IP Library Granted Patent US 9,776,859
Granted Patent B2
US 9,776,859 · App. 13/657,678 · Granted Oct 3, 2017

Microscale metallic CNT templated devices and related methods

Inventors: Robert C. Davis (Provo, UT); Richard R. Vanfleet (Provo, UT)
Assignee: Brigham Young University
B81C1/00666B81B3/0072B81C1/00619B81B2201/025B82Y15/00B82Y30/00B82Y40/00
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Quick Facts
Patent No.
US 9,776,859
App. No.
13/657,678
Granted
Oct 3, 2017
Kind
B2
Abstract

A microscale device comprises a patterned forest of vertically grown and aligned carbon nanotubes defining a carbon nanotube forest with the nanotubes having a height defining a thickness of the forest, the patterned forest defining a patterned frame that defines one or more components of a microscale device. A conformal coating of substantially uniform thickness at least partially coats the nanotubes, defining coated nanotubes and connecting adjacent nanotubes together, without substantially filling interstices between individual coated nanotubes. A metallic interstitial material infiltrates the carbon nanotube forest and at least partially fills interstices between individual coated nanotubes.

Claims (28)

1. A microscale device, comprising:

a patterned forest of vertically grown and aligned carbon nanotubes defining a carbon nanotube forest with the nanotubes having a height defining a thickness of the forest, the patterned forest defining a patterned frame that defines one or more components of the microscale device;

a conformal coating of substantially uniform thickness extending throughout the carbon nanotube forest, the carbon nanotube forest having a thickness of at least three microns, the conformal coating substantially coating the nanotubes, defining coated nanotubes and connecting adjacent nanotubes together such that the carbon nanotube forest is sufficiently robust for liquid processing, without substantially filling interstices between individual coated nanotubes, wherein the conformal coating comprises a carbon material; and

a metallic interstitial material infiltrating the carbon nanotube forest and at least partially filling interstices between individual coated nanotubes.

2. The device of claim 1 , wherein at least one component of the patterned frame is fixed and at least one component of the patterned frame is moveable relative to the fixed component.

3. The device of claim 2 , wherein the microscale device comprises a MEMS device.

4. The device of claim 1 , wherein the metallic interstitial material is applied by an electroplating process, wherein the metallic interstitial material infiltrates the carbon nanotube forest with an infiltration uniformity achieved by application of the electroplating process to the carbon nanotube forest.

5. The device of claim 1 , wherein the thickness of the carbon nanotube forest is between 3 μm (microns) and 9 mm.

6. The device of claim 1 , wherein the microscale device defines at least a portion of a sensor.

7. The device of claim 6 , wherein the sensor comprises a gyro.

8. The device of claim 7 , wherein the gyro comprises a transductive capacitor comprising a capacitive gap in the form of a trench defined by the microscale device, the trench comprising a height-to-width ratio of at least 100:1.

9. The device of claim 1 , wherein the metallic interstitial material comprises Nickel.

10. A microscale device, comprising:

a patterned forest of vertically grown and aligned carbon nanotubes defining a carbon nanotube forest with the nanotubes having a height defining a thickness of the forest, the patterned forest defining a patterned frame that defines one or more components of the microscale device, the carbon nanotube forest comprising at least one feature comprising a height-to-width ratio greater than 100:1;

a conformal coating of substantially uniform thickness extending throughout the carbon nanotube forest, the carbon nanotube forest having a thickness of at least three microns, the conformal coating substantially coating the nanotubes, defining coated nanotubes and connecting adjacent nanotubes together, without substantially filling interstices between individual coated nanotubes, wherein the conformal coating comprises a carbon material; and

a metallic interstitial material infiltrating the carbon nanotube forest and at least partially filling interstices between individual coated nanotubes.

11. The microscale device of claim 10 , wherein the feature comprises a height-to-width ratio greater than 200:1.

12. The microscale device of claim 10 , wherein at least one component of the patterned frame is fixed and at least one component of the patterned frame is moveable relative to the fixed component, wherein the microscale device defines at least a portion of a gyro comprising a transductive capacitor, wherein the feature comprises a capacitive gap in the form of a trench defined by the microscale device.

13. The microscale device of claim 10 , wherein the metallic interstitial material is applied by an electroplating process, wherein the metallic interstitial material infiltrates the carbon nanotube forest with an infiltration uniformity achieved by application of the electroplating process to the carbon nanotube forest.

14. The microscale device of claim 10 , wherein the metallic interstitial material comprises Nickel.

15. A microscale device, comprising:

a patterned forest of vertically grown and aligned carbon nanotubes defining a carbon nanotube forest with the nanotubes having a height defining a thickness of the forest, the patterned forest defining a patterned frame that defines one or more components of the microscale device;

a conformal coating of substantially uniform thickness extending throughout the carbon nanotube forest, the carbon nanotube forest having a thickness of at least three microns, the conformal coating substantially coating the nanotubes, defining coated nanotubes and connecting adjacent nanotubes together, without substantially filling interstices between individual coated nanotubes, wherein the conformal coating comprises a carbon material; and

a metallic interstitial material infiltrating the carbon nanotube forest and at least partially filling interstices between individual coated nanotubes, wherein the metallic interstitial material infiltrates the carbon nanotube forest with an infiltration uniformity achieved by application of an electroplating process to the carbon nanotube forest.

16. The microscale device of claim 15 , wherein the infiltration uniformity is achieved by application of a pulsed current.

17. The microscale device of claim 15 , wherein the carbon nanotube forest comprises at least one feature comprising a height-to-width ratio greater than 100:1.

18. The microscale device of claim 17 , wherein at least one component of the patterned frame is fixed and at least one component of the patterned frame is moveable relative to the fixed component, wherein the microscale device defines at least a portion of a gyro comprising a transductive capacitor, wherein the feature comprises a capacitive gap in the form of a trench defined by the microscale device.

19. The microscale device of claim 15 , wherein the metallic interstitial material comprises Nickel.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2025
From: BRIGHAM YOUNG UNIVERSITY
To: CNT HOLDINGS, LLC
Reel/Frame 071494/0659 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 15, 2013
From: DAVIS, ROBERT C.; VANFLEET, RICHARD R.
To: BRIGHAM YOUNG UNIVERSITY
Reel/Frame 029628/0764 →
Continuity (2)
Provisional Application 61627919 · Oct 20, 2011
Related Publication 20130285160A1 · Oct 31, 2013