IP Library Granted Patent US 9,493,433
Granted Patent B2
US 9,493,433 · App. 13/811,925 · Granted Nov 15, 2016

Method for preserving aqueous solution containing leuco chromogen

Inventors: Haruyo Soya (Sunto-gun, JP); Tomomi Murakami (Sunto-gun, JP); Haruki Tsunoda (Sunto-gun, JP); Yu Ohsugi (Sunto-gun, JP); Ayako Yoda (Sunto-gun, JP); Masashi Matsushita (Sunto-gun, JP)
Assignee: KYOWA MEDEX CO., LTD.
C07D279/30C09B11/12C09B21/00C09B67/0077C09B67/0083C12Q1/28G01N33/723
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Quick Facts
Patent No.
US 9,493,433
App. No.
13/811,925
Granted
Nov 15, 2016
Kind
B2
Abstract

Described is a method for preserving an aqueous solution comprising a leuco chromogen, comprising adding at least one compound selected from the group consisting of polyoxyethylene alkylamine and polyoxyethylene alkenylamine to the aqueous solution containing a leuco chromogen, and a method for stabilizing a leuco chromogen, comprising allowing the leuco chromogen to coexist in an aqueous solution comprising at least one compound selected from the group consisting of polyoxyethylene alkylamine and polyoxyethylene alkenylamine.

Claims (8)

1. A method for stabilizing a leuco chromogen, comprising allowing the leuco chromogen to coexist for at least seven days in an aqueous solution comprising at least one compound selected from the group consisting of polyoxyethylene alkylamine with an alkyl having 8 to 20 carbon atoms and polyoxyethylene alkenylamine with an alkenyl having 8 to 20 carbon atoms, wherein

the leuco chromogen is a phenothiazine chromogen selected from the group consisting of 10-N-(carboxymethylaminocarbonyl)-3,7-bis(dimethylamino)-10H-phenothiazine contained at a concentration of 0.0001 to 2.0 mmol/L and 10-N-methylcarbamoyl-3,7-bis(dimethylamino)-10H-phenothiazine contained at a concentration of 0.1 to 2.0 mmol/L in said aqueous solution, and

the polyoxyethylene alkylamine or the polyoxyethylene alkenylamine is contained at a concentration of 0.5 to 5% in said aqueous solution.

2. The method according to claim 1 , wherein the phenothiazine chromogen is 10-N-(carboxymethylaminocarbonyl)-3,7-bis(dimethylamino)-10H-phenothiazine.

3. The method according to claim 1 , wherein the leuco chromogen is 10-N-(carboxymethylaminocarbonyl)-3,7-bis(dimethylamino)-10H-phenothiazine contained at a concentration of 0.0005 to 1.0 mmol/L in said aqueous solution.

4. The method according to claim 1 , wherein the degree of polymerization of oxyethylene in the polyoxyethylene alkylamine is 1-24, and the degree of polymerization of oxyethylene in the polyoxyethylene alkenylamine is 1-24.

5. The method according to claim 2 , wherein the degree of polymerization of oxyethylene in the polyoxyethylene alkylamine is 1-24, and the degree of polymerization of oxyethylene in the polyoxyethylene alkenylamine is 1-24.

6. The method according to claim 3 , wherein the degree of polymerization of oxyethylene in the polyoxyethylene alkylamine is 1-24, and the degree of polymerization of oxyethylene in the polyoxyethylene alkenylamine is 1-24.

Assignments (4)
CHANGE OF NAME Recorded Sep 23, 2025
From: KYOWA MEDEX CO., LTD.
To: HITACHI CHEMICAL DIAGNOSTICS SYSTEMS CO., LTD.
Reel/Frame 072925/0508 →
CHANGE OF NAME Recorded Sep 23, 2025
From: HITACHI CHEMICAL DIAGNOSTICS SYSTEMS CO., LTD.
To: MINARIS MEDICAL CO., LTD.
Reel/Frame 072925/0657 →
CHANGE OF NAME Recorded Sep 23, 2025
From: MINARIS MEDICAL CO., LTD.
To: CANON MEDICAL DIAGNOSTICS CORPORATION
Reel/Frame 072925/0690 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 24, 2013
From: SOYA, HARUYO; MURAKAMI, TOMOMI; TSUNODA, HARUKI; OHSUGI, YU; YODA, AYAKO; MATSUSHITA, MASASHI
To: KYOWA MEDEX CO., LTD.
Reel/Frame 029686/0435 →
Priority Claims (1)
JP 2010-180564 · Aug 11, 2010 · national
Continuity (1)
Related Publication 20130123491A1 · May 16, 2013