IP Library Granted Patent US 9,068,283
Granted Patent B2
US 9,068,283 · App. 13/662,955 · Granted Jun 30, 2015

Strain sensors, methods of making same, and applications of same

Inventors: Alexandru S. Biris (Little Rock, AR); Steven Trigwell (Kennedy Space Center, FL); Walter Hatfield (Merritt Island, FL)
Assignee: BOARD OF TRUSTEES OF THE UNIVERSITY OF ARKANSAS
D01F9/127Y10T428/25Y10T428/30B82Y30/00B82Y40/00G01B7/18H01B1/04
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Quick Facts
Patent No.
US 9,068,283
App. No.
13/662,955
Granted
Jun 30, 2015
Kind
B2
Abstract

In one aspect, the present invention relates to a layered structure usable in a strain sensor. In one embodiment, the layered structure has a substrate with a first surface and an opposite, second surface defining a body portion therebetween; and a film of carbon nanotubes deposited on the first surface of the substrate, wherein the film of carbon nanotubes is conductive and characterized with an electrical resistance. In one embodiment, the carbon nanotubes are aligned in a preferential direction. In one embodiment, the carbon nanotubes are formed in a yarn such that any mechanical stress increases their electrical response. In one embodiment, the carbon nanotubes are incorporated into a polymeric scaffold that is attached to the surface of the substrate. In one embodiment, the surfaces of the carbon nanotubes are functionalized such that its electrical conductivity is increased.

Claims (37)

1. A layered structure usable in a strain sensor, comprising:

a substrate with a first surface and an opposite, second surface defining a body portion therebetween;

a film of carbon nanotubes deposited on the first surface of the substrate, wherein the film of carbon nanotubes is electrically conductive and characterized with an electrical resistance; and

a flexible polymeric film placed between the film of carbon nanotubes and the substrate,

wherein the mechanical properties of the flexible polymeric film match that of the substrate;

wherein the substrate is insulative, and comprises a carbon composite material having a substantial amount of non-carbon elements, to allow material compatibility between the carbon-based substrate and the film of carbon nanotubes; and

wherein the carbon nanotubes are randomly directed in the film, such that the resistance can be monitored independent of direction.

2. The layered structure of claim 1 , wherein the carbon nanotubes comprise multi-wall carbon nanotubes.

3. The layered structure of claim 2 , wherein the film of multi-wall carbon nanotubes is formed with superelasticity.

4. The layered structure of claim 2 , wherein the film of multi-wall carbon nanotubes is formed such that the electrical resistance is a function of a stress applied to the film of multi-wall carbon nanotubes.

5. The layered structure of claim 4 , wherein the electrical resistance is a linear function of the stress applied to the film of multi-wall carbon nanotubes, wherein the linear function is obtained using a 3-point bend test assembly.

6. The layered structure of claim 2 , wherein the multi-wall carbon nanotubes are formed with inner diameters in a range of about 2-8 nm, outer diameters in a range of about 10-30 nm, and lengths in a range of about 5.0-50 micros or longer.

7. The layered structure of claim 1 , wherein the carbon nanotubes are formed in a yarn such that any mechanical stress increases their electrical response.

8. The layered structure of claim 1 , wherein the carbon nanotubes are incorporated into a polymeric scaffold that is attached to the surface of the substrate.

9. The layered structure of claim 1 , wherein the surfaces of the carbon nanotubes are functionalized such that its electrical conductivity is increased.

10. A strain sensor comprising the layered structure of claim 1 .

11. A strain sensor, comprising:

a substrate with a first surface and an opposite, second surface defining a body portion therebetween;

a film of carbon nanotubes deposited on the first surface of the substrate, wherein the film of carbon nanotubes is electrically conductive and characterized with an electrical resistance that is changeable in response to a change in an environment surrounding the film of carbon nanotubes; and

a flexible polymeric film placed between the film of carbon nanotubes and the substrate,

wherein the mechanical properties of the flexible polymeric film match that of the substrate;

wherein the substrate is insulative, and comprises a carbon composite material having a substantial amount of non-carbon elements, to allow material compatibility between the carbon-based substrate and the film of carbon nanotubes; and

wherein the carbon nanotubes are randomly directed in the film, such that the resistance can be monitored independent of direction.

12. The strain sensor of claim 11 , wherein the change in the environment surrounding the film of carbon nanotubes comprises a change in a stress applied to the film of carbon nanotubes, a change in a temperature at the film of carbon nanotubes, or a change in a pressure applied to the film of carbon nanotubes.

13. The strain sensor of claim 11 , further comprising:

(a) a first electrically conducting terminal positioned in a first place of the film of carbon nanotubes; and

(b) a second electrically conducting terminal positioned in a second place of the film of carbon nanotubes,

wherein the first and second electrically conducting terminals are positioned apart such that in use, an electrically conductive path is formed therebetween to detect changes in the electrical resistance of the film of carbon nanotubes in response to the change in the environment surrounding the film of carbon nanotubes.

14. The strain sensor of claim 13 , wherein each of the first and second electrically conducting terminals is formed of an electrically conductive material.

15. The strain sensor of claim 11 , wherein the carbon nanotubes comprise multi-wall carbon nanotubes.

16. The strain sensor of claim 15 , wherein the film of multi-wall carbon nanotubes is formed to have superelasticity.

17. The strain sensor of claim 15 , wherein the film of multi-wall carbon nanotubes is formed such that the electrical resistance is a function of a stress applied to the film of multi-wall carbon nanotubes.

18. The strain sensor of claim 17 , wherein the electrical resistance is a linear function of the stress applied to the film of multi-wall carbon nanotubes, wherein the linear function is obtained using a 3-point bend test assembly.

19. The strain sensor of claim 15 , wherein the multi-wall carbon nanotubes are formed with inner diameters in a range of about 2-8 nm, outer diameters in a range of about 10-30 nm, and lengths in a range of about 5.0-50 micros or longer.

20. The strain sensor of claim 11 , wherein the carbon nanotubes are formed in a yarn such that any mechanical stress increases their electrical response.

21. The strain sensor of claim 11 , wherein the carbon nanotubes are incorporated into a polymeric scaffold that is attached to the surface of the substrate.

22. The strain sensor of claim 11 , wherein the surfaces of the carbon nanotubes are functionalized such that its electrical conductivity is increased.

Assignments (2)
CONFIRMATORY LICENSE Recorded Oct 12, 2023
From: UNIVERSITY OF ARKANSAS AT FAYETTEVILLE
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 065220/0163 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 29, 2012
From: BIRIS, ALEXANDRU S.; TRIGWELL, STEVEN; HATFIELD, WALTER
To: BOARD OF TRUSTEES OF THE UNIVERSITY OF ARKANSAS
Reel/Frame 029205/0922 →
Continuity (2)
Provisional Application 61552849 · Oct 28, 2011
Related Publication 20130104665A1 · May 2, 2013