IP Library Granted Patent US 9,217,085
Granted Patent B2
US 9,217,085 · App. 13/811,526 · Granted Dec 22, 2015

Method of coating an inorganic substrate with a stable organic layer

Inventors: Fabien Bellenger (Shanghai, CN); Floryan De Campo (Shanghai, CN); Camille Jourde (Paris, FR); Tao Zhang (Shanghai, CN)
Assignee: SOLVAY (CHINA) CO;. LTD
C09D4/00C03C17/324C07F9/3826C07F9/48
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Quick Facts
Patent No.
US 9,217,085
App. No.
13/811,526
Granted
Dec 22, 2015
Kind
B2
Abstract

A method for coating a metallic or inorganic substrate is described, such as metal or glass supports, with an organic layer comprising conjugated diene phosphinate or phosphonate compounds.

Claims (24)

1. A method of coating at least one surface of an inorganic substrate with an organic coating, the method comprising the following steps:

(a) treating the at least one surface of the substrate by contacting said surface with a composition consisting of a solvent and at least one compound having the following formula (I):

wherein,

each of R 1 , R 2 , R 3 , R 4 , and R 5 , which can be identical or different, and is selected from hydrogen, an alkyl, an aryl, an alkaryl, an aralkyl, a cycloalkyl, a heterocycloalkyl, or an alkenyl group;

R 6 is selected from H, an alkyl, an aryl, an alkaryl, an aralkyl, a cycloalkyl, a heterocycloalkyl,

an alkenyl group, or an —OR 8 group, wherein R 8 is selected from a hydrogen, an alkyl, an aryl, an alkaryl, an aralkyl, a cycloalkyl, a heterocycloalkyl, an alkenyl group, or a metal selected from the group consisting of Na, Li, and Ca, or an ammonium compound;

R 7 is selected from a hydrogen, an alkyl, an aryl, an alkaryl, an aralkyl, a cycloalkyl, or an alkenyl group, or a metal selected from the group consisting of Na, Li, and Ca, or an ammonium compound;

whereby the at least one compound of formula (I) adsorbs on said surface; and

(b) submitting the surface of the substrate modified in the treatment of step (a) to heat or UV irradiation;

whereby the at least one compound of formula (I) reacts and forms a stable coating on said surface.

2. The method as defined by claim 1 , wherein R 1 , R 2 and R 4 are hydrogen; R 3 and R 5 are methyl; and R 7 is hydrogen.

3. The method as defined by claim 1 , wherein R 6 is hydrogen.

4. The method as defined by claim 1 , wherein R 8 is hydrogen.

5. The method as defined by claim 1 , wherein the compound of formula (I) is a conjugated diene phosphinate.

6. The method as defined by claim 1 , wherein the compound of formula (I) is a conjugated diene phosphonate compound having the following formula:

7. The method as defined by claim 1 , wherein the method further comprises a preliminary treatment of the substrate before step (a).

8. The method as defined by claim 7 , wherein the preliminary treatment comprises oxidation of the surface of the substrate.

9. The method as defined by claim 1 , wherein the method further comprises washing of the substrate after step (b).

10. The method as defined by claim 9 , wherein the substrate is washed with acetone.

11. The method as defined by claim 1 , wherein the substrate comprises steel, aluminium, an alloy thereof, or an oxide thereof.

12. The method as defined by claim 1 , wherein the substrate is glass or tin oxide.

13. The method as defined by claim 1 , wherein the method protects the substrate against corrosion.

14. The method as defined by claim 1 , wherein the method modifies wettability and/or hydrophobicity of the substrate.

15. The method as defined by claim 1 , wherein the method improves paintability of the substrate.

Assignments (2)
CHANGE OF NAME Recorded Apr 1, 2014
From: RHODIA (CHINA) CO., LTD
To: SOLVAY (CHINA) CO., LTD
Reel/Frame 032579/0488 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 17, 2013
From: BELLENGER, FABIEN; DE CAMPO, FLORYAN; JOURDE, CAMILLE; ZHANG, TAO
To: RHODIA (CHINA) CO., LTD.
Reel/Frame 030625/0267 →
Continuity (1)
Related Publication 20130122213A1 · May 16, 2013