IP Library Granted Patent US 10,357,575
Granted Patent B2
US 10,357,575 · App. 13/825,941 · Granted Jul 23, 2019

Stabilized nanobubbles for diagnostic and therapeutic applications

Inventors: Agata Exner (Westlake, OH); Tianyi Krupka (Westlake, OH); Luis Solorio (University Heights, OH)
Assignee: CASE WESTERN RESERVE UNIVERSITY
A61K49/223A61K9/1271
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,357,575
App. No.
13/825,941
Granted
Jul 23, 2019
Kind
B2
Abstract

A stabilized nanobubble can include a membrane that defines at least one internal void, which includes at least one gas. The membrane can include at least one lipid and at least one nonionic triblock copolymer that is effective to control the size of the nanobubble without compromising in vitro and in vivo echogenicity of the nanobubble.

Claims (15)

1. A plurality of stabilized nanobubbles, each nanobubble comprising:

a membrane that defines at least one internal void, which includes at least one gas, the membrane including a plurality of lipids and poloxamers that are incorporated between lipids of the membrane and that are effective to control the size of the nanobubble without compromising in vitro and in vivo echogenicity of the nanobubble, each poloxamer having a molecular weight of 1100 Da to 4600 Da, each nanobubble having a diameter of about 50 nm to about 800 nm, and the nanobubbles having a polydispersity of about 0.1 to about 0.5, a zeta potential of about −30 mV to about −70 mV, and a poloxamer concentration of 0.06 mg/ml to 6 mg/ml.

2. The stabilized nanobubbles of claim 1 , each nanobubble having a diameter of about 100 nm to about 600 nm.

3. The stabilized nanobubbles of claim 1 , the poloxamers comprising at least one poloxamer having the chemical formula of:

HO—(C 2 H 4 O) 2 (C 3 H 6 O) 31 (C 2 H 4 O) 2 —H.

4. The stabilized nanobubbles of claim 3 , each nanobubble having a lipid:poloxamer molar ratio of about 30:1 to about 40:1.

5. The stabilized nanobubbles of claim 1 , the poloxamers comprising at least one poloxamer having the chemical formula of:

HO—(C 2 H 4 O) 3 (C 3 H 6 O) 43 (C 2 H 4 O) 3 —H.

6. The stabilized nanobubbles of claim 5 , each nanobubble having a lipid:poloxamer molar ratio of about 40:1 to about 50:1.

7. The stabilized nanobubbles of claim 1 , the lipids comprising 1,2-dipalmitoyl-sn-glycero-3-phosphocholine, dipalmitoyl-sn-glycero-3-phosphoethanolamine, and dipalmitoyl-sn-glycero-3-phosphate.

8. The stabilized nanobubbles of claim 1 , further comprising at least one targeting moiety that is linked to the membrane of each nanobubble.

9. The stabilized nanobubbles of claim 8 , the targeting moiety being selected from the group consisting of polypeptides, polynucleotides, small molecules, elemental compounds, antibodies, and antibody fragments.

10. The stabilized nanobubbles of claim 1 , further comprising at least one therapeutic agent that is contained within the membrane of each nanobubble or conjugated to the membrane of each nanobubble.

11. The stabilized nanobubbles of claim 10 , the at least one therapeutic agent comprising a chemotherapeutic agent, anti-proliferative agent, biocidal agent, biostatic agent, and/or an anti-microbial agent.

12. The stabilized nanobubbles of claim 1 , the poloxamers having a hydrophobic/lipophilic balance (HLB) between about 1 to about 7.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jun 7, 2016
From: CASE WESTERN RESERVE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 038903/0553 →
CONFIRMATORY LICENSE Recorded Feb 24, 2014
From: CASE WESTERN RESERVE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 032329/0830 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2013
From: EXNER, AGATA; KRUPKA, TIANYI; SOLORIO, LUIS
To: CASE WESTERN RESERVE UNIVERSITY
Reel/Frame 030653/0135 →
Continuity (2)
Provisional Application 61386193 · Sep 24, 2010
Related Publication 20140147390A1 · May 29, 2014