IP Library Granted Patent US 9,377,245
Granted Patent B2
US 9,377,245 · App. 13/833,357 · Granted Jun 28, 2016

Heat exchanger life extension via in-situ reconditioning

Inventors: David E. Holcomb (Oak Ridge, TN); Govindarajan Muralidharan (Knoxville, TN)
Assignee: UT-Battelle, LLC
F28D7/06C22F1/10C22F1/00F28F2225/02F28F2245/00F28F2265/00
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Quick Facts
Patent No.
US 9,377,245
App. No.
13/833,357
Granted
Jun 28, 2016
Kind
B2
Abstract

A method of in-situ reconditioning a heat exchanger includes the steps of: providing an in-service heat exchanger comprising a precipitate-strengthened alloy wherein at least one mechanical property of the heat exchanger is degraded by coarsening of the precipitate, the in-service heat exchanger containing a molten salt working heat exchange fluid; deactivating the heat exchanger from service in-situ; in a solution-annealing step, in-situ heating the heat exchanger and molten salt working heat exchange fluid contained therein to a temperature and for a time period sufficient to dissolve the coarsened precipitate; in a quenching step, flowing the molten salt working heat-exchange fluid through the heat exchanger in-situ to cool the alloy and retain a supersaturated solid solution while preventing formation of large precipitates; and in an aging step, further varying the temperature of the flowing molten salt working heat-exchange fluid to re-precipitate the dissolved precipitate.

Claims (18)

1. A method of in-situ reconditioning a heat exchanger comprising the steps of:

a. providing an in-service heat exchanger comprising a precipitate-strengthened alloy wherein at least one mechanical property of said heat exchanger is degraded by coarsening of said precipitate, said in-service heat exchanger containing a molten salt working heat exchange fluid;

b. deactivating said heat exchanger from service in-situ;

c. in a solution-annealing step, in-situ heating said heat exchanger and molten salt working heat exchange fluid contained therein to a temperature and for a time period sufficient to dissolve said coarsened precipitate;

d. in a quenching step, flowing said molten salt working heat-exchange fluid through said heat exchanger in-situ to cool said alloy and retain a supersaturated solid solution; and

e. in an aging step, further varying the temperature of said flowing molten salt working heat-exchange fluid to re-precipitate said dissolved precipitate.

2. A method in accordance with claim 1 wherein said precipitate is a gamma-prime (γ′) precipitate.

3. A method in accordance with claim 1 wherein said solution-annealing step is carried out at a temperature in the range of 870° C. to 1150° C.

4. A method in accordance with claim 1 wherein said solution-annealing step is carried out by energizing a heating jacket.

5. A method in accordance with claim 1 wherein said quenching step is carried out at a temperature in the range of no lower than the lowest temperature at which said working fluid will remain sufficiently fluid to flow to a temperature below a working temperature of said heat exchanger.

6. A method in accordance with claim 5 wherein said temperature range is 550° C. to 650° C.

7. A method in accordance with claim 1 wherein said aging step is carried out at a temperature in the range of 600° C. to 850° C.

8. A method in accordance with claim 1 wherein said aging step is carried out at a maximum temperature no greater than a normal operating temperature of said heat-exchanger.

9. A method in accordance with claim 1 wherein said aging step further comprises flowing a power cycle fluid through said heat exchanger.

10. A method in accordance with claim 1 wherein said aging step further comprises energizing a heating jacket.

11. A method in accordance with claim 1 further comprising an additional, subsequent step of:

f. reactivating said heat exchanger to service.

12. A method in accordance with claim 1 further comprising an additional step of, after said deactivating step and prior to said solution-annealing step, draining a power cycle heat-exchange fluid from said heat exchanger.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 28, 2013
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 031106/0388 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 22, 2013
From: HOLCOMB, DAVID E.; MURALIDHARAN, GOVINDARAJAN
To: UT-BATTELLE, LLC
Reel/Frame 030068/0518 →
Continuity (1)
Related Publication 20140261901A1 · Sep 18, 2014