IP Library Granted Patent US 9,255,334
Granted Patent B2
US 9,255,334 · App. 13/664,122 · Granted Feb 9, 2016

Hydrogen evolution reaction catalyst

Inventors: Ram Subbaraman (Westmont, IL); Vojislav Stamenkovic (Naperville, IL); Nenad Markovic (Hinsdale, IL); Dusan Tripkovic (Hinsdale, IL)
Assignee: UChicago Argonne, LLC
C25B11/0447C25B1/04C25B9/06C25B11/0452C25B11/0457Y02E60/366
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Quick Facts
Patent No.
US 9,255,334
App. No.
13/664,122
Granted
Feb 9, 2016
Kind
B2
Abstract

Systems and methods for a hydrogen evolution reaction catalyst are provided. Electrode material includes a plurality of clusters. The electrode exhibits bifunctionality with respect to the hydrogen evolution reaction. The electrode with clusters exhibits improved performance with respect to the intrinsic material of the electrode absent the clusters.

Claims (26)

1. An electrode for use in a hydrogen evolution reaction, comprising:

an electrode platinum substrate interactive with atomic hydrogen to adsorb atomic hydrogen;

a plurality of nickel oxide or nickel hydroxide clusters directly deposited on the surface of the electrode platinum substrate as island shapes and interactive with water to dissociate hydrogen and hydroxide from water;

wherein the electrode exhibits bifunctionality with respect to the hydrogen evolution reaction.

2. The electrode of claim 1 , wherein the electrode platinum substrate comprises a plurality of low coordination areas on its surface.

3. The electrode of claim 2 , wherein the low coordination areas comprise a plurality of surface defects.

4. The electrode of claim 3 , wherein substantially all of the plurality of nickel oxide or nickel hydroxide clusters are deposited on the plurality of surface defects.

5. The electrode of claim 1 , wherein the nickel oxide or nickel hydroxide consists essentially of Ni(OH) 2 .

6. The electrode of claim 1 , about 35% of the electrode is covered with deposited nickel oxide or nickel clusters.

7. The electrode of claim 1 , wherein the nickel oxide or nickel hydroxide clusters have a height of about 0.7 nm and a width of about 8 nm to about 10 nm.

8. An electrolytic cell comprising:

an anode;

a cathode platinum substrate interactive with atomic hydrogen to adsorb atomic hydrogen and having a plurality of nickel oxide or nickel hydroxide clusters directly deposited on the surface of the cathode platinum substrate as island shapes and interactive with water to dissociate hydrogen and hydroxide from water;

an electrolyte;

wherein the cathode exhibits bifunctionality with respect to the hydrogen evolution reaction.

9. The electrolytic cell of claim 8 , wherein the electrolyte is an alkaline electrolyte.

10. The electrolytic cell of claim 8 , further comprising lithium ions.

11. The electrolytic cell of claim 8 , wherein the cathode platinum substrate comprises a plurality of low coordination areas on its surface.

12. The electrolytic cell of claim 11 , wherein the low coordination areas comprise a plurality of surface defects.

13. The electrolytic cell of claim 12 , wherein substantially all of the plurality of nickel oxide or nickel hydroxide clusters are deposited on the plurality of surface defects.

14. The electrolytic cell of claim 8 , wherein the nickel oxide or nickel hydroxide consists essentially of Ni(OH) 2 .

15. An electrode for use in the hydrogen evolution reaction, comprising:

an electrode platinum substrate;

a plurality of metal oxide or metal hydroxide clusters directly deposited on the surface of the electrode platinum substrate as island shapes;

where about 35% of the electrode is covered with deposited Ni(OH) 2 clusters.

wherein the electrode exhibits bifunctionality with respect to the hydrogen evolution reaction.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 033142 FRAME: 0389. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jul 1, 2014
From: MARKOVIC, NENAD; STAMENKOVIC, VOJISLAV; SUBBARAMAN, RAM; TRIPKOVIC, DUSAN
To: UCHICAGO ARGONNE, LLC.
Reel/Frame 033264/0193 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2014
From: MARKOVIC, NENAD; STAMENKOVIC, VOJISLAV; SUBBARAMAN, RAM; TRIPKOVIC, DUSAN
To: UCHICAGO ARGONNE, LLC.
Reel/Frame 033142/0489 →
CONFIRMATORY LICENSE Recorded Jun 3, 2013
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 030583/0631 →
CONFIRMATORY LICENSE Recorded Feb 8, 2013
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 029786/0014 →
Continuity (1)
Related Publication 20140116890A1 · May 1, 2014