IP Library Granted Patent US 9,006,268
Granted Patent B2
US 9,006,268 · App. 13/702,656 · Granted Apr 14, 2015

Prolylcarboxypeptidase inhibitors

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Quick Facts
Patent No.
US 9,006,268
App. No.
13/702,656
Granted
Apr 14, 2015
Kind
B2
Abstract

Compounds of structural formula I are inhibitors of prolylcarboxypeptidase (PrCP). The compounds of the present invention are useful for the prevention and treatment of conditions related to the enzymatic activity of PrCP such as abnormal metabolism, including obesity; diabetes; metabolic syndrome; obesity related disorders; and diabetes related disorders.

Claims (183)

1. A compound of structural formula I:

or a pharmaceutically acceptable salt thereof; wherein

X is selected from the group consisting of:

(1) —O—,

(2) —S—, and

(3) —NR a —;

Y is selected from the group consisting of:

(1) —N—, and

(2) —CH—;

Z is selected from the group consisting of:

(1) —CH 2 —, and

(2) —NR 5 —,

provided that if Y is N, then Z is not —NR 5 —;

each R 1 is independently selected from the group consisting of:

(1) phenyl, and

(2) —(CH 2 ) 2 -phenyl,

wherein each CH 2 , and phenyl is unsubstituted or substituted with one to two groups independently selected from R b ;

each R 2 is independently selected from the group consisting of:

(1) hydrogen,

(2) —OH,

(3) halogen,

(4) —CF 3 ,

(5) —OCF 3 ,

(6) —C 1-6 alkyl,

(7) —OC 1-6 alkyl,

(8) —CO 2 H, and

(9) —C(O)N(R g ) 2 ,

wherein each alkyl is unsubstituted or substituted with one to four substituents selected from R c ;

each R 3 is independently selected from the group consisting of:

(1) —(CH 2 ) p aryl, and

(2) —(CH 2 ) p heteroaryl,

wherein CH 2 , aryl and heteroaryl are unsubstituted or substituted with one to three substituents selected from R d ;

R 4 is phenyl, wherein phenyl is unsubstituted or substituted with one to three substituents selected from R e ;

each R 5 is independently selected from the group consisting of:

(1) hydrogen,

(2) —CO 2 C 1-6 alkyl,

(3) —C(O)N(R g )C 1-6 alkyl,

(4) —C(O)C 1-6 alkyl, and

(5) —(CH 2 ) q aryl,

wherein each alkyl and aryl is unsubstituted or substituted with one to four substituents selected from R h ;

each R a is independently selected from the group consisting of:

(1) hydrogen, and

(2) —C 1-6 alkyl;

each R b is independently selected from the group consisting of:

(1) oxo,

(2) —OH,

(3) —CF 3 ,

(4) —OCF 3 ,

(5) halogen,

(6) C 1-6 alkyl,

(7) —OC 1-6 alkyl,

(8) —CO 2 H, and

(9) —CO 2 C 1-6 alkyl;

each R c is independently selected from the group consisting of:

(1) —OH,

(2) —CN,

(3) —CF 3 ,

(4) —OCF 3 ,

(5) halogen,

(6) —C 1-6 alkyl,

(7) —OC 1-6 alkyl,

(8) —CO 2 H, and

(9) —CO 2 C 1-6 alkyl;

each R d is independently selected from the group consisting of:

(1) —OH,

(2) —CN,

(3) —CF 3 ,

(4) —OCF 3 ,

(5) halogen,

(6) —C 1-6 alkyl,

(7) —OC 1-6 alkyl,

(8) —CO 2 H, and

(9) —CO 2 C 1-6 alkyl;

each R e is independently selected from the group consisting of:

(1) —OH,

(2) —CN,

(3) —CF 3 ,

(4) —OCF 3 ,

(5) halogen,

(6) —C 1-6 alkyl,

(7) —OC 1-6 alkyl,

(8) —CO 2 H, and

(9) —CO 2 C 1-6 alkyl;

each R f is independently selected from the group consisting of:

(1) hydrogen, and

(2) —C 1-6 alkyl;

each R g is independently selected from the group consisting of:

(1) hydrogen, and

(2) —C 1-6 alkyl;

each R h is independently selected from the group consisting of:

(1) —OH,

(2) oxo,

(3) —CN,

(4) —CF 3 ,

(5) —OCF 3 ,

(6) halogen,

(7) —C 1-6 alkyl,

(8) —OC 1-6 alkyl,

(9) —CO 2 H, and

(10) —CO 2 C 1-6 alkyl;

m is selected from 0, 1, 2 and 3;

n is selected from 0, 1, 2, and 3;

p is selected from 0, 1, 2 and 3; and

q is selected from 0, 1, 2 and 3.

2. The compound of claim 1 wherein Y is —N—; and Z is —CH 2 —; or a pharmaceutically acceptable salt thereof.

3. The compound of claim 1 wherein each R 1 is —(CH 2 ) 2 -phenyl, wherein each —CH 2 and phenyl is unsubstituted or substituted with one to two groups independently selected from R b ; or a pharmaceutically acceptable salt thereof.

4. The compound of claim 1 wherein each R 2 is independently selected from the group consisting of:

(1) hydrogen, and

(2) —OH;

or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 wherein each R 3 is independently selected from the group consisting of:

(1) phenyl,

(2) pyridine, and

(3) pyrimidine,

wherein phenyl, pyridine and pyrimidine are unsubstituted or substituted with one to three substituents selected from R d ; or a pharmaceutically acceptable salt thereof.

6. The compound of claim 1 wherein

X is selected from the group consisting of:

(1) —O—,

(2) —S—, and

(3) —NR a —;

Y is selected from the group consisting of:

(1) —N—, and

(2) —CH—;

Z is selected from the group consisting of:

(1) —CH 2 —, and

(2) —NR 5 —,

provided that if Y is N, then Z is not —NR 5 —;

each R 1 is independently selected from the group consisting of:

(1) phenyl, and

(2) —(CH 2 ) 2 -phenyl,

wherein each CH 2 , and phenyl is unsubstituted or substituted with one to two groups independently selected from R b ;

each R 2 is independently selected from the group consisting of:

(1) hydrogen, and

(2) —OH;

each R 3 is independently selected from the group consisting of:

(1) —(CH 2 ) p aryl, and

(2) —(CH 2 ) p heteroaryl,

wherein CH 2 , aryl and heteroaryl are unsubstituted or substituted with one to three substituents selected from R d ;

R 4 is phenyl, wherein phenyl is unsubstituted or substituted with one to three substituents selected from R e ;

each R 5 is independently selected from the group consisting of:

(1) hydrogen,

(2) —CO 2 C 1-6 alkyl,

(3) —C(O)N(R g )C 1-6 alkyl,

(4) —C(O)C 1-6 alkyl, and

(5) —(CH 2 ) q aryl,

wherein each alkyl and aryl is unsubstituted or substituted with one to four substituents selected from R h ;

m is 0 or 2;

p is 0 or 1; and

q is 0 or 1;

or a pharmaceutically acceptable salt thereof.

7. The compound of claim 1 wherein:

X is selected from the group consisting of:

(1) —O—,

(2) —S—, and

(3) —NR a —;

Y is selected from the group consisting of:

(1) —N—, and

(2) —CH—;

Z is selected from the group consisting of:

(1) —CH 2 —, and

(2) —NR 5 —,

provided that if Y is N, then Z is not —NR 5 —;

each R 1 is independently selected from the group consisting of:

(1) phenyl, and

(2) —(CH 2 ) 2 -phenyl,

wherein each CH 2 , and phenyl is unsubstituted or substituted with one to two groups independently selected from R b ;

each R 2 is independently selected from the group consisting of:

(1) hydrogen, and

(2) —OH;

each R 3 is independently selected from the group consisting of:

(1) phenyl,

(2) pyridine, and

(3) pyrimidine,

wherein phenyl, pyridine and pyrimidine are unsubstituted or substituted with one to three substituents selected from R d ;

R 4 is phenyl, wherein phenyl is unsubstituted or substituted with one to three substituents selected from R e ;

each R 5 is independently selected from the group consisting of:

(1) hydrogen, and

(2) —(CH 2 ) 2 -phenyl,

wherein each phenyl is unsubstituted or substituted with one to four substituents selected from R h ;

or a pharmaceutically acceptable salt thereof.

8. The compound of claim 7 selected from the group consisting of:

or a pharmaceutically acceptable salt thereof.

9. A pharmaceutical composition comprising a compound of claim 1 in combination with a pharmaceutically acceptable carrier.

Assignments (2)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 7, 2012
From: DEBENHAM, JOHN S.; JIANG, JINLONG; MADSEN-DUGGAN, CHRISTINA B.; SHEN, DONG-MING
To: MERCK SHARP & DOHME CORP
Reel/Frame 029425/0169 →