IP Library › Granted Patent US 9,312,130
Granted Patent B2
US 9,312,130 · App. 13/942,257 · Granted Apr 12, 2016

Surface doping and bandgap tunability in hydrogenated graphene

Inventors: Jeffrey W. Baldwin (Fairfax, VA); Bernard R. Matis (Alexandria, VA); James S. Burgess (Nahsua, NH); Felipe Bulat-Jara (Washington, DC); Adam L. Friedman (Silver Spring, MD); Brian H Houston (Fairfax, VA)
Assignee: The United States of America, as represented by the Secretary of the Navy
H01L21/02518H01B5/14H01B13/30H01L21/02381H01L21/02488H01L21/02527H01L21/02664H01L21/2236H01L29/1606
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Quick Facts
Patent No.
US 9,312,130
App. No.
13/942,257
Granted
Apr 12, 2016
Kind
B2
Abstract

A method of introducing a bandgap in single layer graphite on a SiO 2 substrate comprising the steps of preparing graphene flakes and CVD grown graphene films on a SiO 2 /Si substrate and performing hydrogenation of the graphene. Additionally, controlling the majority carrier type via surface adsorbates.

Claims (27)

1. A method of introducing a bandgap in single layer graphene on a SiO 2 substrate comprising the steps of:

preparing graphene flakes or chemical vapor deposition grown graphene films on a SiO 2 /Si substrate;

exposing the graphene flakes or the chemical vapor deposition grown graphene film to hydrogen plasma;

performing hydrogenation of the graphene;

wherein the hydrogenated graphene has a majority carrier type;

creating a bandgap from the hydrogenation of the graphene;

applying an electric field to the hydrogenated graphene; and

tuning the bandgap.

2. The method of claim 1 further including the step of:

controlling the majority carrier type via surface adsorbates.

3. The method of claim 2 further comprising the steps of:

attaching by physisorption the surface adsorbates to the hydrogenated graphene;

converting the majority carrier type from electrons to holes using the surface adsorbates;

converting the majority carrier type from n-type to p-type;

removing the surface adsorbates;

preserving the hydrogenated graphene band structure; and

converting the majority carrier type from p-type to n-type.

4. A method of hydrogenating graphene and forming a bandgap comprising the steps of:

preparing exfoliated graphene flakes or a chemical vapor deposition (CVD) grown graphene film on a SiO 2 /Si substrate;

depositing contact electrodes on the exfoliated graphene flakes or the CVD grown graphene films;

exposing the exfoliated graphene flakes or the chemical vapor deposition grown graphene film to hydrogen plasma;

hydrogenating the exfoliated graphene flakes or the CVD grown graphene films;

creating a bandgap from the step of hydrogenating the graphene;

applying an electric field to the hydrogenated graphene; and

tuning the bandgap.

5. The method of claim 4 wherein the hydrogenating is performed with 15-30 W, 1.5 Torr H 2 , 100 sccm H 2 , 32 C, for 15-30 seconds.

6. The method of claim 5 wherein said contact electrodes are Cr/Au contact electrodes.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 4, 2014
From: BALDWIN, JEFFREY W; MATIS, BERNARD R; BURGESS, JAMES S; FRIEDMAN, ADAM L; HOUSTON, BRIAN H; BULAT-JARA, FELIPE
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY COMPANY
Reel/Frame 033023/0738 →
Continuity (2)
Provisional Application 61701029 · Sep 14, 2012
Related Publication 20140080295A1 · Mar 20, 2014