IP Library Granted Patent US 9,192,919
Granted Patent B2
US 9,192,919 · App. 13/830,320 · Granted Nov 24, 2015

Selective alkane activation with single-site atoms on amorphous support

Inventors: Adam S. Hock (Chicago, IL); Neil M. Schweitzer (Evanston, IL); Jeffrey T. Miller (Naperville, IL); Bo Hu (Chicago, IL)
Assignee: UChicago Argonne, LLC
B01J23/755B01J21/08B01J23/06B01J23/08B01J23/72B01J23/745B01J23/75B01J35/002B01J35/023B01J35/1019B01J35/1047B01J37/0201B01J37/0203B01J37/0209B01J37/0238B01J37/035B01J37/06B01J37/18C07C5/322C07C5/3332C07C2521/08C07C2523/06
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,192,919
App. No.
13/830,320
Granted
Nov 24, 2015
Kind
B2
Abstract

The present invention relates generally to catalysts and methods for use in olefin production. More particularly, the present invention relates to novel amorphously supported single-center, Lewis acid metal ions and use of the same as catalysts.

Claims (11)

1. A method of alkane dehydrogenation comprising the step of:

reacting an alkane with a single-atom Lewis acid catalyst on an amorphous silica support to form an alkene and hydrogen;

wherein the amorphously supported single-atom Lewis acid catalyst comprises a Lewis acid metal that is selected from the group consisting of Fe, Co, Zn, Ni, Ti, Sc, Zr, Hf, Ce, Ta, La, Ga, and the lanthanides.

2. The method of claim 1 , wherein the Lewis acid metal is selected from the group consisting of Fe, Co, Zn, and Ga.

3. The method of claim 1 , wherein the catalytically active ion does not change oxidation state under the alkane dehydrogenation reaction conditions.

4. The method of claim 1 , wherein the catalyst has a selectivity of greater than 75% for C—H activation.

5. The method of claim 1 , wherein the catalyst has a selectivity of greater than 90% for C—H activation.

6. The method of claim 1 , wherein the catalyst has a selectivity of greater than 95% for C—H activation.

7. The method of claim 1 , wherein the catalyst retains catalytic activity for longer than 1 hour.

8. The method of claim 1 , wherein the catalyst retains catalytic activity for longer than 12 hours.

9. The method of claim 1 , wherein the catalyst retains catalytic activity for longer than 24 hours.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE SERIAL NO. 13/830230 SHOULD BE 13/830320 PREVIOUSLY RECORDED ON REEL 036811 FRAME 0034. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Nov 16, 2015
From: SCHWEITZER, NEIL M.; MILLER, JEFFREY T.
To: UCHICAGO ARGONNE, LLC
Reel/Frame 037525/0410 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 16, 2015
From: SCHWEITZER, NEIL M.; MILLER, JEFFREY T.
To: UCHICAGO ARGONNE, LLC
Reel/Frame 036811/0034 →
CONFIRMATORY LICENSE Recorded Aug 16, 2013
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 031189/0915 →
Continuity (1)
Related Publication 20140275686A1 · Sep 18, 2014