18) , substituted aralkyl (C≦18) , heteroaralkyl (C≦18) or substituted heteroaralkyl (C≦18) .

11. The pharmaceutical composition of claim 2 , wherein R 1 is cyano.

12. The pharmaceutical composition of claim 2 , wherein the compound is further defined by the formula:

wherein R 1 is:

cyano, or

alkyl (C≦18) , alkenyl (C≦18) , alkynyl (C≦18) , aryl (C≦18) , aralkyl (C≦18) , heteroaryl (C≦18) , heteroaralkyl (C≦18) , acyl (C≦18) , alkoxy (C≦18) , alkenyloxy (C≦18) , alkynyloxy (C≦18) , aryloxy (C≦18) , aralkoxy (C≦18) , heteroaryloxy (C≦18) , heteroaralkoxy (C≦18) , acyloxy (C≦18) , alkylamino (C≦18) , dialkylamino (C≦18) , alkoxyamino (C≦18) , alkenylamino (C≦18) , alkynylamino (C≦18) , arylamino (C≦18) , aralkylamino (C≦18) , heteroarylamino (C≦18) , heteroaralkylamino (C≦18) , alkyl-sulfonylamino (C≦18) , amido (C≦18) , alkylideneamino (C≦18) , aralkylidene-amino (C≦18) , or a substituted version of any of these groups;

or a pharmaceutically acceptable salt or tautomer of the formula.

13. The pharmaceutical composition of claim 1 , wherein the compound is selected from the group consisting of:

14. A pharmaceutical composition, comprising a compound of the formula:

and a pharmaceutically acceptable carrier.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jul 16, 2018
From: DARMOUTH COLLEGE
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 046547/0621 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 14, 2015
From: HONDA, TADASHI; DAVID, EMILIE; MIERKE, DALE
To: TRUSTEES OF DARTMOUTH COLLEGE
Reel/Frame 036789/0719 →
Continuity (3)
Continuation 13055418
Provisional Application 61082550 · Jul 22, 2008
Related Publication 20130274480A1 · Oct 17, 2013